ICS-1000 Ion Chromatography System Operator's Manual

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ICS-1000 Ion Chromatography SystemSuppressorThe suppressor reduces the eluent conductivity and enhances theconductivity of the sample ions, thereby increasing detection sensitivity.Either an AES® Atlas Electrolytic Suppressor, SRS® Self-RegeneratingSuppressor, or MMS MicroMembrane Suppressor can be used withthe ICS-1000. See Section 2.4.6 for details.DS6 Heated Conductivity CellThe flow-through conductivity cell measures the electrical conductanceof analyte ions as they pass through the cell. A heat exchanger inside thecell regulates the temperature, which can be set to between 30 °C and55 °C. For optimum performance, set the temperature to at least 7 °Cabove the ambient temperature. See Section 2.4.7 for details about thecell.Tubing ChasesThe upper tubing chase routes tubing from the top cover to the componentpanel. The lower tubing chase routes tubing from the component panelthrough the ICS-1000 interior to the rear panel.2-6 Doc. 031879-01 3/03
2 • Features2.1.4 Rear PanelFigure 2-5 illustrates the ICS-1000 rear panel.Tubing ClipsPowerSwitchAnalog OutputConnectorUSBConnectionsMain PowerReceptacleTTL and RelayConnector StripWaste LinesFigure 2-5. ICS-1000 Rear PanelAnalog Output ConnectorThe analog output connector outputs conductivity data (scaled to 1 volt)to an integrator or recording device. See Section B.19 for connection andsetup information.USB ConnectionsA USB receptacle is provided to allow connection to the Chromeleoncomputer. Two USB ports are provided for connecting to other USBdevices. See Section B.5 for connection instructions.Doc. 031879-01 3/03 2-7
Page 1 and 2: ICS-1000 ION CHROMATOGRAPHY SYSTEMO
Page 3 and 4: Contents1 • Introduction1.1 Intro
Page 6 and 7: ICS-1000 Ion Chromatography System4
Page 8 and 9: ICS-1000 Ion Chromatography SystemB
Page 10 and 11: ICS-1000 Ion Chromatography SystemE
Page 12 and 13: ICS-1000 Ion Chromatography SystemA
Page 20 and 21: ICS-1000 Ion Chromatography SystemI
Page 26 and 27: ICS-1000 Ion Chromatography SystemT
Page 28 and 29: ICS-1000 Ion Chromatography System
Page 31 and 32: 2 • Features2.3.2 The ICS-1000 Co
Page 33 and 34: 2 • FeaturesSystem Controls Overv
Page 35 and 36: 2 • FeaturesInject ValveDisplays
Page 37 and 38: 2 • Features2.4 System Component
Page 39 and 40: 2 • Features2.4.2 Eluent ValveThe
Page 41 and 42: 2 • FeaturesPressure TransducerFl
Page 43 and 44: 2 • Featuressample loops in vario
Page 45 and 46: 2 • Features2.4.6 SuppressorThe s
Page 47 and 48: 3 • Operation and MaintenanceThis
Page 49 and 50: 3 • Operation and Maintenance3.2
Page 51 and 52: 3 • Operation and Maintenance3. I
Page 53 and 54: 3 • Operation and Maintenance•
Page 59 and 60: 3 • Operation and Maintenance3.9.
Page 61 and 62: 3 • Operation and Maintenancestan
Page 65 and 66: 3 • Operation and Maintenancenew
Page 69 and 70: 4 • TroubleshootingThis chapter i
Page 71 and 72: 4 • Troubleshooting4.1 Alarms and
Page 73 and 74: 4 • TroubleshootingLOAD/INJECT VA
Page 75 and 76:
4 • TroubleshootingPUMP UNDER PRE
Page 77 and 78:
4 • TroubleshootingSUPPRESSOR STO
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4 • TroubleshootingMake sure the
Page 81 and 82:
4 • Troubleshooting• Blockages
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4 • Troubleshooting4.6 Erratic Fl
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4 • Troubleshooting• Malfunctio
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4 • Troubleshooting• Cell out o
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4 • Troubleshootingb. Under Insta
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5•ServiceThis chapter describes I
Page 93 and 94:
5•ServiceUse the Wellness Panel t
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5•ServiceAfter calibration, the c
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5•Service5.1.4 Calibrating the Va
Page 99 and 100:
5•Service5.3 Replacing Tubing and
Page 101 and 102:
5•Service5.5 Cleaning and Replaci
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5•Service5.6 Replacing a Pump Pis
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5•Service6. The piston does not c
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5•ServiceReinstalling the Head an
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5•ServiceValve KnobO-Ring(P/N 055
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5•Service5. Slide the new cell as
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5•Service11. Align the top of the
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5•Service9. Enter the column heat
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5•Service6. Pull the valve straig
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5•Service5.15 Priming with Isopro
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A • SpecificationsA.1 ElectricalM
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A • SpecificationsA.6 DetectorRan
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B • InstallationThis chapter prov
Page 127 and 128:
Unpacking the ICS-1000 System3. Rem
Page 129 and 130:
Installing ChromeleonB.3 Installing
Page 131 and 132:
Installing the Chromeleon Software
Page 133 and 134:
Connecting the ICS-1000 to the Chro
Page 135 and 136:
Connecting the Power CordB.6 Connec
Page 137 and 138:
Setting Up ChromeleonB.8 Setting Up
Page 139 and 140:
Setting Up Chromeleon10. Click the
Page 141 and 142:
Setting Up Chromeleon2. Select the
Page 143 and 144:
Installing and Plumbing the Columns
Page 145 and 146:
Installing and Plumbing the Columns
Page 147 and 148:
Connecting the Waste LinesB.10 Conn
Page 149 and 150:
Setting Up the Eluent ReservoirVERS
Page 151 and 152:
Setting Up a Chromeleon Application
Page 153 and 154:
Page 155 and 156:
Page 157 and 158:
Page 159 and 160:
Setting the Eluent LevelNOTEIf the
Page 161 and 162:
Priming the Pump3. Open the priming
Page 163 and 164:
Equilibrating the SystemB.15 Equili
Page 165 and 166:
Connecting an AS50 Autosampler (Opt
Page 167 and 168:
Connecting an AS50 Autosampler (Opt
Page 169 and 170:
Connecting an AS40 Automated Sample
Page 171 and 172:
Pressurizing the Eluent Reservoir (
Page 173 and 174:
Pump Continuous Seal Wash Connectio
Page 175 and 176:
Manually Connecting to a Control Pa
Page 177 and 178:
Installation TroubleshootingB.23 In
Page 179 and 180:
C • TTL and Relay ControlNOTEThe
Page 181 and 182:
C • TTL and Relay Controlc. Conne
Page 183 and 184:
C • TTL and Relay Control• Inve
Page 185 and 186:
C • TTL and Relay ControlC.3 Exam
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C • TTL and Relay ControlEnable A
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D • Reordering InformationPart Nu
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E•FAQE.1 How do I hook up an auto
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E•FAQE.12 How do I know when a co
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F • GlossaryAnalytical ColumnSyno
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F • Glossaryof relatively clean s
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F • GlossarySiemens (S)Unit measu
Page 201 and 202:
IndexAAir particulate samples, 3-12
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IndexData rise time, B-46Decibel le
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IndexKKey code (Chromeleon), B-6LLe
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IndexRRear panel, 2-7Analog output
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IndexTTL outputsControlling, C-5Rea
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ICS-1000 Ion Chromatography System Operator's Manual

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