ISQ User Guide - Write Frame of Mind

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Preface Power Ratings Power Ratings Contacting Us Mass Spectrometer (MS) • 100-240 V ac, 50/60 Hz, 15 A max Gas Chromatograph (GC) • 120 V ac +6%/-10%, 50/60 Hz, 20 A max • 230 V ac ±10%, 50/60 Hz, 10 A max The foreline pump must be set to the line voltage that will be used at your location. Detailed instrument specifications are in the Product Specification or Product Brochure. Note Always make sure that, in case of emergency, it is easy to disconnect the electrical cable of the system. There are several ways to contact Thermo Fisher Scientific. � To contact Technical Support Phone 800-532-4752 Fax 561-688-8736 E-mail US.Techsupport.Analyze@thermofisher.com Find software updates and utilities to download at http://mssupport.thermo.com. � To contact Customer Service for ordering information Phone 800-532-4752 Fax 561-688-8731 E-mail us.customer-support.analyze@thermofisher.com � To suggest changes to documentation or to Instrument Help • Fill out a reader survey online at www.thermo.com/lcms-techpubs. • Send an e-mail message to the Technical Publications Editor at techpubsaustin@thermofisher.com. x ISQ User Guide Thermo Scientific
Related Documentation Preface Related Documentation In addition to this guide, Thermo Scientific provides the following documents for the ISQ. These documents are also available on a “Print-By-Request” basis. ISQ Document Set, PN 1R120555 • ISQ Preinstallation Requirements Guide, PN 1R120555-0001 • ISQ Hardware Manual, PN 1R120555-0002 • ISQ User Guide, PN 1R120555-0003 • ISQ Spare Parts Guide, PN 1R120555-0004 Instrument Help is available from within the ISQ Autotune and Method Editor software. To suggest ways we can improve the documentation, use your browser to complete our documentation survey. Safety Alerts and Important Information Make sure you follow the precautionary notices presented in this guide. Safety and other special notices appear in boxes and include the following: WARNING This is the general warning safety symbol and safety alert word to prevent actions that could cause personal injury. It highlights hazards to humans or environment. Each WARNING safety alert is preceded with this safety symbol and another appropriate safety symbol (see Safety Symbols and Signal Words.) Then it is followed with an appropriate safety precautionary message. When you see a safety alert on your instrument or in the publications, please carefully follow the safety instructions before proceeding. CAUTION This is the safety alert word to prevent actions that may cause personal injury or instrument damage. We use it to highlight information necessary to prevent personal injury or damage to software, loss of data, or invalid test results; or might contain information that is critical for optimal system performance. A CAUTION safety alert is always preceded with an appropriate safety symbol (see Safety Symbols and Signal Words.) Then it is followed with an appropriate safety precautionary message. When you see a safety alert on your instrument or in the publications, please carefully follow the safety instructions before proceeding. IMPORTANT Highlights information necessary to prevent damage to software, loss of data, or invalid test results; or might contain information that is critical for optimal performance of the system. Note Emphasizes important information about a task. Tip Helpful information that can make a task easier. Thermo Scientific ISQ User Guide xi
Page 1 and 2: ISQ User Guide 1R120555-0003 Revisi
Page 3 and 4: Manufacturer: Thermo Fisher Scienti
Page 5 and 6: WEEE Compliance This product is req
Page 7 and 8: Contents Thermo Scientific ISQ User
Page 9: Preface About Your System This guid
Page 13 and 14: Hydrogen Safety Precautions Preface
Page 15 and 16: Hydrogen Connection Guidelines Use
Page 17 and 18: Properly Storing Hydrogen Preface H
Page 19 and 20: Preface Hydrogen Safety Precautions
Page 21 and 22: Changing the Column The ISQ ships w
Page 23 and 24: Replacing the Factory-Installed Col
Page 25 and 26: 15. Perform a column leak check. 1
Page 27 and 28: j. Repeat the leak check until no l
Page 29 and 30: i. The following message will indic
Page 31 and 32: 1 Changing the Column Replacing the
Page 33 and 34: Confirming Your GC/MS System is Wor
Page 35 and 36: Checking the Vacuum and Temperature
Page 37 and 38: Tuning the ISQ Tuning will improve
Page 39 and 40: 3 Tuning the ISQ Using ISQ Autotune
Page 41 and 42: 3 Tuning the ISQ Using ISQ Autotune
Page 43 and 44: 9. Click the Print Report button to
Page 45 and 46: 3 Tuning the ISQ Tuning the ISQ wit
Page 51 and 52: Creating a Method Once you’ve got
Page 53 and 54: . Configure the Pre-Injection group
Page 55 and 56: 4 Creating a Method b. Set the MS T
Page 57 and 58: 4 Creating a Method At 4 minutes in
Page 59 and 60: 4 Creating a Method • The Filamen
Page 61 and 62:
4 Creating a Method You can select
Page 63 and 64:
4 Creating a Method Finally, if you
Page 65 and 66:
If you have a FOCUS GC: 4 Creating
Page 67 and 68:
4 Creating a Method c. Click the Ca
Page 69 and 70:
4 Creating a Method 6. When you are
Page 71 and 72:
Running a Sample Preparing Your Sam
Page 73 and 74:
5 Running a Sample Running a Sequen
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Page 77 and 78:
Page 79 and 80:
Page 81 and 82:
Page 83 and 84:
e. Configure the Run Synchronously
Page 85 and 86:
Exploring Your Data Once you have a
Page 87 and 88:
6 Exploring Your Data 5. The chroma
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6 Exploring Your Data 8. Right-clic
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6 Exploring Your Data 12. In this s
Page 93 and 94:
6 Exploring Your Data The full scan
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Optimizing Your Method If you did n
Page 97 and 98:
Modifying an Automatic Tune 7 Optim
Page 99 and 100:
6. Configure the General tab. • N
Page 101 and 102:
7 Optimizing Your Method Modifying
Page 103 and 104:
Page 105 and 106:
Page 107 and 108:
Page 109 and 110:
Troubleshooting This section contai
Page 111 and 112:
Investigating Baseline Issues Table
Page 113 and 114:
Table 3. Troubleshooting Peak Issue
Page 115 and 116:
Table 3. Troubleshooting Peak Issue
Page 117 and 118:
Table 4. Troubleshooting Results Is
Page 119 and 120:
8 Troubleshooting Reconfiguring You
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Page 125 and 126:
16. Click the Done button to close
Page 127 and 128:
Index A acquisition methods, purpos
Page 129 and 130:
tune report, 22, 29 tune types addi
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