ICS-1000 Ion Chromatography System Operator's Manual

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ICS-1000 Ion Chromatography System4.13 Baseline Noise or Drift . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-194.14 Vacuum Degas Assembly Does Not Run . . . . . . . . . . . . . . . . . . . . . . 4-205 • Service5.1 Diagnostic and Calibration Procedures . . . . . . . . . . . . . . . . . . . . . . . . 5-15.1.1 Chromeleon Wellness Panel Overview . . . . . . . . . . . . . . . . . . 5-25.1.2 Calibrating the Conductivity Cell . . . . . . . . . . . . . . . . . . . . . . 5-45.1.3 Calibrating the Flow Rate . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-65.1.4 Calibrating the Vacuum Degas Assembly . . . . . . . . . . . . . . . . 5-75.2 Isolating a Restriction in the Liquid Lines . . . . . . . . . . . . . . . . . . . . . . 5-75.3 Replacing Tubing and Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-95.4 Rebuilding the Injection Valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-105.5 Cleaning and Replacing the Pump Check Valves . . . . . . . . . . . . . . . 5-115.6 Replacing a Pump Piston Seal and Piston Rinse Seal . . . . . . . . . . . . 5-135.7 Replacing a Pump Piston . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-175.8 Replacing the Waste Valve or Priming Valve O-Ring . . . . . . . . . . . . 5-185.9 Replacing the Conductivity Cell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-205.10 Replacing the Suppressor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-225.11 Replacing the Column Heater . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-235.12 Replacing the Column Heater Heat Exchanger . . . . . . . . . . . . . . . . . 5-255.13 Replacing the Eluent Valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-265.14 Replacing the Leak Sensor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-285.15 Priming with Isopropyl Alcohol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-295.16 Changing Main Power Fuses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-30iv Doc. 031879-01 3/03
ContentsA • SpecificationsA.1 Electrical . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-1A.2 Physical . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-1A.3 Environmental . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-1A.4 Front Panel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-2A.5 Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-2A.6 Detector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-3A.7 Conductivity Cell with Heat Exchanger . . . . . . . . . . . . . . . . . . . . . . . A-3A.8 Injection Valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-3A.9 Vacuum Degas Assembly (Optional) . . . . . . . . . . . . . . . . . . . . . . . . . A-3A.10 Column Heater (Optional) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A-4B • InstallationB.1 Facility Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . B-1B.2 Unpacking the ICS-1000 System . . . . . . . . . . . . . . . . . . . . . . . . . . . . B-2B.2.1 Unpacking the Computer (North America only). . . . . . . . . . . B-4B.2.2 Unpacking the Computer (outside North America) . . . . . . . . B-4B.3 Installing Chromeleon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . B-5B.4 Installing the Chromeleon Software License . . . . . . . . . . . . . . . . . . . B-6B.5 Connecting the ICS-1000 to the Chromeleon PC . . . . . . . . . . . . . . . . B-9B.5.1 Connecting the ICS-1000 to the PC . . . . . . . . . . . . . . . . . . . . B-9B.5.2 Connecting Additional USB Devices . . . . . . . . . . . . . . . . . . B-10B.6 Connecting the Power Cord . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . B-11B.7 Turning On the ICS-1000 Power . . . . . . . . . . . . . . . . . . . . . . . . . . . . B-12Doc. 031879-01 3/03v
Page 1 and 2: ICS-1000 ION CHROMATOGRAPHY SYSTEMO
Page 3 and 4: Contents1 • Introduction1.1 Intro
Page 8 and 9: ICS-1000 Ion Chromatography SystemB
Page 10 and 11: ICS-1000 Ion Chromatography SystemE
Page 12 and 13: ICS-1000 Ion Chromatography SystemA
Page 14 and 15: ICS-1000 Ion Chromatography System1
Page 20 and 21: ICS-1000 Ion Chromatography SystemI
Page 24 and 25: ICS-1000 Ion Chromatography SystemS
Page 26 and 27: ICS-1000 Ion Chromatography SystemT
Page 28 and 29: ICS-1000 Ion Chromatography System
Page 31 and 32: 2 • Features2.3.2 The ICS-1000 Co
Page 33 and 34: 2 • FeaturesSystem Controls Overv
Page 35 and 36: 2 • FeaturesInject ValveDisplays
Page 37 and 38: 2 • Features2.4 System Component
Page 39 and 40: 2 • Features2.4.2 Eluent ValveThe
Page 41 and 42: 2 • FeaturesPressure TransducerFl
Page 43 and 44: 2 • Featuressample loops in vario
Page 45 and 46: 2 • Features2.4.6 SuppressorThe s
Page 47 and 48: 3 • Operation and MaintenanceThis
Page 49 and 50: 3 • Operation and Maintenance3.2
Page 51 and 52: 3 • Operation and Maintenance3. I
Page 53 and 54: 3 • Operation and Maintenance•
Page 55 and 56:
3 • Operation and Maintenance3.5
Page 57 and 58:
Page 59 and 60:
3 • Operation and Maintenance3.9.
Page 61 and 62:
3 • Operation and Maintenancestan
Page 63 and 64:
Page 65 and 66:
3 • Operation and Maintenancenew
Page 67 and 68:
Page 69 and 70:
4 • TroubleshootingThis chapter i
Page 71 and 72:
4 • Troubleshooting4.1 Alarms and
Page 73 and 74:
4 • TroubleshootingLOAD/INJECT VA
Page 75 and 76:
4 • TroubleshootingPUMP UNDER PRE
Page 77 and 78:
4 • TroubleshootingSUPPRESSOR STO
Page 79 and 80:
4 • TroubleshootingMake sure the
Page 81 and 82:
4 • Troubleshooting• Blockages
Page 83 and 84:
4 • Troubleshooting4.6 Erratic Fl
Page 85 and 86:
4 • Troubleshooting• Malfunctio
Page 87 and 88:
4 • Troubleshooting• Cell out o
Page 89 and 90:
4 • Troubleshootingb. Under Insta
Page 91 and 92:
5•ServiceThis chapter describes I
Page 93 and 94:
5•ServiceUse the Wellness Panel t
Page 95 and 96:
5•ServiceAfter calibration, the c
Page 97 and 98:
5•Service5.1.4 Calibrating the Va
Page 99 and 100:
5•Service5.3 Replacing Tubing and
Page 101 and 102:
5•Service5.5 Cleaning and Replaci
Page 103 and 104:
5•Service5.6 Replacing a Pump Pis
Page 105 and 106:
5•Service6. The piston does not c
Page 107 and 108:
5•ServiceReinstalling the Head an
Page 109 and 110:
5•ServiceValve KnobO-Ring(P/N 055
Page 111 and 112:
5•Service5. Slide the new cell as
Page 113 and 114:
5•Service11. Align the top of the
Page 115 and 116:
5•Service9. Enter the column heat
Page 117 and 118:
5•Service6. Pull the valve straig
Page 119 and 120:
5•Service5.15 Priming with Isopro
Page 121 and 122:
A • SpecificationsA.1 ElectricalM
Page 123 and 124:
A • SpecificationsA.6 DetectorRan
Page 125 and 126:
B • InstallationThis chapter prov
Page 127 and 128:
Unpacking the ICS-1000 System3. Rem
Page 129 and 130:
Installing ChromeleonB.3 Installing
Page 131 and 132:
Installing the Chromeleon Software
Page 133 and 134:
Connecting the ICS-1000 to the Chro
Page 135 and 136:
Connecting the Power CordB.6 Connec
Page 137 and 138:
Setting Up ChromeleonB.8 Setting Up
Page 139 and 140:
Setting Up Chromeleon10. Click the
Page 141 and 142:
Setting Up Chromeleon2. Select the
Page 143 and 144:
Installing and Plumbing the Columns
Page 145 and 146:
Installing and Plumbing the Columns
Page 147 and 148:
Connecting the Waste LinesB.10 Conn
Page 149 and 150:
Setting Up the Eluent ReservoirVERS
Page 151 and 152:
Setting Up a Chromeleon Application
Page 153 and 154:
Page 155 and 156:
Page 157 and 158:
Page 159 and 160:
Setting the Eluent LevelNOTEIf the
Page 161 and 162:
Priming the Pump3. Open the priming
Page 163 and 164:
Equilibrating the SystemB.15 Equili
Page 165 and 166:
Connecting an AS50 Autosampler (Opt
Page 167 and 168:
Connecting an AS50 Autosampler (Opt
Page 169 and 170:
Connecting an AS40 Automated Sample
Page 171 and 172:
Pressurizing the Eluent Reservoir (
Page 173 and 174:
Pump Continuous Seal Wash Connectio
Page 175 and 176:
Manually Connecting to a Control Pa
Page 177 and 178:
Installation TroubleshootingB.23 In
Page 179 and 180:
C • TTL and Relay ControlNOTEThe
Page 181 and 182:
C • TTL and Relay Controlc. Conne
Page 183 and 184:
C • TTL and Relay Control• Inve
Page 185 and 186:
C • TTL and Relay ControlC.3 Exam
Page 187 and 188:
C • TTL and Relay ControlEnable A
Page 189 and 190:
D • Reordering InformationPart Nu
Page 191 and 192:
E•FAQE.1 How do I hook up an auto
Page 193 and 194:
E•FAQE.12 How do I know when a co
Page 195 and 196:
F • GlossaryAnalytical ColumnSyno
Page 197 and 198:
F • Glossaryof relatively clean s
Page 199 and 200:
F • GlossarySiemens (S)Unit measu
Page 201 and 202:
IndexAAir particulate samples, 3-12
Page 203 and 204:
IndexData rise time, B-46Decibel le
Page 205 and 206:
IndexKKey code (Chromeleon), B-6LLe
Page 207 and 208:
IndexRRear panel, 2-7Analog output
Page 209 and 210:
IndexTTL outputsControlling, C-5Rea
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ICS-1000 Ion Chromatography System Operator's Manual

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