ICS-1000 Ion Chromatography System Operator's Manual

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ICS-1000 Ion Chromatography System4. Unscrew the sixthumbscrews on thetop metal plate (seeFigure B-18) andremove the plate.5. Go on toSection B.9.2.Thumbscrew (6)Figure B-18. ICS-1000 Column Heater Cover RemovedB.9.2Installing the Columns1. Remove the union connecting GUARD IN and GUARD OUT.2. Connect GUARD IN to the guard column inlet. Check the arrow on thecolumn label; it should point down (flow away from the injectionvalve).3. Connect GUARD OUT to the guard column outlet.4. Push the guard column onto the back column clip.5. Remove the union connecting COL IN and COL OUT and6. Connect COL IN to the separator column inlet. Connect COL OUT tothe separator column outlet. Check the arrow on the column label. Itshould point up (flow toward the cell).7. Push the separator column onto the front column clips.8. Replace the top metal plate on the column heater (if installed).B-20 Doc. 031879-01 3/03
Installing and Plumbing the Columns and SuppressorB.9.3Installing the Suppressor1. Locate the suppressormounting tabs on thecomponent panel (seeFigure B-19). Reachinto the openingbetween the tabs andpull the yellowconnector and attachedcable slightly out of theopening.2. Connect this cable to thecable from thesuppressor (align thepins on the twoconnectors and pushthem together).4311 211 SuppressorMounting Tabs2 Suppressor CableConnector3 Guideline for AES4 Guideline for SRSFigure B-19. Suppressor Mounting Tabsand Guidelines3. Orient the suppressor with the REGEN OUT fitting on top and thecable to the right.4. Feed the cable into the opening in the component panel.5. Align the top of the suppressor with the guideline printed on thecomponent panel (see Figure B-19) and align the slots on the rear ofthe suppressor with the tabs on the panel.Doc. 031879-01 3/03 B-21
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ICS-1000 ION CHROMATOGRAPHY SYSTEMO
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Contents1 • Introduction1.1 Intro
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ICS-1000 Ion Chromatography System4
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ICS-1000 Ion Chromatography SystemB
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ICS-1000 Ion Chromatography SystemE
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ICS-1000 Ion Chromatography SystemA
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ICS-1000 Ion Chromatography SystemI
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ICS-1000 Ion Chromatography SystemS
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ICS-1000 Ion Chromatography SystemT
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ICS-1000 Ion Chromatography System
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2 • Features2.3.2 The ICS-1000 Co
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2 • FeaturesSystem Controls Overv
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2 • FeaturesInject ValveDisplays
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2 • Features2.4 System Component
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2 • Features2.4.2 Eluent ValveThe
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2 • FeaturesPressure TransducerFl
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2 • Featuressample loops in vario
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2 • Features2.4.6 SuppressorThe s
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3 • Operation and MaintenanceThis
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3 • Operation and Maintenance3.2
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3 • Operation and Maintenance3. I
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3 • Operation and Maintenance•
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3 • Operation and Maintenance3.9.
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3 • Operation and Maintenancestan
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3 • Operation and Maintenancenew
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4 • TroubleshootingThis chapter i
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4 • Troubleshooting4.1 Alarms and
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4 • TroubleshootingLOAD/INJECT VA
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4 • TroubleshootingPUMP UNDER PRE
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4 • TroubleshootingSUPPRESSOR STO
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4 • TroubleshootingMake sure the
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4 • Troubleshooting• Blockages
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4 • Troubleshooting4.6 Erratic Fl
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4 • Troubleshooting• Malfunctio
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4 • Troubleshooting• Cell out o
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4 • Troubleshootingb. Under Insta
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5•ServiceThis chapter describes I
Page 93 and 94: 5•ServiceUse the Wellness Panel t
Page 95 and 96: 5•ServiceAfter calibration, the c
Page 97 and 98: 5•Service5.1.4 Calibrating the Va
Page 99 and 100: 5•Service5.3 Replacing Tubing and
Page 101 and 102: 5•Service5.5 Cleaning and Replaci
Page 103 and 104: 5•Service5.6 Replacing a Pump Pis
Page 105 and 106: 5•Service6. The piston does not c
Page 107 and 108: 5•ServiceReinstalling the Head an
Page 109 and 110: 5•ServiceValve KnobO-Ring(P/N 055
Page 111 and 112: 5•Service5. Slide the new cell as
Page 113 and 114: 5•Service11. Align the top of the
Page 115 and 116: 5•Service9. Enter the column heat
Page 117 and 118: 5•Service6. Pull the valve straig
Page 119 and 120: 5•Service5.15 Priming with Isopro
Page 121 and 122: A • SpecificationsA.1 ElectricalM
Page 123 and 124: A • SpecificationsA.6 DetectorRan
Page 125 and 126: B • InstallationThis chapter prov
Page 127 and 128: Unpacking the ICS-1000 System3. Rem
Page 129 and 130: Installing ChromeleonB.3 Installing
Page 131 and 132: Installing the Chromeleon Software
Page 133 and 134: Connecting the ICS-1000 to the Chro
Page 135 and 136: Connecting the Power CordB.6 Connec
Page 137 and 138: Setting Up ChromeleonB.8 Setting Up
Page 139 and 140: Setting Up Chromeleon10. Click the
Page 141 and 142: Setting Up Chromeleon2. Select the
Page 143: Installing and Plumbing the Columns
Page 147 and 148: Connecting the Waste LinesB.10 Conn
Page 149 and 150: Setting Up the Eluent ReservoirVERS
Page 151 and 152: Setting Up a Chromeleon Application
Page 159 and 160: Setting the Eluent LevelNOTEIf the
Page 161 and 162: Priming the Pump3. Open the priming
Page 163 and 164: Equilibrating the SystemB.15 Equili
Page 165 and 166: Connecting an AS50 Autosampler (Opt
Page 167 and 168: Connecting an AS50 Autosampler (Opt
Page 169 and 170: Connecting an AS40 Automated Sample
Page 171 and 172: Pressurizing the Eluent Reservoir (
Page 173 and 174: Pump Continuous Seal Wash Connectio
Page 175 and 176: Manually Connecting to a Control Pa
Page 177 and 178: Installation TroubleshootingB.23 In
Page 179 and 180: C • TTL and Relay ControlNOTEThe
Page 181 and 182: C • TTL and Relay Controlc. Conne
Page 183 and 184: C • TTL and Relay Control• Inve
Page 185 and 186: C • TTL and Relay ControlC.3 Exam
Page 187 and 188: C • TTL and Relay ControlEnable A
Page 189 and 190: D • Reordering InformationPart Nu
Page 191 and 192: E•FAQE.1 How do I hook up an auto
Page 193 and 194: E•FAQE.12 How do I know when a co
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F • GlossaryAnalytical ColumnSyno
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F • Glossaryof relatively clean s
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F • GlossarySiemens (S)Unit measu
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IndexAAir particulate samples, 3-12
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IndexData rise time, B-46Decibel le
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IndexKKey code (Chromeleon), B-6LLe
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IndexRRear panel, 2-7Analog output
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IndexTTL outputsControlling, C-5Rea
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ICS-1000 Ion Chromatography System Operator's Manual

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