ICS-1000 Ion Chromatography System Operator's Manual

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ICS-1000 Ion Chromatography SystemB.8 Setting Up Chromeleon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-13B.8.1 Assigning the ICS-1000 to a Timebase . . . . . . . . . . . . . . . . .B-13B.8.2 Assigning DX-LAN Devices to the Timebase (Optional) . . .B-16B.9 Installing and Plumbing the Columns and Suppressor . . . . . . . . . . . .B-19B.9.1 Column Heater Setup (Optional) . . . . . . . . . . . . . . . . . . . . . .B-19B.9.2 Installing the Columns . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-20B.9.3 Installing the Suppressor . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-21B.10 Connecting the Waste Lines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-23B.10.1 Installing the Gas Separator Waste Tube . . . . . . . . . . . . . . . .B-23B.11 Setting Up the Eluent Reservoir . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-25B.12 Setting Up a Chromeleon Application . . . . . . . . . . . . . . . . . . . . . . . .B-26B.12.1 Verifying Chromeleon Communication. . . . . . . . . . . . . . . . .B-35B.13 Setting the Eluent Level . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-35B.14 Priming the Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-36B.14.1 Priming the Eluent Lines with a Syringe . . . . . . . . . . . . . . . .B-36B.14.2 Priming with the Prime Button. . . . . . . . . . . . . . . . . . . . . . . .B-38B.15 Equilibrating the System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-39B.16 Verifying Operational Status . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-39B.17 Connecting an AS50 Autosampler (Optional) . . . . . . . . . . . . . . . . . .B-40B.17.1 AS50 Configuration Requirements . . . . . . . . . . . . . . . . . . . .B-40B.17.2 AS50 Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .B-41B.17.3 Enable AS50 Control of the Injection Valve . . . . . . . . . . . . .B-43B.18 Connecting an AS40 Automated Sampler (Optional) . . . . . . . . . . . .B-44B.19 Analog Output Connection (Optional) . . . . . . . . . . . . . . . . . . . . . . . .B-46B.20 Pressurizing the Eluent Reservoir (Optional) . . . . . . . . . . . . . . . . . . .B-46vi Doc. 031879-01 3/03
ContentsB.20.1 Connecting the Gas Source (Optional) . . . . . . . . . . . . . . . . . B-47B.20.2 Pressurizing the Eluent Reservoir (Optional) . . . . . . . . . . . . B-48B.21 Pump Continuous Seal Wash Connections (Optional) . . . . . . . . . . . B-49B.22 Manually Connecting to a Control Panel . . . . . . . . . . . . . . . . . . . . . B-51B.23 Installation Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . B-53C • TTL and Relay ControlC.1 TTL and Relay Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . C-1C.1.1 Selecting TTL Input Functions and Control Types. . . . . . . . . C-3C.2 Controlling TTL and Relay Outputs . . . . . . . . . . . . . . . . . . . . . . . . . . C-5C.3 Example Setup for Stand-Alone Operation . . . . . . . . . . . . . . . . . . . . . C-7D • Reordering InformationE • FAQE.1 How do I hook up an autosampler? . . . . . . . . . . . . . . . . . . . . . . . . . . . E-1E.2 How do I print? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-1E.3 Why are the retention times moving? . . . . . . . . . . . . . . . . . . . . . . . . . E-1E.4 How do I adjust retention times? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-1E.5 When should I remake standards? . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-2E.6 When should I remake eluents? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-2E.7 How do I start Chromeleon? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-2E.8 How do I delete data? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-2E.9 How do I back up data? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . E-2Doc. 031879-01 3/03vii
Page 1 and 2: ICS-1000 ION CHROMATOGRAPHY SYSTEMO
Page 3 and 4: Contents1 • Introduction1.1 Intro
Page 6 and 7: ICS-1000 Ion Chromatography System4
Page 10 and 11: ICS-1000 Ion Chromatography SystemE
Page 12 and 13: ICS-1000 Ion Chromatography SystemA
Page 20 and 21: ICS-1000 Ion Chromatography SystemI
Page 24 and 25: ICS-1000 Ion Chromatography SystemS
Page 26 and 27: ICS-1000 Ion Chromatography SystemT
Page 28 and 29: ICS-1000 Ion Chromatography System
Page 31 and 32: 2 • Features2.3.2 The ICS-1000 Co
Page 33 and 34: 2 • FeaturesSystem Controls Overv
Page 35 and 36: 2 • FeaturesInject ValveDisplays
Page 37 and 38: 2 • Features2.4 System Component
Page 39 and 40: 2 • Features2.4.2 Eluent ValveThe
Page 41 and 42: 2 • FeaturesPressure TransducerFl
Page 43 and 44: 2 • Featuressample loops in vario
Page 45 and 46: 2 • Features2.4.6 SuppressorThe s
Page 47 and 48: 3 • Operation and MaintenanceThis
Page 49 and 50: 3 • Operation and Maintenance3.2
Page 51 and 52: 3 • Operation and Maintenance3. I
Page 53 and 54: 3 • Operation and Maintenance•
Page 59 and 60:
3 • Operation and Maintenance3.9.
Page 61 and 62:
3 • Operation and Maintenancestan
Page 63 and 64:
3 • Operation and Maintenance3.10
Page 65 and 66:
3 • Operation and Maintenancenew
Page 67 and 68:
3 • Operation and Maintenance3.12
Page 69 and 70:
4 • TroubleshootingThis chapter i
Page 71 and 72:
4 • Troubleshooting4.1 Alarms and
Page 73 and 74:
4 • TroubleshootingLOAD/INJECT VA
Page 75 and 76:
4 • TroubleshootingPUMP UNDER PRE
Page 77 and 78:
4 • TroubleshootingSUPPRESSOR STO
Page 79 and 80:
4 • TroubleshootingMake sure the
Page 81 and 82:
4 • Troubleshooting• Blockages
Page 83 and 84:
4 • Troubleshooting4.6 Erratic Fl
Page 85 and 86:
4 • Troubleshooting• Malfunctio
Page 87 and 88:
4 • Troubleshooting• Cell out o
Page 89 and 90:
4 • Troubleshootingb. Under Insta
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5•ServiceThis chapter describes I
Page 93 and 94:
5•ServiceUse the Wellness Panel t
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5•ServiceAfter calibration, the c
Page 97 and 98:
5•Service5.1.4 Calibrating the Va
Page 99 and 100:
5•Service5.3 Replacing Tubing and
Page 101 and 102:
5•Service5.5 Cleaning and Replaci
Page 103 and 104:
5•Service5.6 Replacing a Pump Pis
Page 105 and 106:
5•Service6. The piston does not c
Page 107 and 108:
5•ServiceReinstalling the Head an
Page 109 and 110:
5•ServiceValve KnobO-Ring(P/N 055
Page 111 and 112:
5•Service5. Slide the new cell as
Page 113 and 114:
5•Service11. Align the top of the
Page 115 and 116:
5•Service9. Enter the column heat
Page 117 and 118:
5•Service6. Pull the valve straig
Page 119 and 120:
5•Service5.15 Priming with Isopro
Page 121 and 122:
A • SpecificationsA.1 ElectricalM
Page 123 and 124:
A • SpecificationsA.6 DetectorRan
Page 125 and 126:
B • InstallationThis chapter prov
Page 127 and 128:
Unpacking the ICS-1000 System3. Rem
Page 129 and 130:
Installing ChromeleonB.3 Installing
Page 131 and 132:
Installing the Chromeleon Software
Page 133 and 134:
Connecting the ICS-1000 to the Chro
Page 135 and 136:
Connecting the Power CordB.6 Connec
Page 137 and 138:
Setting Up ChromeleonB.8 Setting Up
Page 139 and 140:
Setting Up Chromeleon10. Click the
Page 141 and 142:
Setting Up Chromeleon2. Select the
Page 143 and 144:
Installing and Plumbing the Columns
Page 145 and 146:
Installing and Plumbing the Columns
Page 147 and 148:
Connecting the Waste LinesB.10 Conn
Page 149 and 150:
Setting Up the Eluent ReservoirVERS
Page 151 and 152:
Setting Up a Chromeleon Application
Page 153 and 154:
Page 155 and 156:
Page 157 and 158:
Page 159 and 160:
Setting the Eluent LevelNOTEIf the
Page 161 and 162:
Priming the Pump3. Open the priming
Page 163 and 164:
Equilibrating the SystemB.15 Equili
Page 165 and 166:
Connecting an AS50 Autosampler (Opt
Page 167 and 168:
Connecting an AS50 Autosampler (Opt
Page 169 and 170:
Connecting an AS40 Automated Sample
Page 171 and 172:
Pressurizing the Eluent Reservoir (
Page 173 and 174:
Pump Continuous Seal Wash Connectio
Page 175 and 176:
Manually Connecting to a Control Pa
Page 177 and 178:
Installation TroubleshootingB.23 In
Page 179 and 180:
C • TTL and Relay ControlNOTEThe
Page 181 and 182:
C • TTL and Relay Controlc. Conne
Page 183 and 184:
C • TTL and Relay Control• Inve
Page 185 and 186:
C • TTL and Relay ControlC.3 Exam
Page 187 and 188:
C • TTL and Relay ControlEnable A
Page 189 and 190:
D • Reordering InformationPart Nu
Page 191 and 192:
E•FAQE.1 How do I hook up an auto
Page 193 and 194:
E•FAQE.12 How do I know when a co
Page 195 and 196:
F • GlossaryAnalytical ColumnSyno
Page 197 and 198:
F • Glossaryof relatively clean s
Page 199 and 200:
F • GlossarySiemens (S)Unit measu
Page 201 and 202:
IndexAAir particulate samples, 3-12
Page 203 and 204:
IndexData rise time, B-46Decibel le
Page 205 and 206:
IndexKKey code (Chromeleon), B-6LLe
Page 207 and 208:
IndexRRear panel, 2-7Analog output
Page 209 and 210:
IndexTTL outputsControlling, C-5Rea
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