ICS-1000 Ion Chromatography System Operator's Manual

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ICS-1000 Ion Chromatography System4.5 No Flow• Pump waste or priming valve open (see Figure 4-2).Close the valves by turning the knobs clockwise until fingertight. DO NOTOVERTIGHTEN! Overtightening may damage the valve and the pumphead.Waste ValvePriming ValveFigure 4-2. Waste and Priming Valves• Flow rate is set to 0Set the flow rate from either the Chromeleon Control Panel.• Eluent valve is closedOpen the eluent valve from either the Chromeleon Control Panel.• Pump not primedPrime the pump (see Section B.12).• Broken pump pistonReplace the piston (see Section 5.7).4-14 Doc. 031879-01 3/03
4 • Troubleshooting4.6 Erratic Flow/Pressure Reading• Pump needs primingPrime the pump (see Section B.12).• Damaged piston sealReplace the piston seal (see Section 5.6).• Dirty pump check valveClean or replace the check valve (see Section 5.5).• Leaking liquid lines or fittingsCheck the liquid lines and fittings for small leaks. Tighten or, if necessary,replace the liquid line connection (see Section 5.3). Refer to Installation ofDionex Liquid Line Fittings (Document No. 031432) for tighteningrequirements. The manual is on the Dionex Reference Library CD-ROM(P/N 053891).4.7 Excessive System Backpressure• Restriction in the system plumbingCheck all liquid lines for crimping or blockage. Make sure the ferrule fittingsare not overtightened onto tubing. Refer to Installation of Dionex Liquid LineFittings (Document No. 031432) for details. The manual is on the DionexReference Library CD-ROM (P/N 053891). If you have trouble isolating therestriction, refer to Section 5.2.• Plugged or damaged fittingIsolate the faulty fitting by loosening fittings one by one until the pressurereturns to normal. Repair or replace the fitting (see Section 5.3).• Flow rate through the columns too highSet the correct rate for your application. If an incorrect flow rate calibration issuspected, calibrate the flow (see Section 5.1.3).Doc. 031879-01 3/03 4-15
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ICS-1000 ION CHROMATOGRAPHY SYSTEMO
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Contents1 • Introduction1.1 Intro
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ICS-1000 Ion Chromatography System4
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ICS-1000 Ion Chromatography SystemB
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ICS-1000 Ion Chromatography SystemE
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ICS-1000 Ion Chromatography SystemA
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ICS-1000 Ion Chromatography SystemI
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ICS-1000 Ion Chromatography SystemS
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ICS-1000 Ion Chromatography SystemT
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ICS-1000 Ion Chromatography System
Page 31 and 32: 2 • Features2.3.2 The ICS-1000 Co
Page 33 and 34: 2 • FeaturesSystem Controls Overv
Page 35 and 36: 2 • FeaturesInject ValveDisplays
Page 37 and 38: 2 • Features2.4 System Component
Page 39 and 40: 2 • Features2.4.2 Eluent ValveThe
Page 41 and 42: 2 • FeaturesPressure TransducerFl
Page 43 and 44: 2 • Featuressample loops in vario
Page 45 and 46: 2 • Features2.4.6 SuppressorThe s
Page 47 and 48: 3 • Operation and MaintenanceThis
Page 49 and 50: 3 • Operation and Maintenance3.2
Page 51 and 52: 3 • Operation and Maintenance3. I
Page 53 and 54: 3 • Operation and Maintenance•
Page 59 and 60: 3 • Operation and Maintenance3.9.
Page 61 and 62: 3 • Operation and Maintenancestan
Page 65 and 66: 3 • Operation and Maintenancenew
Page 69 and 70: 4 • TroubleshootingThis chapter i
Page 71 and 72: 4 • Troubleshooting4.1 Alarms and
Page 73 and 74: 4 • TroubleshootingLOAD/INJECT VA
Page 75 and 76: 4 • TroubleshootingPUMP UNDER PRE
Page 77 and 78: 4 • TroubleshootingSUPPRESSOR STO
Page 79 and 80: 4 • TroubleshootingMake sure the
Page 81: 4 • Troubleshooting• Blockages
Page 85 and 86: 4 • Troubleshooting• Malfunctio
Page 87 and 88: 4 • Troubleshooting• Cell out o
Page 89 and 90: 4 • Troubleshootingb. Under Insta
Page 91 and 92: 5•ServiceThis chapter describes I
Page 93 and 94: 5•ServiceUse the Wellness Panel t
Page 95 and 96: 5•ServiceAfter calibration, the c
Page 97 and 98: 5•Service5.1.4 Calibrating the Va
Page 99 and 100: 5•Service5.3 Replacing Tubing and
Page 101 and 102: 5•Service5.5 Cleaning and Replaci
Page 103 and 104: 5•Service5.6 Replacing a Pump Pis
Page 105 and 106: 5•Service6. The piston does not c
Page 107 and 108: 5•ServiceReinstalling the Head an
Page 109 and 110: 5•ServiceValve KnobO-Ring(P/N 055
Page 111 and 112: 5•Service5. Slide the new cell as
Page 113 and 114: 5•Service11. Align the top of the
Page 115 and 116: 5•Service9. Enter the column heat
Page 117 and 118: 5•Service6. Pull the valve straig
Page 119 and 120: 5•Service5.15 Priming with Isopro
Page 121 and 122: A • SpecificationsA.1 ElectricalM
Page 123 and 124: A • SpecificationsA.6 DetectorRan
Page 125 and 126: B • InstallationThis chapter prov
Page 127 and 128: Unpacking the ICS-1000 System3. Rem
Page 129 and 130: Installing ChromeleonB.3 Installing
Page 131 and 132: Installing the Chromeleon Software
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Connecting the ICS-1000 to the Chro
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Connecting the Power CordB.6 Connec
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Setting Up ChromeleonB.8 Setting Up
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Setting Up Chromeleon10. Click the
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Setting Up Chromeleon2. Select the
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Installing and Plumbing the Columns
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Installing and Plumbing the Columns
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Connecting the Waste LinesB.10 Conn
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Setting Up the Eluent ReservoirVERS
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Setting Up a Chromeleon Application
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Setting the Eluent LevelNOTEIf the
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Priming the Pump3. Open the priming
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Equilibrating the SystemB.15 Equili
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Connecting an AS50 Autosampler (Opt
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Connecting an AS50 Autosampler (Opt
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Connecting an AS40 Automated Sample
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Pressurizing the Eluent Reservoir (
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Pump Continuous Seal Wash Connectio
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Manually Connecting to a Control Pa
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Installation TroubleshootingB.23 In
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C • TTL and Relay ControlNOTEThe
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C • TTL and Relay Controlc. Conne
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C • TTL and Relay Control• Inve
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C • TTL and Relay ControlC.3 Exam
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C • TTL and Relay ControlEnable A
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D • Reordering InformationPart Nu
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E•FAQE.1 How do I hook up an auto
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E•FAQE.12 How do I know when a co
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F • GlossaryAnalytical ColumnSyno
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F • Glossaryof relatively clean s
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F • GlossarySiemens (S)Unit measu
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IndexAAir particulate samples, 3-12
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IndexData rise time, B-46Decibel le
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IndexKKey code (Chromeleon), B-6LLe
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IndexRRear panel, 2-7Analog output
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IndexTTL outputsControlling, C-5Rea
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ICS-1000 Ion Chromatography System Operator's Manual

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