ICS-1000 Ion Chromatography System Operator's Manual

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ICS-1000 Ion Chromatography System• Eluent from the eluent reservoir flows first through the pump degasassembly (if it is installed) and then through the eluent valve to thepump. It is then pushed through the pressure transducer, which measuresthe system pressure.• From there, it is pushed through a pulse damper, which smooths minorpressure variations from the pump to minimize baseline noise. The eluent thenflows into the injection valve.• After sample is loaded into the sample loop and the injection valve istoggled to the Inject position, eluent passes through the sample loop.• If the optional column heater is installed, the eluent/sample mixture ispumped through the heat exchanger, which heats the mixture to the columnheater temperature.• The mixture then goes to the guard and separator columns and through thesuppressor.• From the suppressor, the mixture flows through the cell 11, where the analytesare detected. A digital signal is sent to Chromeleon software. Analog outputcan be collected simultaneously.• Finally, the mixture flows out of the cell and is recycled back into thesuppressor, where it is used as the water source for the regenerant chamber.Flow is then routed to waste. 122-10 Doc. 031879-01 3/03
2 • Features2.3 The Chromeleon InterfaceNOTEThis section provides a brief overview of theChromeleon interface. For details, refer to theChromeleon Help or user’s manual.Chromeleon software is used for remote control of ICS-1000 operation. Twomodes of software control are available: direct control and automated control.• With direct control, you select operating parameters and commands from theChromeleon menu bar, toolbars, and Control Panels. Direct controlcommands are executed as soon as they are entered. Section 2.3.2 describesthe commands available from the ICS-1000 Control Panels.• With automated control, you create a list of samples (a sequence) to beprocessed automatically. The sequence includes programs with commandsand parameters for controlling the ICS-1000, acquiring sample data, andproducing reports. Section 3.11.2 describes automatic sample processing.Doc. 031879-01 3/03 2-11
Page 1 and 2: ICS-1000 ION CHROMATOGRAPHY SYSTEMO
Page 3 and 4: Contents1 • Introduction1.1 Intro
Page 6 and 7: ICS-1000 Ion Chromatography System4
Page 8 and 9: ICS-1000 Ion Chromatography SystemB
Page 10 and 11: ICS-1000 Ion Chromatography SystemE
Page 12 and 13: ICS-1000 Ion Chromatography SystemA
Page 20 and 21: ICS-1000 Ion Chromatography SystemI
Page 24 and 25: ICS-1000 Ion Chromatography SystemS
Page 26 and 27: ICS-1000 Ion Chromatography SystemT
Page 31 and 32: 2 • Features2.3.2 The ICS-1000 Co
Page 33 and 34: 2 • FeaturesSystem Controls Overv
Page 35 and 36: 2 • FeaturesInject ValveDisplays
Page 37 and 38: 2 • Features2.4 System Component
Page 39 and 40: 2 • Features2.4.2 Eluent ValveThe
Page 41 and 42: 2 • FeaturesPressure TransducerFl
Page 43 and 44: 2 • Featuressample loops in vario
Page 45 and 46: 2 • Features2.4.6 SuppressorThe s
Page 47 and 48: 3 • Operation and MaintenanceThis
Page 49 and 50: 3 • Operation and Maintenance3.2
Page 51 and 52: 3 • Operation and Maintenance3. I
Page 53 and 54: 3 • Operation and Maintenance•
Page 59 and 60: 3 • Operation and Maintenance3.9.
Page 61 and 62: 3 • Operation and Maintenancestan
Page 65 and 66: 3 • Operation and Maintenancenew
Page 69 and 70: 4 • TroubleshootingThis chapter i
Page 71 and 72: 4 • Troubleshooting4.1 Alarms and
Page 73 and 74: 4 • TroubleshootingLOAD/INJECT VA
Page 75 and 76: 4 • TroubleshootingPUMP UNDER PRE
Page 77 and 78: 4 • TroubleshootingSUPPRESSOR STO
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4 • TroubleshootingMake sure the
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4 • Troubleshooting• Blockages
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4 • Troubleshooting4.6 Erratic Fl
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4 • Troubleshooting• Malfunctio
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4 • Troubleshooting• Cell out o
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4 • Troubleshootingb. Under Insta
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5•ServiceThis chapter describes I
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5•ServiceUse the Wellness Panel t
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5•ServiceAfter calibration, the c
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5•Service5.1.4 Calibrating the Va
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5•Service5.3 Replacing Tubing and
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5•Service5.5 Cleaning and Replaci
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5•Service5.6 Replacing a Pump Pis
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5•Service6. The piston does not c
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5•ServiceReinstalling the Head an
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5•ServiceValve KnobO-Ring(P/N 055
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5•Service5. Slide the new cell as
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5•Service11. Align the top of the
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5•Service9. Enter the column heat
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5•Service6. Pull the valve straig
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5•Service5.15 Priming with Isopro
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A • SpecificationsA.1 ElectricalM
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A • SpecificationsA.6 DetectorRan
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B • InstallationThis chapter prov
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Unpacking the ICS-1000 System3. Rem
Page 129 and 130:
Installing ChromeleonB.3 Installing
Page 131 and 132:
Installing the Chromeleon Software
Page 133 and 134:
Connecting the ICS-1000 to the Chro
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Connecting the Power CordB.6 Connec
Page 137 and 138:
Setting Up ChromeleonB.8 Setting Up
Page 139 and 140:
Setting Up Chromeleon10. Click the
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Setting Up Chromeleon2. Select the
Page 143 and 144:
Installing and Plumbing the Columns
Page 145 and 146:
Installing and Plumbing the Columns
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Connecting the Waste LinesB.10 Conn
Page 149 and 150:
Setting Up the Eluent ReservoirVERS
Page 151 and 152:
Setting Up a Chromeleon Application
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Page 155 and 156:
Page 157 and 158:
Page 159 and 160:
Setting the Eluent LevelNOTEIf the
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Priming the Pump3. Open the priming
Page 163 and 164:
Equilibrating the SystemB.15 Equili
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Connecting an AS50 Autosampler (Opt
Page 167 and 168:
Connecting an AS50 Autosampler (Opt
Page 169 and 170:
Connecting an AS40 Automated Sample
Page 171 and 172:
Pressurizing the Eluent Reservoir (
Page 173 and 174:
Pump Continuous Seal Wash Connectio
Page 175 and 176:
Manually Connecting to a Control Pa
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Installation TroubleshootingB.23 In
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C • TTL and Relay ControlNOTEThe
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C • TTL and Relay Controlc. Conne
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C • TTL and Relay Control• Inve
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C • TTL and Relay ControlC.3 Exam
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C • TTL and Relay ControlEnable A
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D • Reordering InformationPart Nu
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E•FAQE.1 How do I hook up an auto
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E•FAQE.12 How do I know when a co
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F • GlossaryAnalytical ColumnSyno
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F • Glossaryof relatively clean s
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F • GlossarySiemens (S)Unit measu
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IndexAAir particulate samples, 3-12
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IndexData rise time, B-46Decibel le
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IndexKKey code (Chromeleon), B-6LLe
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IndexRRear panel, 2-7Analog output
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IndexTTL outputsControlling, C-5Rea
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ICS-1000 Ion Chromatography System Operator's Manual

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