Stereo Scan 440 - DCU

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~ Running the Filament Up Standard run-up macros for Denka and Kimball LaB6 filaments are provided by Leica. These will set the EHT to 5kV and the filament current to a value normally below the saturation point for the appropriate filament type. It is recommended that these are used initially when running with LaB6 and then when the desired operating conditions are achieved that additional run-up macros are created for future use. ~ Kimball To select the appropriate macro select File from the top menu line followed by Load state. This produced a list of application macros from which the appropriate run-up macro can be selected. Select DenkaS.app for Denka M3 filaments and KimbS.app for Kimball Physics filaments. filaments run with a much lower heating current so the selection of an incorrect macro could result in the filament being destroyed. Once Open has been selected the macro will be loaded and run up of the filament will commence. If there is a conflict between the conditions in the macro and those currently set on the system then the macro will halt and a warning will be given and the Operator will be asked whether or not to proceed. It is advisable to select No and to investigate the reason for the conflict. Once this has been corrected then the macro can be loaded and run again. Once the run up sequence is completed it is advisable to check for correct filament saturation and beam alignment. Use the Gun Align panel to select Emiaion Image mode and adjust the filament cuuent to produce the desired emission image (see Figures 9,10,11,12). Stereoscan 440 Operator Manual
Figures 9,10,11,12 Emission Images ~ ~ Changes to the filament current will be implemented slowly in order to safeguard the filament. Use the Gun TOt conttol to position the emission image in the centre of the screen. Then with the magnification set to very low and Optibeam depth mode selected, re-centre the emission image using the Gun shift conttols. Turn off Optibeam depth mode and increase the magnification and fe-check the position of the emission image, if necessary make adjustments using the Gun TOt conttols. When the alignment has been completed the emission image mode can be turned off by selecting the Nonnal button within the Gun Align panel. Stereoscan 440 Operator Manual
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All reasonable steps have been take
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Instrument Photographic Choice of I
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iv Contents Chapter 5 - Maintenance
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The specimen chamber of the Slereos
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The User Interface Overview The use
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5. Panel Selection There is one oth
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B If B is pressed. the arrow keys m
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The top window, see Figure 1.3, pro
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Individual items can be selected or
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1~1~ Chapter 1 Getting Started i '
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all the operating conditions of the
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1-20 ~bapter 1 ~g S~ move the mouse
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FIgUre 1.10 Image of First Peak Set
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Chapter 2 This chapter contains the
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Chapter 1. Operation 2--3 " -- Scan
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Chapter 2. Operation 2.,.,5 ,- . ..
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, , Chapter 1. ~ - 2-- 7 ""a-uu"" 1
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1. Admit air to the gun. Open the g
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Automatic Stage lnitialise The stag
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For LaB,:- 1 Press the Emission but
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~I.~ Chapter 2 Operation -'--"=-,'Z
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2-18 Chapter 1. Operation - - - - a
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2-20 Chapter 2. Operation. 1 2 t Se
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2-22 Chapter 1. Operation If the wo
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2-24 Chapter 2 Operation The Zone T
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Quad Mode Quad mode is selected fro
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2-28 Chapter 2 Operation . - -, , "
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On the histogram display there is a
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Panels A panel is a special kind of
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current text string). In addition t
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Micron Markers Two types of micron
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Graticule and Crosshairs Graticule
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HRRU Camera This sets the type of c
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2..42 Cbapter 1. Operation ~ I It h
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current when the image was saved. T
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2-46 Chapter 2 Operation The Clipbo
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Having now become familiar with the
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high a probe current, thus the acce
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, Chapter 3 Advanced Operation 3-5
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3. The retractable backscattered el
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I~.." - Chapter 3 Advanced Operatio
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"".~-I Chapter 3 Advanced Operation
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" Chapter 3 Advanced Operation 3-13
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Non-Volatile, Non-Conductors If it
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The solvent is then allowed to evap
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Chapter 3 Advanced ~OD 3-19 -c - -
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Other Menu Features The display of
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Points and Steps In addition to the
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Confirm This instruction check that
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._~ Chapter c" ~ 3 Advanced Operati
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Remove Removing a macro from a libr
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The position in the list can be con
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Install The install option copies t
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Chapter 3 AdvancedOperati on 3-35 3
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I I PARAMETER I En"ECT OPTIMUM COMM
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4.5. Good Housekeeping, i.e. keepin
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Chapter -. 4 System Management - +3
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4.1.5. Directory Contents I \nGA i
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4.3. The User Directory Concept A u
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I this be reql!i~. File Types, e.g.
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6-12 Chapter 6 Fault Diagnosis The
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5-2 Chapter 5 Maintenance 5.1.2. Ai
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STEEL AND ST ~S STEEL, COPPER AND m
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5-6 Chapter 5 Maintenance Cleaning
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Cleaning the Aperture Assembly Vent
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PC Related Faults PC related proble
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6-4 Chapter 6 Fault Diagnosis , .".
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6-6 Chapter 6 Fault Diagnosis The I
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6-8 Chapter 6 Fault Diagnosis . 4.
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6-10 Chapter 6 Fault Diagnosis! "I
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This file contains the configuratio
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Please report the problem. F All..E
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Stereoscan 440 Operator Manual NVRA
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6-20 Chapter 6 Fault Diagnosis 4 WW
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Code numbers greater than 40 indica
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WINDOWSTM APPUCA nON ERROR When a W
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Introduction As new Window~ applica
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Appendix ~ The Stereoscan 440 PC! A
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" c., Appeudb C Expansion via the P
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Appendix D Reporting software probl
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Service Manager - SEM Harry M azal
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B-2 Appendix E Options- . Operation
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Controls Angular Measurement The an
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Angular Measurement Each measuremen
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The position of the box can be adju
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I Set the magnification to the requ
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Positioning the Poin~ In Move mode
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&14 Appendix E Options I II Image D
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~ AMaxB This function freezes the i
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Histogram Equalisation The histogra
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Overview The input LUT is used to p
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E-22 Appendix E Options Sawtooth Th
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A group box at the top left of the
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" The communication port used by th
Page 191 and 192: Selection I The signal mixing panel
Page 193 and 194: E- 30 Appendix E Options Select one
Page 195 and 196: E-32 Appendix E Qptions . . High Us
Page 197 and 198: . The stage Move window comprises a
Page 199 and 200: Keyboard Control The cursor (arrow)
Page 201 and 202: E-38 Ap~ ~ Options In addition Macr
Page 203 and 204: Grainl Grain2 actionedl I To indica
Page 205 and 206: The function is provided as part of
Page 207 and 208: Operation Selection Operation of th
Page 209 and 210: Stage Scan Invalid This indicates i
Page 211 and 212: E-48 Appendix E Options ~-",,-;,,~_
Page 213 and 214: Freeze This function will freeze th
Page 215 and 216: 1.21 Trackerbal/ Introduction This
Page 217 and 218: Controls Display the pop up control
Page 219 and 220: Operation Configuration XRay Interf
Page 221 and 222: E-58 Appendix E Options 11_- X Ray
Page 223 and 224: Intensity Dot Map Set Up In dot map
Page 225 and 226: The Linescan data is displayed in a
Page 227 and 228: E-64 AppeDdjx E ~oos ... ~~ full sc
Page 229 and 230: Annotation A set of annotation labe
Page 231 and 232: 2. 2.1 Stage Motorisation The stage
Page 233 and 234: Camera Image Select between Live, S
Page 235 and 236: If the box marked Fast is selected,
Page 237 and 238: Remove the Camera assembly from the
Page 239 and 240: ~--~- ~- , -~~::~ '#:r: .TungsIen F
Page 241: .,, , or_~ :---1 ' ' --~... 'FG'-~-
Page 245 and 246: Assembly Assembly . of the STEM det
Page 247 and 248: 4. Select SCM Image from the Specim
Page 249 and 250: ~ ~ ~ ~ E I I I I I I Stereoscan 44
Page 251 and 252: DOS, 4-1 Dose rate, 3-12 Dual magni
Page 253 and 254: 1-4 Index Rotary pump Oil. 5-2 Oil
Page 255: Appendices s+Shift ff ~ I ARRO~ ~ys
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