<strong>ICS</strong>-<strong>1000</strong> <strong>Ion</strong> <strong>Chromatography</strong> <strong>System</strong>Check valvesCleaning procedure, 5-11 – 5-12Replacement procedure, 5-11 – 5-12Chromatogram, 1-3Chromeleon, 2-11Adding devices to a timebase, B-16Alarm conditions, 4-3Browser, 2-12, 3-5Control Panel, 2-11, 3-18Creating a sequence, 3-19Degas options, 4-20Direct control, 2-11Error messages, 4-3Installation, B-5, B-13Interface, 2-11License installation, B-5 – B-6Menu, 2-11, 3-18Programs, 2-11, 2-15, 3-16 – 3-19Starting, 3-4, B-26<strong>System</strong> properties dialog box, B-16Timebase, 3-5Toolbars, 2-11, 3-18Verifying communication, B-35Wellness Panel, 5-1Chromeleon ServerStarting, 3-4, B-13Chromeleon Server Configuration programStarting, B-13Timebase, B-15Column heater, 2-5, 2-26Replacement procedure, 5-23Specifications, A-4Column heater alarmsColumn heater exceeds safe temperature,4-3Column heater open circuit, 4-3Column heater short circuit, 4-3Columns, 2-5Cleaning, E-3Contaminated, 4-17Damage from IPA, 5-29Installing, B-19Storing, E-2CommandsChromeleon, 2-11, 3-19, B-34Component panel, 2-4ComputerConnections, B-9Operating system requirements, B-5Unpacking, B-4ConductivityCauses of high conductivity, E-3Temperature effect, 2-27Conductivity cell, 2-6, 2-27Calibrating, 5-4Calibration constant, 5-21High cell output, 4-18Leaking, 4-10No response, 4-18Replacement procedure, 5-20Specifications, A-3Volume, 2-27Conductivity cell specificationsActive volume, A-3Cell body, A-3Electrodes, A-3Maximum pressure, A-3Contacting Dionex, 5-1ContaminationColumn, 4-16 – 4-17Eluents, 4-16Sample, 4-17Standard, 4-16Control Panel, 2-11, 2-13, 3-18<strong>System</strong> Panel, 2-13Wellness Panel, 2-13DDaily maintenance, 3-21DataBacking up, E-2Deleting, E-2Saving, 3-19Data acquisition, 3-18Data analysis description, 1-3Index-2 Doc. 031879-01 3/03
IndexData rise time, B-46Decibel level, A-1Degas tubing assemblySee Vacuum degas assemblyDegas calibration failed alarm, 4-4Degassing eluents, 2-19, 3-6Delay volume, A-2Detection description, 1-3Detector specificationsCell drive, A-3Linearity, A-3Range, A-3Temperature compensation, A-3Diagnostics, 5-1Dimensions, A-1DionexContacting, 5-1Direct control, 2-11Dongle, B-6Drip tray, 2-5DS6 Heated Conductivity CellSee Conductivity cellDuty cycle, 2-20EElectrical specificationsFuses, A-1Main power, A-1EluentAqueous, 3-21, 4-12Degassing, 2-19Delivery process, 1-2Filtering, 3-7Preparing, 3-6When to remake, E-2Eluent bottleSee Eluent reservoirEluent level, 3-8, B-35Eluent reservoirConnecting, 3-8, B-25Filling, 3-8Gas connection, B-47Monitoring liquid level in, 3-8, B-35Pressurization, B-48Storage on top cover, 2-3Eluent valve, 2-5Replacing, 5-26End-line filterSee Filter, end-lineEnvironmental specificationsHumidity, A-1Operating pressure, A-1Operating temperature, A-1Equilibration time, 3-11Error messages, 4-3 – 4-8Column heater exceeds safe temperature,4-3Column heater open circuit, 4-3Column heater short circuit, 4-3Degas calibration failed, 4-4Hardware not present, 4-4Leak sensor wet, 4-4Load/inject valve error, 4-5Option not installed, 4-5Pressure slope calibration error, 4-5Pump motor lost control, 4-5Pump over pressure, 4-6Pump pressure hardware error, 4-6Pump under pressure, 4-7Suppressor not connected, 4-8Suppressor over current, 4-7Suppressor over power, 4-8Suppressor stopped for zero flow rate, 4-8FFacility requirements, B-1Filter, end-lineBacterial contamination, 3-21, 4-12Dirty or clogged, 3-21, 4-12Installation, 3-7FittingsLeaking, 4-9Replacing, 5-9Requirements, 5-9Doc. 031879-01 3/03Index-3
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ICS-1000 ION CHROMATOGRAPHY SYSTEMO
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Contents1 • Introduction1.1 Intro
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ICS-1000 Ion Chromatography System4
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ICS-1000 Ion Chromatography SystemB
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ICS-1000 Ion Chromatography SystemE
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ICS-1000 Ion Chromatography SystemA
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ICS-1000 Ion Chromatography System1
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ICS-1000 Ion Chromatography System1
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ICS-1000 Ion Chromatography System1
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ICS-1000 Ion Chromatography SystemI
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ICS-1000 Ion Chromatography System2
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ICS-1000 Ion Chromatography SystemS
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ICS-1000 Ion Chromatography SystemT
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ICS-1000 Ion Chromatography System
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2 • Features2.3.2 The ICS-1000 Co
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2 • FeaturesSystem Controls Overv
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2 • FeaturesInject ValveDisplays
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2 • Features2.4 System Component
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2 • Features2.4.2 Eluent ValveThe
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2 • FeaturesPressure TransducerFl
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2 • Featuressample loops in vario
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2 • Features2.4.6 SuppressorThe s
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3 • Operation and MaintenanceThis
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3 • Operation and Maintenance3.2
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3 • Operation and Maintenance3. I
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3 • Operation and Maintenance•
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3 • Operation and Maintenance3.5
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3 • Operation and Maintenance3.8
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3 • Operation and Maintenance3.9.
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3 • Operation and Maintenancestan
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3 • Operation and Maintenance3.10
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3 • Operation and Maintenancenew
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3 • Operation and Maintenance3.12
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4 • TroubleshootingThis chapter i
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4 • Troubleshooting4.1 Alarms and
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4 • TroubleshootingLOAD/INJECT VA
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4 • TroubleshootingPUMP UNDER PRE
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4 • TroubleshootingSUPPRESSOR STO
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4 • TroubleshootingMake sure the
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4 • Troubleshooting• Blockages
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4 • Troubleshooting4.6 Erratic Fl
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4 • Troubleshooting• Malfunctio
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4 • Troubleshooting• Cell out o
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4 • Troubleshootingb. Under Insta
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5•ServiceThis chapter describes I
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5•ServiceUse the Wellness Panel t
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5•ServiceAfter calibration, the c
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5•Service5.1.4 Calibrating the Va
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5•Service5.3 Replacing Tubing and
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5•Service5.5 Cleaning and Replaci
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5•Service5.6 Replacing a Pump Pis
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5•Service6. The piston does not c
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5•ServiceReinstalling the Head an
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5•ServiceValve KnobO-Ring(P/N 055
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5•Service5. Slide the new cell as
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5•Service11. Align the top of the
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5•Service9. Enter the column heat
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5•Service6. Pull the valve straig
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5•Service5.15 Priming with Isopro
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A • SpecificationsA.1 ElectricalM
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A • SpecificationsA.6 DetectorRan
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B • InstallationThis chapter prov
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Unpacking the ICS-1000 System3. Rem
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Installing ChromeleonB.3 Installing
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Installing the Chromeleon Software
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Connecting the ICS-1000 to the Chro
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Connecting the Power CordB.6 Connec
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Setting Up ChromeleonB.8 Setting Up
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Setting Up Chromeleon10. Click the
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Setting Up Chromeleon2. Select the
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Installing and Plumbing the Columns
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Installing and Plumbing the Columns
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Connecting the Waste LinesB.10 Conn
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Setting Up the Eluent ReservoirVERS
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- Page 163 and 164: Equilibrating the SystemB.15 Equili
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- Page 173 and 174: Pump Continuous Seal Wash Connectio
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- Page 177 and 178: Installation TroubleshootingB.23 In
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