ICS-1000 Ion Chromatography System Operator's Manual

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ICS-1000 Ion Chromatography SystemSample Processing OverviewSamples can be run either manually (one at a time), or they can be grouped andrun automatically in batches. Figure 3-2 shows the typical steps for manual andbatch sample processing. Samples can be loaded into the sample loop with anautosampler or with a syringe through the injection port on the ICS-1000 frontdoor.Manual SampleProcessingUsing ChromeleonLoad the sampleBatch SampleProcessingUsing ChromeleonCreate a Sequence(Sequence Wizard)Start dataacquisitionAdd the Sequenceto the BatchAutozeroStart the BatchInject the sampleStop dataacquisition(Optional)Save the manualsequence dataFigure 3-2. Sample Processing Overview3-2 Doc. 031879-01 3/03
3 • Operation and Maintenance3.2 Power Up the SystemPowerSwitchPress the power switch on the ICS-1000 rear panel (see Figure 3-3) toturn on the system power. Table 3-2shows the ICS-1000 conditions atpower up.Also turn on the power to thecomputer and the autosampler (ifused).Figure 3-3. ICS-1000 Rear PanelFeaturePumpInjection valveCellSuppressorCell heaterColumn oven temperature(Optional)Power-Up ConditionOffLoad positionReading current valueOff*Set to the last value used. The default when theICS-1000 is turned on for the first time is 35 °C.Set to the last value used. The default when theICS-1000 is turned on for the first time is 30 °C.Table 3-2. ICS-1000 Power-Up Conditions* When you start the suppressor, the value used last is restored.Doc. 031879-01 3/03 3-3
Page 1 and 2: ICS-1000 ION CHROMATOGRAPHY SYSTEMO
Page 3 and 4: Contents1 • Introduction1.1 Intro
Page 6 and 7: ICS-1000 Ion Chromatography System4
Page 8 and 9: ICS-1000 Ion Chromatography SystemB
Page 10 and 11: ICS-1000 Ion Chromatography SystemE
Page 12 and 13: ICS-1000 Ion Chromatography SystemA
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Page 24 and 25: ICS-1000 Ion Chromatography SystemS
Page 26 and 27: ICS-1000 Ion Chromatography SystemT
Page 28 and 29: ICS-1000 Ion Chromatography System
Page 31 and 32: 2 • Features2.3.2 The ICS-1000 Co
Page 33 and 34: 2 • FeaturesSystem Controls Overv
Page 35 and 36: 2 • FeaturesInject ValveDisplays
Page 37 and 38: 2 • Features2.4 System Component
Page 39 and 40: 2 • Features2.4.2 Eluent ValveThe
Page 41 and 42: 2 • FeaturesPressure TransducerFl
Page 43 and 44: 2 • Featuressample loops in vario
Page 45 and 46: 2 • Features2.4.6 SuppressorThe s
Page 47: 3 • Operation and MaintenanceThis
Page 51 and 52: 3 • Operation and Maintenance3. I
Page 53 and 54: 3 • Operation and Maintenance•
Page 55 and 56: 3 • Operation and Maintenance3.5
Page 59 and 60: 3 • Operation and Maintenance3.9.
Page 61 and 62: 3 • Operation and Maintenancestan
Page 65 and 66: 3 • Operation and Maintenancenew
Page 69 and 70: 4 • TroubleshootingThis chapter i
Page 71 and 72: 4 • Troubleshooting4.1 Alarms and
Page 73 and 74: 4 • TroubleshootingLOAD/INJECT VA
Page 75 and 76: 4 • TroubleshootingPUMP UNDER PRE
Page 77 and 78: 4 • TroubleshootingSUPPRESSOR STO
Page 79 and 80: 4 • TroubleshootingMake sure the
Page 81 and 82: 4 • Troubleshooting• Blockages
Page 83 and 84: 4 • Troubleshooting4.6 Erratic Fl
Page 85 and 86: 4 • Troubleshooting• Malfunctio
Page 87 and 88: 4 • Troubleshooting• Cell out o
Page 89 and 90: 4 • Troubleshootingb. Under Insta
Page 91 and 92: 5•ServiceThis chapter describes I
Page 93 and 94: 5•ServiceUse the Wellness Panel t
Page 95 and 96: 5•ServiceAfter calibration, the c
Page 97 and 98: 5•Service5.1.4 Calibrating the Va
Page 99 and 100:
5•Service5.3 Replacing Tubing and
Page 101 and 102:
5•Service5.5 Cleaning and Replaci
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5•Service5.6 Replacing a Pump Pis
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5•Service6. The piston does not c
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5•ServiceReinstalling the Head an
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5•ServiceValve KnobO-Ring(P/N 055
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5•Service5. Slide the new cell as
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5•Service11. Align the top of the
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5•Service9. Enter the column heat
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5•Service6. Pull the valve straig
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5•Service5.15 Priming with Isopro
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A • SpecificationsA.1 ElectricalM
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A • SpecificationsA.6 DetectorRan
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B • InstallationThis chapter prov
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Unpacking the ICS-1000 System3. Rem
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Installing ChromeleonB.3 Installing
Page 131 and 132:
Installing the Chromeleon Software
Page 133 and 134:
Connecting the ICS-1000 to the Chro
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Connecting the Power CordB.6 Connec
Page 137 and 138:
Setting Up ChromeleonB.8 Setting Up
Page 139 and 140:
Setting Up Chromeleon10. Click the
Page 141 and 142:
Setting Up Chromeleon2. Select the
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Installing and Plumbing the Columns
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Installing and Plumbing the Columns
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Connecting the Waste LinesB.10 Conn
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Setting Up the Eluent ReservoirVERS
Page 151 and 152:
Setting Up a Chromeleon Application
Page 153 and 154:
Page 155 and 156:
Page 157 and 158:
Page 159 and 160:
Setting the Eluent LevelNOTEIf the
Page 161 and 162:
Priming the Pump3. Open the priming
Page 163 and 164:
Equilibrating the SystemB.15 Equili
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Connecting an AS50 Autosampler (Opt
Page 167 and 168:
Connecting an AS50 Autosampler (Opt
Page 169 and 170:
Connecting an AS40 Automated Sample
Page 171 and 172:
Pressurizing the Eluent Reservoir (
Page 173 and 174:
Pump Continuous Seal Wash Connectio
Page 175 and 176:
Manually Connecting to a Control Pa
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Installation TroubleshootingB.23 In
Page 179 and 180:
C • TTL and Relay ControlNOTEThe
Page 181 and 182:
C • TTL and Relay Controlc. Conne
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C • TTL and Relay Control• Inve
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C • TTL and Relay ControlC.3 Exam
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C • TTL and Relay ControlEnable A
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D • Reordering InformationPart Nu
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E•FAQE.1 How do I hook up an auto
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E•FAQE.12 How do I know when a co
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F • GlossaryAnalytical ColumnSyno
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F • Glossaryof relatively clean s
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F • GlossarySiemens (S)Unit measu
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IndexAAir particulate samples, 3-12
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IndexData rise time, B-46Decibel le
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IndexKKey code (Chromeleon), B-6LLe
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IndexRRear panel, 2-7Analog output
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IndexTTL outputsControlling, C-5Rea
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ICS-1000 Ion Chromatography System Operator's Manual

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