<strong>ICS</strong>-<strong>1000</strong> <strong>Ion</strong> <strong>Chromatography</strong> <strong>System</strong>PCSee ComputerPeak ghosting, 4-16Peak heightReproducibility, 2-27Troubleshooting, 4-17PeaksExtraneous (ghosting), 4-16PEEKConductivity cell body, 2-27Physical specificationsDecibel level, A-1Dimensions, A-1Weight, A-1Piston sealsReplacement procedure, 5-13 – 5-14,5-16 – 5-17PistonsReplacement procedure, 5-17Plotting detector output, 2-18PlumbingColumns and suppressor, B-25Injection valve, 5-10Replacing tubing and fittings, 5-9Troubleshooting, 5-7PowerTurning on, 3-3, B-12Power cord, 5-30, B-11Power receptacle, 2-8, B-11Power requirements, A-1Power-up conditions, 3-3PressureLimit, 4-7Pump operating specifications, A-2<strong>System</strong>, 4-6 – 4-7Pressure ripple, A-2Pressure slope calibration error, 4-5Pressure transducer, 2-5, 2-23Leaking, 4-10<strong>System</strong> backpressure, 2-23PressurizingEluent reservoir, B-48Priming, 3-9, 5-29, B-36 – B-38Pump is out of prime, 4-12With a syringe, B-36With isopropyl alcohol, 5-29With the Prime button, B-38Priming valveOpening, 2-22O-ring replacement procedure, 5-18Printing, E-1Processing samples, 3-2, 3-18 – 3-19Automatically (batch), 3-2, 3-19<strong>Manual</strong>ly, 3-2, 3-18Product warranty, 5-1Program time, 2-15Programs (Chromeleon), 2-11, 2-15, 3-16 –3-19Run time, 2-15Pulse damper, 2-10, 2-23Pump, 2-21Flow rate, 2-5Leaks, 4-10Operating pressure, A-2Over pressure alarm, 4-6Primary pump head, 2-21Priming, 3-9, B-36Priming problems, 4-11Secondary pump head, 2-22Troubleshooting, 4-13Under pressure alarm, 4-7Pump check valve leaking, 4-9Pump components, 2-21Pump degasSee Vacuum degas assemblyPump head waste valveLeaking, 4-10O-ring replacement procedure, 5-18Pump heads, 5-11Pump motor lost control alarm, 4-5Pump pressure hardware error, 4-6Pump priming valveO-ring replacement procedure, 5-18Pump specificationsFlow rate, A-2Operating pressure, A-2Type, A-2Index-6 Doc. 031879-01 3/03
IndexRRear panel, 2-7Analog output connector, 2-7Power receptacle, 2-8USB connections, 2-7Rebuilding the injection valve, 5-10Relay connectionsAS40, B-44Rear panel connector, 2-8, C-1Relay outputsControlling, C-5Voltage and current specifications, C-2Reordering information, D-1Reproducibility, 2-27ReservoirConnecting, 3-8Filling, 3-8Monitoring liquid level in, 3-8, B-35Storage on top cover, 2-3Restriction in liquid lines, 4-6, 5-7Retention timeAdjusting, E-1Moving, E-1Troubleshooting, 4-17Run time, 2-15Running samples, 3-18See also Processing samplesSSafety messages, 1-6Sample loop, 2-5, 2-24Changing, 5-9Injecting, 2-24Injection valve connections, 2-24, 5-10Loading, 2-24Reordering, D-1Sample processing, 3-2, 3-18 – 3-19Batch, 3-2, 3-19<strong>Manual</strong>, 3-2, 3-18With Chromeleon, 3-18 – 3-19SamplesCollecting and storing, 3-12Diluting, 3-13Filtering, 3-12Injecting, 3-14, 3-16Loading, 3-14Pretreating, 3-12Saving data, 3-19SchematicFlow, 2-9Seal replacement, 5-14, 5-16 – 5-17SelectivityTroubleshooting, 4-17Self-Regenerating Suppressor, 2-6See also SuppressorSeparation process, 1-3Separator column, 2-5, B-19Installation, B-20Sequence, 2-11Creating, 3-19Sequence Wizard, 3-19Serial number, B-16Server Configuration programAS50 configuration properties, B-18Starting, 3-4, B-13Timebase, B-15Server Monitor, B-6Service chase, 2-3, 2-6Service procedures, 5-12Check valve cleaning, 5-11 – 5-12Check valve replacement, 5-11Conductivity cell replacement, 5-20Fuse replacement, 5-30Injection valve rebuilding, 5-10Isolation of liquid lines restriction, 5-7Leak sensor replacement, 5-28Piston replacement, 5-17Piston seal replacement, 5-13Priming valve O-ring replacement, 5-18Rebuilding the injection valve, 5-10Replacing tubing and fittings, 5-9Suppressor replacement, 5-22Tubing and fittings replacement, 5-9Waste valve O-ring replacement, 5-18Doc. 031879-01 3/03Index-7
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ICS-1000 ION CHROMATOGRAPHY SYSTEMO
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Contents1 • Introduction1.1 Intro
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ICS-1000 Ion Chromatography System4
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ICS-1000 Ion Chromatography SystemB
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ICS-1000 Ion Chromatography SystemE
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ICS-1000 Ion Chromatography SystemA
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ICS-1000 Ion Chromatography System1
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ICS-1000 Ion Chromatography System1
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ICS-1000 Ion Chromatography System1
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ICS-1000 Ion Chromatography SystemI
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ICS-1000 Ion Chromatography System2
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ICS-1000 Ion Chromatography SystemS
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ICS-1000 Ion Chromatography SystemT
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ICS-1000 Ion Chromatography System
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2 • Features2.3.2 The ICS-1000 Co
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2 • FeaturesSystem Controls Overv
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2 • FeaturesInject ValveDisplays
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2 • Features2.4 System Component
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2 • Features2.4.2 Eluent ValveThe
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2 • FeaturesPressure TransducerFl
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2 • Featuressample loops in vario
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2 • Features2.4.6 SuppressorThe s
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3 • Operation and MaintenanceThis
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3 • Operation and Maintenance3.2
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3 • Operation and Maintenance3. I
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3 • Operation and Maintenance•
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3 • Operation and Maintenance3.5
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3 • Operation and Maintenance3.8
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3 • Operation and Maintenance3.9.
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3 • Operation and Maintenancestan
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3 • Operation and Maintenance3.10
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3 • Operation and Maintenancenew
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3 • Operation and Maintenance3.12
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4 • TroubleshootingThis chapter i
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4 • Troubleshooting4.1 Alarms and
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4 • TroubleshootingLOAD/INJECT VA
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4 • TroubleshootingPUMP UNDER PRE
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4 • TroubleshootingSUPPRESSOR STO
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4 • TroubleshootingMake sure the
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4 • Troubleshooting• Blockages
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4 • Troubleshooting4.6 Erratic Fl
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4 • Troubleshooting• Malfunctio
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4 • Troubleshooting• Cell out o
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4 • Troubleshootingb. Under Insta
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5•ServiceThis chapter describes I
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5•ServiceUse the Wellness Panel t
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5•ServiceAfter calibration, the c
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5•Service5.1.4 Calibrating the Va
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5•Service5.3 Replacing Tubing and
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5•Service5.5 Cleaning and Replaci
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5•Service5.6 Replacing a Pump Pis
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5•Service6. The piston does not c
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5•ServiceReinstalling the Head an
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5•ServiceValve KnobO-Ring(P/N 055
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5•Service5. Slide the new cell as
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5•Service11. Align the top of the
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5•Service9. Enter the column heat
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5•Service6. Pull the valve straig
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5•Service5.15 Priming with Isopro
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A • SpecificationsA.1 ElectricalM
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A • SpecificationsA.6 DetectorRan
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B • InstallationThis chapter prov
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Unpacking the ICS-1000 System3. Rem
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Installing ChromeleonB.3 Installing
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Installing the Chromeleon Software
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Connecting the ICS-1000 to the Chro
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Connecting the Power CordB.6 Connec
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Setting Up ChromeleonB.8 Setting Up
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Setting Up Chromeleon10. Click the
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Setting Up Chromeleon2. Select the
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Installing and Plumbing the Columns
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Installing and Plumbing the Columns
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Connecting the Waste LinesB.10 Conn
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Setting Up the Eluent ReservoirVERS
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Setting Up a Chromeleon Application
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Setting Up a Chromeleon Application
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- Page 159 and 160: Setting the Eluent LevelNOTEIf the
- Page 161 and 162: Priming the Pump3. Open the priming
- Page 163 and 164: Equilibrating the SystemB.15 Equili
- Page 165 and 166: Connecting an AS50 Autosampler (Opt
- Page 167 and 168: Connecting an AS50 Autosampler (Opt
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- Page 173 and 174: Pump Continuous Seal Wash Connectio
- Page 175 and 176: Manually Connecting to a Control Pa
- Page 177 and 178: Installation TroubleshootingB.23 In
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- Page 201 and 202: IndexAAir particulate samples, 3-12
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