ISQ User Guide - Write Frame of Mind

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Conformité DEEE Ce produit doit être conforme à la directive européenne (2002/96/EC) des Déchets d'Equipements Electriques et Electroniques (DEEE). Il est marqué par le symbole suivant: Thermo Fisher Scientific s'est associé avec une ou plusieurs compagnies de recyclage dans chaque état membre de l’union européenne et ce produit devrait être collecté ou recyclé par celles-ci. Davantage d'informations sur la conformité de Thermo Fisher Scientific à ces directives, les recycleurs dans votre pays et les informations sur les produits Thermo Fisher Scientific qui peuvent aider la détection des substances sujettes à la directive RoHS sont disponibles sur www.thermo.com/WEEERoHS.
Contents Thermo Scientific ISQ User Guide vii C Preface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ix About Your System. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .ix Power Ratings. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . x Contacting Us . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . x Related Documentation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .xi Safety Alerts and Important Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .xi Hydrogen Safety Precautions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .xiii Chapter 1 Changing the Column . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Replacing the Factory-Installed Column . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Chapter 2 Confirming Your GC/MS System is Working . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13 Checking Power to the System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 Verifying the Carrier Gas Flow Rate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 Checking Your Carrier Gas Tank Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 Checking the Vacuum and Temperature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 Chapter 3 Tuning the ISQ . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17 Using ISQ Autotune . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18 Tuning the ISQ with Xcalibur. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24 Chapter 4 Creating a Method. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31 Chapter 5 Running a Sample . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51 Preparing Your Sample . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51 Running a Sequence . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52 Chapter 6 Exploring Your Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .65 Chapter 7 Optimizing Your Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .75 Changing the Chromatographic Separation. . . . . . . . . . . . . . . . . . . . . . . . . . . . 75 Finding the Best Way to Make an Injection . . . . . . . . . . . . . . . . . . . . . . . . . . . 75 Improving the Way You Prepare Samples . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76
Page 1 and 2: ISQ User Guide 1R120555-0003 Revisi
Page 3 and 4: Manufacturer: Thermo Fisher Scienti
Page 5: WEEE Compliance This product is req
Page 9 and 10: Preface About Your System This guid
Page 11 and 12: Related Documentation Preface Relat
Page 13 and 14: Hydrogen Safety Precautions Preface
Page 15 and 16: Hydrogen Connection Guidelines Use
Page 17 and 18: Properly Storing Hydrogen Preface H
Page 19 and 20: Preface Hydrogen Safety Precautions
Page 21 and 22: Changing the Column The ISQ ships w
Page 23 and 24: Replacing the Factory-Installed Col
Page 25 and 26: 15. Perform a column leak check. 1
Page 27 and 28: j. Repeat the leak check until no l
Page 29 and 30: i. The following message will indic
Page 31 and 32: 1 Changing the Column Replacing the
Page 33 and 34: Confirming Your GC/MS System is Wor
Page 35 and 36: Checking the Vacuum and Temperature
Page 37 and 38: Tuning the ISQ Tuning will improve
Page 39 and 40: 3 Tuning the ISQ Using ISQ Autotune
Page 41 and 42: 3 Tuning the ISQ Using ISQ Autotune
Page 43 and 44: 9. Click the Print Report button to
Page 45 and 46: 3 Tuning the ISQ Tuning the ISQ wit
Page 51 and 52: Creating a Method Once you’ve got
Page 53 and 54: . Configure the Pre-Injection group
Page 55 and 56: 4 Creating a Method b. Set the MS T
Page 57 and 58:
4 Creating a Method At 4 minutes in
Page 59 and 60:
4 Creating a Method • The Filamen
Page 61 and 62:
4 Creating a Method You can select
Page 63 and 64:
4 Creating a Method Finally, if you
Page 65 and 66:
If you have a FOCUS GC: 4 Creating
Page 67 and 68:
4 Creating a Method c. Click the Ca
Page 69 and 70:
4 Creating a Method 6. When you are
Page 71 and 72:
Running a Sample Preparing Your Sam
Page 73 and 74:
5 Running a Sample Running a Sequen
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Page 77 and 78:
Page 79 and 80:
Page 81 and 82:
Page 83 and 84:
e. Configure the Run Synchronously
Page 85 and 86:
Exploring Your Data Once you have a
Page 87 and 88:
6 Exploring Your Data 5. The chroma
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6 Exploring Your Data 8. Right-clic
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6 Exploring Your Data 12. In this s
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6 Exploring Your Data The full scan
Page 95 and 96:
Optimizing Your Method If you did n
Page 97 and 98:
Modifying an Automatic Tune 7 Optim
Page 99 and 100:
6. Configure the General tab. • N
Page 101 and 102:
7 Optimizing Your Method Modifying
Page 103 and 104:
Page 105 and 106:
Page 107 and 108:
Page 109 and 110:
Troubleshooting This section contai
Page 111 and 112:
Investigating Baseline Issues Table
Page 113 and 114:
Table 3. Troubleshooting Peak Issue
Page 115 and 116:
Table 3. Troubleshooting Peak Issue
Page 117 and 118:
Table 4. Troubleshooting Results Is
Page 119 and 120:
8 Troubleshooting Reconfiguring You
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Page 123 and 124:
Page 125 and 126:
16. Click the Done button to close
Page 127 and 128:
Index A acquisition methods, purpos
Page 129 and 130:
tune report, 22, 29 tune types addi
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