ICS-1000 Ion Chromatography System Operator's Manual

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ICS-1000 Ion Chromatography SystemE.10 How do I shut off the system? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-2E.11 How do I store columns? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-2E.12 How do I know when a column is dirty? . . . . . . . . . . . . . . . . . . . . . . . E-3E.13 How do I clean a column? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-3E.14 Why is the conductivity high? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-3F • Glossaryviii Doc. 031879-01 3/03
1 • Introduction1.1 Introduction to Ion Chromatography (IC)The Dionex ICS-1000 Ion Chromatography System (ICS-1000) performs ionanalyses using suppressed or non-suppressed conductivity detection. An ionchromatography system typically consists of a liquid eluent, a high-pressurepump, a sample injector, a guard and separator column, a chemical suppressor, aconductivity cell, and a data collection system.Before running a sample, the ion chromatography system is calibrated using astandard solution. By comparing the data obtained from a sample to that obtainedfrom the known standard, sample ions can be identified and quantitated. The datacollection system, typically a computer running chromatography software,produces a chromatogram (a plot of the detector output vs. time). Thechromatography software converts each peak in the chromatogram to a sampleconcentration and produces a printout of the results.Doc. 031879-01 3/03 1-1
Page 1 and 2: ICS-1000 ION CHROMATOGRAPHY SYSTEMO
Page 3 and 4: Contents1 • Introduction1.1 Intro
Page 6 and 7: ICS-1000 Ion Chromatography System4
Page 8 and 9: ICS-1000 Ion Chromatography SystemB
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Page 20 and 21: ICS-1000 Ion Chromatography SystemI
Page 24 and 25: ICS-1000 Ion Chromatography SystemS
Page 26 and 27: ICS-1000 Ion Chromatography SystemT
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Page 31 and 32: 2 • Features2.3.2 The ICS-1000 Co
Page 33 and 34: 2 • FeaturesSystem Controls Overv
Page 35 and 36: 2 • FeaturesInject ValveDisplays
Page 37 and 38: 2 • Features2.4 System Component
Page 39 and 40: 2 • Features2.4.2 Eluent ValveThe
Page 41 and 42: 2 • FeaturesPressure TransducerFl
Page 43 and 44: 2 • Featuressample loops in vario
Page 45 and 46: 2 • Features2.4.6 SuppressorThe s
Page 47 and 48: 3 • Operation and MaintenanceThis
Page 49 and 50: 3 • Operation and Maintenance3.2
Page 51 and 52: 3 • Operation and Maintenance3. I
Page 53 and 54: 3 • Operation and Maintenance•
Page 59 and 60: 3 • Operation and Maintenance3.9.
Page 61 and 62:
3 • Operation and Maintenancestan
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3 • Operation and Maintenance3.10
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3 • Operation and Maintenancenew
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3 • Operation and Maintenance3.12
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4 • TroubleshootingThis chapter i
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4 • Troubleshooting4.1 Alarms and
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4 • TroubleshootingLOAD/INJECT VA
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4 • TroubleshootingPUMP UNDER PRE
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4 • TroubleshootingSUPPRESSOR STO
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4 • TroubleshootingMake sure the
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4 • Troubleshooting• Blockages
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4 • Troubleshooting4.6 Erratic Fl
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4 • Troubleshooting• Malfunctio
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4 • Troubleshooting• Cell out o
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4 • Troubleshootingb. Under Insta
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5•ServiceThis chapter describes I
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5•ServiceUse the Wellness Panel t
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5•ServiceAfter calibration, the c
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5•Service5.1.4 Calibrating the Va
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5•Service5.3 Replacing Tubing and
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5•Service5.5 Cleaning and Replaci
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5•Service5.6 Replacing a Pump Pis
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5•Service6. The piston does not c
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5•ServiceReinstalling the Head an
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5•ServiceValve KnobO-Ring(P/N 055
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5•Service5. Slide the new cell as
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5•Service11. Align the top of the
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5•Service9. Enter the column heat
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5•Service6. Pull the valve straig
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5•Service5.15 Priming with Isopro
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A • SpecificationsA.1 ElectricalM
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A • SpecificationsA.6 DetectorRan
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B • InstallationThis chapter prov
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Unpacking the ICS-1000 System3. Rem
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Installing ChromeleonB.3 Installing
Page 131 and 132:
Installing the Chromeleon Software
Page 133 and 134:
Connecting the ICS-1000 to the Chro
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Connecting the Power CordB.6 Connec
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Setting Up ChromeleonB.8 Setting Up
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Setting Up Chromeleon10. Click the
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Setting Up Chromeleon2. Select the
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Installing and Plumbing the Columns
Page 145 and 146:
Installing and Plumbing the Columns
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Connecting the Waste LinesB.10 Conn
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Setting Up the Eluent ReservoirVERS
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Setting Up a Chromeleon Application
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Page 155 and 156:
Page 157 and 158:
Page 159 and 160:
Setting the Eluent LevelNOTEIf the
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Priming the Pump3. Open the priming
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Equilibrating the SystemB.15 Equili
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Connecting an AS50 Autosampler (Opt
Page 167 and 168:
Connecting an AS50 Autosampler (Opt
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Connecting an AS40 Automated Sample
Page 171 and 172:
Pressurizing the Eluent Reservoir (
Page 173 and 174:
Pump Continuous Seal Wash Connectio
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Manually Connecting to a Control Pa
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Installation TroubleshootingB.23 In
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C • TTL and Relay ControlNOTEThe
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C • TTL and Relay Controlc. Conne
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C • TTL and Relay Control• Inve
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C • TTL and Relay ControlC.3 Exam
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C • TTL and Relay ControlEnable A
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D • Reordering InformationPart Nu
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E•FAQE.1 How do I hook up an auto
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E•FAQE.12 How do I know when a co
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F • GlossaryAnalytical ColumnSyno
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F • Glossaryof relatively clean s
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F • GlossarySiemens (S)Unit measu
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IndexAAir particulate samples, 3-12
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IndexData rise time, B-46Decibel le
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IndexKKey code (Chromeleon), B-6LLe
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IndexRRear panel, 2-7Analog output
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IndexTTL outputsControlling, C-5Rea
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ICS-1000 Ion Chromatography System Operator's Manual

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