<strong>ICS</strong>-<strong>1000</strong> <strong>Ion</strong> <strong>Chromatography</strong> <strong>System</strong>Flow rate, 2-5, A-2Calibration, 5-6Troubleshooting, 4-14Flow schematic, 2-9FROM PCUSB connections, B-9Front panel, 2-1Specifications, A-2FusesReplacement procedure, 5-30Requirements, A-1GGas separator waste tube, B-23Gas sourceConnection, B-47Installation, B-47Pressure requirement, B-47Ghosting, 4-16Guard column, 2-5, B-19Installation, B-20HHardware not present error, 4-4HeaterColumn, 2-26High pressure alarm, 4-6High pressure limit, A-2Humidity limits, A-1IInjecting samples, 3-14Via autosampler, 3-16Via syringe, 3-15Via vacuum syringe, 3-16Injection port, 2-1Injecting via syringe, 3-15Injection valve, 2-5, 2-24Controlling with an AS50, B-43, C-9Leaking, 4-10Plumbing connections, 2-24Rebuilding, 5-10Specifications, A-3Troubleshooting, 4-5Installation, B-1 – B-53Adding devices to a timebase, B-16Analog output connection, C-9AS40 autosampler, B-44AS50 Autosampler, B-40Assigning devices to a timebase, B-15Assigning USB devices, B-14Chromeleon, B-5, B-13Columns, B-19Computer, B-4Eluent reservoir, B-25, B-48Equilibrating the system, B-39Gas separator waste tube, B-23Gas source, B-47Guard column, B-20Key code, B-8Operating system requirements, B-5Operational status verification, B-39PC connections, B-9Plumbing, B-25Power connection, B-11Priming, B-36 – B-38Separator column, B-20Software license, B-5 – B-6Stand-alone operation setup, C-7 – C-8Starting the <strong>ICS</strong>, B-12Suppressor, B-21TTL and relay connections, C-1 – C-2Unpacking, B-2USB connections, B-9 – B-10Waste lines, B-23Installation troubleshooting, B-53Inverted edge TTL input control, C-4Inverted pulse TTL input control, C-5<strong>Ion</strong> chromatographyOverview, 1-1<strong>Ion</strong> exchange, 1-3Isocratic delivery system, 1-2Isopropyl alcohol, 5-29Index-4 Doc. 031879-01 3/03
IndexKKey code (Chromeleon), B-6LLeak sensor, 2-5Leak sensor wet alarm, 4-4Replacement, 5-28LeaksCell, 4-10Fittings, 4-9Injection valve, 4-10Liquid, 4-9Pressure transducer, 4-10Pump check valve, 4-9Pump head, 4-10Pump head waste valve, 4-10Pump piston seal, 4-10Suppressor, 4-10LED, A-2License (Chromeleon), B-5 – B-6License server (Chromeleon), B-6Linearity requirements, A-3Liquid leaks, 4-9See also LeaksLoad/inject valve alarm, 4-5Loading samples, 3-14LoopSee Sample loopLow pressure limit, A-2MMain power receptacle, 2-8Maintenance, 3-21Daily, 3-21Ongoing, 3-21Weekly, 3-21Yearly, 3-22<strong>Manual</strong> sample processing, 3-2MicroMembrane Suppressor, 2-6See also SuppressorNNitrite in samples, 3-12Normal edge TTL input control, C-4Normal pulse TTL input control, C-4OOffsetting background conductivity, 3-11Operating features, 2-1Operating pressure, A-1Operating rangesCell heater, 2-6Column heater, 2-5Flow rate, 2-5Operating system requirements, B-5Operating temperature, A-1OperationEquilibration time, 3-11Overview, 3-1Priming, 3-9, 5-29, B-38Reservoir setup, 3-6Sample preparation, 3-12Sample processing, 3-2Setting operating conditions, 3-10Starting Chromeleon, 3-4<strong>System</strong> power-up, 3-3Operational status verification, 3-11Option not installed error, 4-5OvenSee Column heaterOverview, 1-4PPanelsChromeleon Control Panel, 2-11, 3-18Chromeleon Wellness Panel, 5-1Component panel, 2-4ParametersChromeleon operating commands, 2-11,3-19, B-34Doc. 031879-01 3/03Index-5
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ICS-1000 ION CHROMATOGRAPHY SYSTEMO
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Contents1 • Introduction1.1 Intro
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ICS-1000 Ion Chromatography System4
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ICS-1000 Ion Chromatography SystemB
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ICS-1000 Ion Chromatography SystemE
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ICS-1000 Ion Chromatography SystemA
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ICS-1000 Ion Chromatography System1
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ICS-1000 Ion Chromatography System1
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ICS-1000 Ion Chromatography System1
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ICS-1000 Ion Chromatography SystemI
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ICS-1000 Ion Chromatography System2
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ICS-1000 Ion Chromatography SystemS
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ICS-1000 Ion Chromatography SystemT
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ICS-1000 Ion Chromatography System
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2 • Features2.3.2 The ICS-1000 Co
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2 • FeaturesSystem Controls Overv
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2 • FeaturesInject ValveDisplays
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2 • Features2.4 System Component
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2 • Features2.4.2 Eluent ValveThe
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2 • FeaturesPressure TransducerFl
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2 • Featuressample loops in vario
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2 • Features2.4.6 SuppressorThe s
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3 • Operation and MaintenanceThis
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3 • Operation and Maintenance3.2
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3 • Operation and Maintenance3. I
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3 • Operation and Maintenance•
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3 • Operation and Maintenance3.5
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3 • Operation and Maintenance3.8
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3 • Operation and Maintenance3.9.
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3 • Operation and Maintenancestan
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3 • Operation and Maintenance3.10
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3 • Operation and Maintenancenew
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3 • Operation and Maintenance3.12
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4 • TroubleshootingThis chapter i
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4 • Troubleshooting4.1 Alarms and
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4 • TroubleshootingLOAD/INJECT VA
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4 • TroubleshootingPUMP UNDER PRE
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4 • TroubleshootingSUPPRESSOR STO
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4 • TroubleshootingMake sure the
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4 • Troubleshooting• Blockages
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4 • Troubleshooting4.6 Erratic Fl
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4 • Troubleshooting• Malfunctio
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4 • Troubleshooting• Cell out o
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4 • Troubleshootingb. Under Insta
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5•ServiceThis chapter describes I
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5•ServiceUse the Wellness Panel t
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5•ServiceAfter calibration, the c
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5•Service5.1.4 Calibrating the Va
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5•Service5.3 Replacing Tubing and
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5•Service5.5 Cleaning and Replaci
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5•Service5.6 Replacing a Pump Pis
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5•Service6. The piston does not c
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5•ServiceReinstalling the Head an
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5•ServiceValve KnobO-Ring(P/N 055
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5•Service5. Slide the new cell as
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5•Service11. Align the top of the
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5•Service9. Enter the column heat
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5•Service6. Pull the valve straig
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5•Service5.15 Priming with Isopro
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A • SpecificationsA.1 ElectricalM
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A • SpecificationsA.6 DetectorRan
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B • InstallationThis chapter prov
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Unpacking the ICS-1000 System3. Rem
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Installing ChromeleonB.3 Installing
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Installing the Chromeleon Software
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Connecting the ICS-1000 to the Chro
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Connecting the Power CordB.6 Connec
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Setting Up ChromeleonB.8 Setting Up
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Setting Up Chromeleon10. Click the
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Setting Up Chromeleon2. Select the
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Installing and Plumbing the Columns
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Installing and Plumbing the Columns
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Connecting the Waste LinesB.10 Conn
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Setting Up the Eluent ReservoirVERS
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Setting Up a Chromeleon Application
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- Page 157 and 158: Setting Up a Chromeleon Application
- Page 159 and 160: Setting the Eluent LevelNOTEIf the
- Page 161 and 162: Priming the Pump3. Open the priming
- Page 163 and 164: Equilibrating the SystemB.15 Equili
- Page 165 and 166: Connecting an AS50 Autosampler (Opt
- Page 167 and 168: Connecting an AS50 Autosampler (Opt
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- Page 173 and 174: Pump Continuous Seal Wash Connectio
- Page 175 and 176: Manually Connecting to a Control Pa
- Page 177 and 178: Installation TroubleshootingB.23 In
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- Page 201 and 202: IndexAAir particulate samples, 3-12
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