ISQ User Guide - Write Frame of Mind

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© 2010 Thermo Fisher Scientific Inc. All rights reserved. Xcalibur, ISQ, TRACE GC, TRACE GC Ultra, and FOCUS GC are trademarks and/or product names of Thermo Fisher Scientific. Microsoft® is a registered trademark of Microsoft. Adobe® is a registered trademark of Adobe Systems Incorporated in the United States and/or other countries. Septum BTO® is a registered trademark of Chromatography Research Supplies, Inc. TORX® is a registered trademark of Camcar LLC of Acument Global Technologies. Swagelok® is a registered trademark of Swagelok Company. ETP is an SGE product. All other trademarks are the property of Thermo Fisher Scientific and its subsidiaries. Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the product operation. This document is copyright protected and any reproduction of the whole or any part of this document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc. The contents of this document are subject to change without notice. All technical information in this document is for reference purposes only. System configurations and specifications in this document supersede all previous information received by the purchaser. Thermo Fisher Scientific Inc. makes no representations that this document is complete, accurate or errorfree and assumes no responsibility and will not be liable for any errors, omissions, damage or loss that might result from any use of this document, even if the information in the document is followed properly. This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser. This document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and Conditions of Sale shall govern all conflicting information between the two documents. Release history: Revision A, May 2010 For Research Use Only. Not for use in diagnostic procedures.
Manufacturer: Thermo Fisher Scientific Declaration Thermo Fisher Scientific is the manufacturer of the instrument described in this manual and, as such, is responsible for the instrument safety, reliability and performance only if: • installation • re-calibration • changes and repairs have been carried out by authorized personnel and if: • the local installation complies with local law regulations • the instrument is used according to the instructions provided and if its operation is only entrusted to qualified trained personnel Thermo Fisher Scientific is not liable for any damages derived from the non-compliance with the aforementioned recommendations. Regulatory Compliance Thermo Fisher Scientific performs complete testing and evaluation of its products to ensure full compliance with applicable domestic and international regulations. When the system is delivered to you, it meets all pertinent electromagnetic compatibility (EMC) and safety standards as described in the next section or sections by product name. Changes that you make to your system may void compliance with one or more of these EMC and safety standards. Changes to your system include replacing a part or adding components, options, or peripherals not specifically authorized and qualified by Thermo Fisher Scientific. To ensure continued compliance with EMC and safety standards, replacement parts and additional components, options, and peripherals must be ordered from Thermo Fisher Scientific or one of its authorized representatives. EMC Directive 89/336/EEC EMC compliance has been evaluated by Professional Testing. • Polaris Q, ITQ, and Ion Trap Series standards: EMC EN 61326-1:2006. Safety IEC 61010-1:2001, IEC 61010-2-081:2001 • DSQ II standards: EMC EN 61326-1:1997 + A1:1998 + A2:2001. Safety EN 61010-1:2001 • Direct Probe Controller (DPC) standards: EMC EN 61326-1:2006. Safety IEC 61010-1:2001, IEC 61010-2-081:2001 • ISQ standards: EMC EN 61326-1:2006. Safety IEC 61010-1:2001, IEC 61010-2-081:2001
Page 1: ISQ User Guide 1R120555-0003 Revisi
Page 5 and 6: WEEE Compliance This product is req
Page 7 and 8: Contents Thermo Scientific ISQ User
Page 9 and 10: Preface About Your System This guid
Page 11 and 12: Related Documentation Preface Relat
Page 13 and 14: Hydrogen Safety Precautions Preface
Page 15 and 16: Hydrogen Connection Guidelines Use
Page 17 and 18: Properly Storing Hydrogen Preface H
Page 19 and 20: Preface Hydrogen Safety Precautions
Page 21 and 22: Changing the Column The ISQ ships w
Page 23 and 24: Replacing the Factory-Installed Col
Page 25 and 26: 15. Perform a column leak check. 1
Page 27 and 28: j. Repeat the leak check until no l
Page 29 and 30: i. The following message will indic
Page 31 and 32: 1 Changing the Column Replacing the
Page 33 and 34: Confirming Your GC/MS System is Wor
Page 35 and 36: Checking the Vacuum and Temperature
Page 37 and 38: Tuning the ISQ Tuning will improve
Page 39 and 40: 3 Tuning the ISQ Using ISQ Autotune
Page 41 and 42: 3 Tuning the ISQ Using ISQ Autotune
Page 43 and 44: 9. Click the Print Report button to
Page 45 and 46: 3 Tuning the ISQ Tuning the ISQ wit
Page 51 and 52: Creating a Method Once you’ve got
Page 53 and 54:
. Configure the Pre-Injection group
Page 55 and 56:
4 Creating a Method b. Set the MS T
Page 57 and 58:
4 Creating a Method At 4 minutes in
Page 59 and 60:
4 Creating a Method • The Filamen
Page 61 and 62:
4 Creating a Method You can select
Page 63 and 64:
4 Creating a Method Finally, if you
Page 65 and 66:
If you have a FOCUS GC: 4 Creating
Page 67 and 68:
4 Creating a Method c. Click the Ca
Page 69 and 70:
4 Creating a Method 6. When you are
Page 71 and 72:
Running a Sample Preparing Your Sam
Page 73 and 74:
5 Running a Sample Running a Sequen
Page 75 and 76:
Page 77 and 78:
Page 79 and 80:
Page 81 and 82:
Page 83 and 84:
e. Configure the Run Synchronously
Page 85 and 86:
Exploring Your Data Once you have a
Page 87 and 88:
6 Exploring Your Data 5. The chroma
Page 89 and 90:
6 Exploring Your Data 8. Right-clic
Page 91 and 92:
6 Exploring Your Data 12. In this s
Page 93 and 94:
6 Exploring Your Data The full scan
Page 95 and 96:
Optimizing Your Method If you did n
Page 97 and 98:
Modifying an Automatic Tune 7 Optim
Page 99 and 100:
6. Configure the General tab. • N
Page 101 and 102:
7 Optimizing Your Method Modifying
Page 103 and 104:
Page 105 and 106:
Page 107 and 108:
Page 109 and 110:
Troubleshooting This section contai
Page 111 and 112:
Investigating Baseline Issues Table
Page 113 and 114:
Table 3. Troubleshooting Peak Issue
Page 115 and 116:
Table 3. Troubleshooting Peak Issue
Page 117 and 118:
Table 4. Troubleshooting Results Is
Page 119 and 120:
8 Troubleshooting Reconfiguring You
Page 121 and 122:
Page 123 and 124:
Page 125 and 126:
16. Click the Done button to close
Page 127 and 128:
Index A acquisition methods, purpos
Page 129 and 130:
tune report, 22, 29 tune types addi
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