ICS-1000 Ion Chromatography System Operator's Manual

More documents

Recommendations

Info

ICS-1000 Ion Chromatography SystemDS6 Heated Conductivity Cell ComponentsThe cell front cover provides CELL IN and CELL OUT fittings forconnecting the cell to the suppressor (see Figure 2-4). The remaining cellcomponents are mounted behind the component panel. To replace, the cellremove the screws on the cell front cover and pull the entire cell assemblyout through the component panel. See Section 5.9 for cell replacementinstructions.2-28 Doc. 031879-01 3/03
3 • Operation and MaintenanceThis chapter describes routine operating and maintenance procedures for the ICS-1000 Ion Chromatography System.3.1 Operation OverviewFigure 3-1 illustrates the basic steps for routine operation of the ICS-1000.Power up the systemStart ChromeleonSet up the reservoirCheck allconnectionsPrime the pumpSet operatingconditionsEquilibrate thesystemPrepare samplesVerify operatingstatusProcess samplesFigure 3-1. ICS-1000 Operation Flow ChartDoc. 031879-01 3/03 3-1
Page 1 and 2: ICS-1000 ION CHROMATOGRAPHY SYSTEMO
Page 3 and 4: Contents1 • Introduction1.1 Intro
Page 6 and 7: ICS-1000 Ion Chromatography System4
Page 8 and 9: ICS-1000 Ion Chromatography SystemB
Page 10 and 11: ICS-1000 Ion Chromatography SystemE
Page 12 and 13: ICS-1000 Ion Chromatography SystemA
Page 20 and 21: ICS-1000 Ion Chromatography SystemI
Page 24 and 25: ICS-1000 Ion Chromatography SystemS
Page 26 and 27: ICS-1000 Ion Chromatography SystemT
Page 28 and 29: ICS-1000 Ion Chromatography System
Page 31 and 32: 2 • Features2.3.2 The ICS-1000 Co
Page 33 and 34: 2 • FeaturesSystem Controls Overv
Page 35 and 36: 2 • FeaturesInject ValveDisplays
Page 37 and 38: 2 • Features2.4 System Component
Page 39 and 40: 2 • Features2.4.2 Eluent ValveThe
Page 41 and 42: 2 • FeaturesPressure TransducerFl
Page 43 and 44: 2 • Featuressample loops in vario
Page 45: 2 • Features2.4.6 SuppressorThe s
Page 49 and 50: 3 • Operation and Maintenance3.2
Page 51 and 52: 3 • Operation and Maintenance3. I
Page 53 and 54: 3 • Operation and Maintenance•
Page 59 and 60: 3 • Operation and Maintenance3.9.
Page 61 and 62: 3 • Operation and Maintenancestan
Page 65 and 66: 3 • Operation and Maintenancenew
Page 69 and 70: 4 • TroubleshootingThis chapter i
Page 71 and 72: 4 • Troubleshooting4.1 Alarms and
Page 73 and 74: 4 • TroubleshootingLOAD/INJECT VA
Page 75 and 76: 4 • TroubleshootingPUMP UNDER PRE
Page 77 and 78: 4 • TroubleshootingSUPPRESSOR STO
Page 79 and 80: 4 • TroubleshootingMake sure the
Page 81 and 82: 4 • Troubleshooting• Blockages
Page 83 and 84: 4 • Troubleshooting4.6 Erratic Fl
Page 85 and 86: 4 • Troubleshooting• Malfunctio
Page 87 and 88: 4 • Troubleshooting• Cell out o
Page 89 and 90: 4 • Troubleshootingb. Under Insta
Page 91 and 92: 5•ServiceThis chapter describes I
Page 93 and 94: 5•ServiceUse the Wellness Panel t
Page 95 and 96: 5•ServiceAfter calibration, the c
Page 97 and 98:
5•Service5.1.4 Calibrating the Va
Page 99 and 100:
5•Service5.3 Replacing Tubing and
Page 101 and 102:
5•Service5.5 Cleaning and Replaci
Page 103 and 104:
5•Service5.6 Replacing a Pump Pis
Page 105 and 106:
5•Service6. The piston does not c
Page 107 and 108:
5•ServiceReinstalling the Head an
Page 109 and 110:
5•ServiceValve KnobO-Ring(P/N 055
Page 111 and 112:
5•Service5. Slide the new cell as
Page 113 and 114:
5•Service11. Align the top of the
Page 115 and 116:
5•Service9. Enter the column heat
Page 117 and 118:
5•Service6. Pull the valve straig
Page 119 and 120:
5•Service5.15 Priming with Isopro
Page 121 and 122:
A • SpecificationsA.1 ElectricalM
Page 123 and 124:
A • SpecificationsA.6 DetectorRan
Page 125 and 126:
B • InstallationThis chapter prov
Page 127 and 128:
Unpacking the ICS-1000 System3. Rem
Page 129 and 130:
Installing ChromeleonB.3 Installing
Page 131 and 132:
Installing the Chromeleon Software
Page 133 and 134:
Connecting the ICS-1000 to the Chro
Page 135 and 136:
Connecting the Power CordB.6 Connec
Page 137 and 138:
Setting Up ChromeleonB.8 Setting Up
Page 139 and 140:
Setting Up Chromeleon10. Click the
Page 141 and 142:
Setting Up Chromeleon2. Select the
Page 143 and 144:
Installing and Plumbing the Columns
Page 145 and 146:
Installing and Plumbing the Columns
Page 147 and 148:
Connecting the Waste LinesB.10 Conn
Page 149 and 150:
Setting Up the Eluent ReservoirVERS
Page 151 and 152:
Setting Up a Chromeleon Application
Page 153 and 154:
Page 155 and 156:
Page 157 and 158:
Page 159 and 160:
Setting the Eluent LevelNOTEIf the
Page 161 and 162:
Priming the Pump3. Open the priming
Page 163 and 164:
Equilibrating the SystemB.15 Equili
Page 165 and 166:
Connecting an AS50 Autosampler (Opt
Page 167 and 168:
Connecting an AS50 Autosampler (Opt
Page 169 and 170:
Connecting an AS40 Automated Sample
Page 171 and 172:
Pressurizing the Eluent Reservoir (
Page 173 and 174:
Pump Continuous Seal Wash Connectio
Page 175 and 176:
Manually Connecting to a Control Pa
Page 177 and 178:
Installation TroubleshootingB.23 In
Page 179 and 180:
C • TTL and Relay ControlNOTEThe
Page 181 and 182:
C • TTL and Relay Controlc. Conne
Page 183 and 184:
C • TTL and Relay Control• Inve
Page 185 and 186:
C • TTL and Relay ControlC.3 Exam
Page 187 and 188:
C • TTL and Relay ControlEnable A
Page 189 and 190:
D • Reordering InformationPart Nu
Page 191 and 192:
E•FAQE.1 How do I hook up an auto
Page 193 and 194:
E•FAQE.12 How do I know when a co
Page 195 and 196:
F • GlossaryAnalytical ColumnSyno
Page 197 and 198:
F • Glossaryof relatively clean s
Page 199 and 200:
F • GlossarySiemens (S)Unit measu
Page 201 and 202:
IndexAAir particulate samples, 3-12
Page 203 and 204:
IndexData rise time, B-46Decibel le
Page 205 and 206:
IndexKKey code (Chromeleon), B-6LLe
Page 207 and 208:
IndexRRear panel, 2-7Analog output
Page 209 and 210:
IndexTTL outputsControlling, C-5Rea
show all

ICS-1000 Ion Chromatography System Operator's Manual

Create successful ePaper yourself

Delete template?

Save as template?