ISQ User Guide - Write Frame of Mind

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5 Running a Sample Running a Sequence 17. In the Run Sequence window, customize the way you want your sequence to run. a. Select the Start When Ready checkbox to run the sequence when the instruments are ready. b. Click the Change Instruments button and use the In Use and Start Instrument columns to define the instruments that are in use and the instrument that will define the start of the sequence. Then click the OK button. Note If you are making a manual injection, deselect the autosampler in the Start Instrument and In Use columns. Once you make the injection, press the Start button on the GC. c. In the Instrument Method group, you can browse to the sequence to be used when the instrument starts up or shuts down. d. In the Programs group, you can browse to the executables for Pre-Acquisition and Post-Acquisition. These fields are used to automatically run processing methods after the data acquisition is complete. Because you are developing your method, you haven’t defined a processing method for this field. 62 ISQ User Guide Thermo Scientific
e. Configure the Run Synchronously group: 5 Running a Sample Running a Sequence • Pre-Acquisition—Select this option to enable the executable to run before the data is acquired or deselect it to run the executable in parallel with data acquisition. • Post-Acquisition—Select this option to enable the executable to run after the data is acquired or deselect it to run the executable in parallel with data acquisition. f. Configure the After Sequence Set System group: • On—Select this option to leave the instrument fully ready after an acquisition. • Standby—Select this option to leave the instrument fully ready after an acquisition. • Off—Select this option to turn off the ISQ by turning off the heaters, turbo pump and foreline pump. g. In the User field, you can change your user name. The user name defaults to the name that was used to log into the computer. h. In the Run Rows field, enter the rows to be run in the sequence. Each value must be separated by a hyphen. i. Select the Priority Sequence checkbox if this sequence has priority over any other sequence. If someone else’s sequence is running in the background, this setting puts your sequence ahead of theirs. j. In the Processing Actions group, select Quan, Qual, Reports, Programs or Create Quan Summary. Since you are developing your method, you can skip this setting. Note The Reports checkbox is only enabled when you select the Qual checkbox. The Reports and Create Quan Summary checkboxes are only enabled when you select the Quan checkbox. 18. Click the OK button to run the sample or sequence. and store your data on the computer. Thermo Scientific ISQ User Guide 63
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ISQ User Guide 1R120555-0003 Revisi
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Manufacturer: Thermo Fisher Scienti
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WEEE Compliance This product is req
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Contents Thermo Scientific ISQ User
Page 9 and 10:
Preface About Your System This guid
Page 11 and 12:
Related Documentation Preface Relat
Page 13 and 14:
Hydrogen Safety Precautions Preface
Page 15 and 16:
Hydrogen Connection Guidelines Use
Page 17 and 18:
Properly Storing Hydrogen Preface H
Page 19 and 20:
Preface Hydrogen Safety Precautions
Page 21 and 22:
Changing the Column The ISQ ships w
Page 23 and 24:
Replacing the Factory-Installed Col
Page 25 and 26:
15. Perform a column leak check. 1
Page 27 and 28:
j. Repeat the leak check until no l
Page 29 and 30:
i. The following message will indic
Page 31 and 32: 1 Changing the Column Replacing the
Page 33 and 34: Confirming Your GC/MS System is Wor
Page 35 and 36: Checking the Vacuum and Temperature
Page 37 and 38: Tuning the ISQ Tuning will improve
Page 39 and 40: 3 Tuning the ISQ Using ISQ Autotune
Page 41 and 42: 3 Tuning the ISQ Using ISQ Autotune
Page 43 and 44: 9. Click the Print Report button to
Page 45 and 46: 3 Tuning the ISQ Tuning the ISQ wit
Page 51 and 52: Creating a Method Once you’ve got
Page 53 and 54: . Configure the Pre-Injection group
Page 55 and 56: 4 Creating a Method b. Set the MS T
Page 57 and 58: 4 Creating a Method At 4 minutes in
Page 59 and 60: 4 Creating a Method • The Filamen
Page 61 and 62: 4 Creating a Method You can select
Page 63 and 64: 4 Creating a Method Finally, if you
Page 65 and 66: If you have a FOCUS GC: 4 Creating
Page 67 and 68: 4 Creating a Method c. Click the Ca
Page 69 and 70: 4 Creating a Method 6. When you are
Page 71 and 72: Running a Sample Preparing Your Sam
Page 73 and 74: 5 Running a Sample Running a Sequen
Page 81: 5 Running a Sample Running a Sequen
Page 85 and 86: Exploring Your Data Once you have a
Page 87 and 88: 6 Exploring Your Data 5. The chroma
Page 89 and 90: 6 Exploring Your Data 8. Right-clic
Page 91 and 92: 6 Exploring Your Data 12. In this s
Page 93 and 94: 6 Exploring Your Data The full scan
Page 95 and 96: Optimizing Your Method If you did n
Page 97 and 98: Modifying an Automatic Tune 7 Optim
Page 99 and 100: 6. Configure the General tab. • N
Page 101 and 102: 7 Optimizing Your Method Modifying
Page 109 and 110: Troubleshooting This section contai
Page 111 and 112: Investigating Baseline Issues Table
Page 113 and 114: Table 3. Troubleshooting Peak Issue
Page 115 and 116: Table 3. Troubleshooting Peak Issue
Page 117 and 118: Table 4. Troubleshooting Results Is
Page 119 and 120: 8 Troubleshooting Reconfiguring You
Page 125 and 126: 16. Click the Done button to close
Page 127 and 128: Index A acquisition methods, purpos
Page 129 and 130: tune report, 22, 29 tune types addi
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ISQ User Guide - Write Frame of Mind

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