ICS-1000 Ion Chromatography System Operator's Manual

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ICS-1000 Ion Chromatography System1ELUENTWASTEOUTOUT128DEGASPUMP(Optional)SAMPLECONDCELLPULSEDAMPER511INOUT10SUPPRESSORINHEAT EXCHANGERSEPARATOR COLUMNCOLUMN HEATER (optional)7SWL6VALVELPC4OUTPRESS.XDUCER9GUARDWASTEOUTPUMPHEAD3PUMPHEADWASTEININ2ELUENTVALVEOUTFigure 5-2. ICS-1000 Flow SchematicNOTEThe numbers on the flow schematic indicate theorder in which liquid flows through the systemcomponents.5-8 Doc. 031879-01 3/03
5•Service5.3 Replacing Tubing and FittingsThe ICS-1000 is plumbed with the tubing and tubing assemblies listed below.Tubing Size and Type Color Used For0.125-mm (0.005-in) ID PEEK(P/N 044221)0.25-mm (0.010-in) ID PEEK(P/N 042690)0.50-mm (0.020-in) ID PEEK(P/N 042855)0.75-mm (0.030-in) ID PEEK(P/N 044777)1.58-mm (0.062-in) ID Teflon®(P/N 014157)25 µL sample loop(P/N 042857)RedBlackOrangeGreenClearOrangeConnection from pump pulse damperto pressure transducerConnections between other systemcomponentsConnection from injection port toinjection valveConnection from injection valve towasteConnection from pump to degas oreluent reservoir; pump wasteConnection between ports L (1) andL (4) on the injection valve• 10-32 fittings (P/N 043275) and ferrules (P/N 043276) are used for mosttubing connections. For tightening requirements, refer to Installation ofDionex Liquid Line Fittings (Document No. 031432). The manual is on theDionex Reference Library CD-ROM (P/N 053891).• 1/8-in fittings (P/N 052267) and ferrules (P/N 048949) are used forconnections to the suppressor REGEN OUT port and the eluent reservoir.Doc. 031879-01 3/03 5-9
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ICS-1000 ION CHROMATOGRAPHY SYSTEMO
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Contents1 • Introduction1.1 Intro
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ICS-1000 Ion Chromatography System4
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ICS-1000 Ion Chromatography SystemB
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ICS-1000 Ion Chromatography SystemE
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ICS-1000 Ion Chromatography SystemA
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ICS-1000 Ion Chromatography SystemI
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ICS-1000 Ion Chromatography SystemS
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ICS-1000 Ion Chromatography SystemT
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ICS-1000 Ion Chromatography System
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2 • Features2.3.2 The ICS-1000 Co
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2 • FeaturesSystem Controls Overv
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2 • FeaturesInject ValveDisplays
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2 • Features2.4 System Component
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2 • Features2.4.2 Eluent ValveThe
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2 • FeaturesPressure TransducerFl
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2 • Featuressample loops in vario
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2 • Features2.4.6 SuppressorThe s
Page 47 and 48: 3 • Operation and MaintenanceThis
Page 49 and 50: 3 • Operation and Maintenance3.2
Page 51 and 52: 3 • Operation and Maintenance3. I
Page 53 and 54: 3 • Operation and Maintenance•
Page 59 and 60: 3 • Operation and Maintenance3.9.
Page 61 and 62: 3 • Operation and Maintenancestan
Page 65 and 66: 3 • Operation and Maintenancenew
Page 69 and 70: 4 • TroubleshootingThis chapter i
Page 71 and 72: 4 • Troubleshooting4.1 Alarms and
Page 73 and 74: 4 • TroubleshootingLOAD/INJECT VA
Page 75 and 76: 4 • TroubleshootingPUMP UNDER PRE
Page 77 and 78: 4 • TroubleshootingSUPPRESSOR STO
Page 79 and 80: 4 • TroubleshootingMake sure the
Page 81 and 82: 4 • Troubleshooting• Blockages
Page 83 and 84: 4 • Troubleshooting4.6 Erratic Fl
Page 85 and 86: 4 • Troubleshooting• Malfunctio
Page 87 and 88: 4 • Troubleshooting• Cell out o
Page 89 and 90: 4 • Troubleshootingb. Under Insta
Page 91 and 92: 5•ServiceThis chapter describes I
Page 93 and 94: 5•ServiceUse the Wellness Panel t
Page 95 and 96: 5•ServiceAfter calibration, the c
Page 97: 5•Service5.1.4 Calibrating the Va
Page 101 and 102: 5•Service5.5 Cleaning and Replaci
Page 103 and 104: 5•Service5.6 Replacing a Pump Pis
Page 105 and 106: 5•Service6. The piston does not c
Page 107 and 108: 5•ServiceReinstalling the Head an
Page 109 and 110: 5•ServiceValve KnobO-Ring(P/N 055
Page 111 and 112: 5•Service5. Slide the new cell as
Page 113 and 114: 5•Service11. Align the top of the
Page 115 and 116: 5•Service9. Enter the column heat
Page 117 and 118: 5•Service6. Pull the valve straig
Page 119 and 120: 5•Service5.15 Priming with Isopro
Page 121 and 122: A • SpecificationsA.1 ElectricalM
Page 123 and 124: A • SpecificationsA.6 DetectorRan
Page 125 and 126: B • InstallationThis chapter prov
Page 127 and 128: Unpacking the ICS-1000 System3. Rem
Page 129 and 130: Installing ChromeleonB.3 Installing
Page 131 and 132: Installing the Chromeleon Software
Page 133 and 134: Connecting the ICS-1000 to the Chro
Page 135 and 136: Connecting the Power CordB.6 Connec
Page 137 and 138: Setting Up ChromeleonB.8 Setting Up
Page 139 and 140: Setting Up Chromeleon10. Click the
Page 141 and 142: Setting Up Chromeleon2. Select the
Page 143 and 144: Installing and Plumbing the Columns
Page 145 and 146: Installing and Plumbing the Columns
Page 147 and 148: Connecting the Waste LinesB.10 Conn
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Setting Up the Eluent ReservoirVERS
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Setting Up a Chromeleon Application
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Setting the Eluent LevelNOTEIf the
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Priming the Pump3. Open the priming
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Equilibrating the SystemB.15 Equili
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Connecting an AS50 Autosampler (Opt
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Connecting an AS50 Autosampler (Opt
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Connecting an AS40 Automated Sample
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Pressurizing the Eluent Reservoir (
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Pump Continuous Seal Wash Connectio
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Manually Connecting to a Control Pa
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Installation TroubleshootingB.23 In
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C • TTL and Relay ControlNOTEThe
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C • TTL and Relay Controlc. Conne
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C • TTL and Relay Control• Inve
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C • TTL and Relay ControlC.3 Exam
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C • TTL and Relay ControlEnable A
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D • Reordering InformationPart Nu
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E•FAQE.1 How do I hook up an auto
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E•FAQE.12 How do I know when a co
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F • GlossaryAnalytical ColumnSyno
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F • Glossaryof relatively clean s
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F • GlossarySiemens (S)Unit measu
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IndexAAir particulate samples, 3-12
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IndexData rise time, B-46Decibel le
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IndexKKey code (Chromeleon), B-6LLe
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IndexRRear panel, 2-7Analog output
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IndexTTL outputsControlling, C-5Rea
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ICS-1000 Ion Chromatography System Operator's Manual

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