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Specimen Label: Date: Ullage: inehes Height of Polymer Matrix: inches ist Hole 2nd Hole 3rd Hole 4th Hole 5th Hole 6th Hole Bottom Hole Total Free Liquid Collected Record additional observations on reserve WHC-SD-W100-TI-003 Rev. 0 PRESENCE OF FREE LIQUID DATA SHEET Liauid Volume (mis) Technician Technician Engineering Stock Eauioment Comoam, C-42 PROCEDURr 90ll0-0 Date Date Date Pace -2L of 37 ;
^-..., 3•0 ASSAY FOR MEI'ALS 3.1 INSTRUMENTATION WHC-SD-W100-TI-003 Rev. 0 PROCEDURE 90110-0 The method chosen for the quantitive determination of cobalt, cesium, and strontium is atomic absorption spearophotometry. An Inmumentation Laboratories Video 11 -pItoMlleter^ Model Number 07570. Serial Number 1207, will be used for all assay work. 7-e approprim itotlow--eathode lamps to be used a.... - Cobalt Cat. No. 62928-02 Cesium Cat. No. 62823 Strontium Cat. No. 62835 3.2 MLTHODS DESCRIPTION The methods used to atomize the samples will be either flame or flameless. The flameless method involves aspirating the sample into a graphite furnace buvette, which is electrically heated to the temperature required for atomization. Due to the nature of the samples to be tested, it is not possible to provide a step-by-step procedure for the assay of these samples. However, the following procedure will be adhered to for all assays. - ^â- ----- --- - ---- - _ + + + The ,K. a.^.a ...., ,..,,. ^rtê.r_ ..._ .L,.1enraHon iahnratnries --- --- Methods Manual for flame and flameless operations will be used whenever possible. 3A calibration curve of each metal of interest, in each matrix (D.L water or sea .vACer), will be prepared. Thesc calibration curves will be replicated as often as netestary -- --- -- gw^ Any chemical ,estnx modifiers (ie+ ammonium ttitnte) used in the assay will be identified and recorded on the Atomic Absorption Data Sheet. 3.2.4 The element, matrix, wavelength, bandwidth, deposition time and background correction will be recorded on the Atomic Absorption Data Sheet. 3.25 Any dilution required to bring the absorbance of a metal specie into the detection range of the instrument will be recorded. All dilutions will be volumetric dilutions. 3.16 The method of atomization, flame or tlameless, will be recorded. 3.2.7 Any modifications to the Instrumentation Laboratories methods used will be recorded. - 3: .8 The Atomic Absorption Data Sheet will be kept in the separate binder. Each ^ data sheet will be photocopies and stored in the Ouality Assurance vault. a"{ - Stock Eouioment Company C-43 Page 30 of .47
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R 2.1 199^ ^.EN GINEERING DATA TRAN
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Date Received% • I INFORMATION RE
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. SUPPORTING DOCUMENT 1. Total Page
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WHC-SD-W100-TI-003 Rev. 0 EXECUTIVE
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WHC-SD-W100-TI-003 Rev. 0 been achi
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__ _ _ MHC-SIL-yJ3,00-TI-D03 Rev. 0
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F`= WHC-SD-W100-TI-003 Rev. 0 DESCR
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WHC-SD-W100-TI-003 Rev. 0 LIST OF T
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WHC-SD-W100-TI-003 Rev. 0 WASTE REC
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WHC-SD-W100-TI-003 Rev. 0 1.2.1 Fee
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^s. WHC-SD-W100-TI-003 Rev. 0 conta
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__-'°'2 WHC-SD-W100-TI-003 Rev. 0
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2.1 REGULATORY FRAMEWORK WHC-SD-W10
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^..." ;_:.. :.^ .^.y^ WHC-SD-W100-T
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WHC-SD-W100-TI-003 Rev. 0 which the
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kIHC-Sû-Wi"v"u-Ti-u03 Rev. V ,--,,
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WHC-SD-W100-TI-003 Rev. 0 Type 1 wa
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3.3 TESTING APPROACH WHC-SD-W100-TI
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^.: fi WNC-SD-W100-TI-003 Rev. 0 Fi
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4.1 SCREENING TEST RESULTS WHC-SD-W
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,^. ----- -- WHC-SD-W100-TI-003 Rev
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WHC-SD-W100-TI-003 Rev. 0 4.1.3 The
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p Sam le Compressive Radiation stre
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WHC-SD-W100-TI-003 Rev. 0 Table 4-3
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..., TESTING RESULTS .^.CSSD-W-1OO-
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A I w ^^',; ^^ ;J ?1Fasf^.}: "q -?
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;..;: .^:. WHC-SD-W100-TI-003 Rev.
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--- ....ti s..` WHC-SD-WI00-TI-003
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1.0 INTRODUCTION WHC-SD-W100-TI-003
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WHC-SD-W100-TI-003 Rev. 0 Waste For
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^-: -- ^ Component Waste Type 1 LET
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.^x. --1vHC-SD iii00- T i-003 Rev.
Page 65 and 66: WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
Page 67 and 68: ,..^ c:-- z ,.E ^=t ^^ln^l WHC-SD-W
Page 69 and 70: Scope WHC-SD-W100-TI-003 Rev. 0 Sup
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Page 73 and 74: WHC-SD-W100-TI-003 Rev. 0 Laborator
Page 75 and 76: WHC-SD-WIOO-TI-003 Rev. 0 APPENDIX
Page 77 and 78: 16490 Chiaccothe Itoad Chagrin Fall
Page 79 and 80: ca-. tY•^_E Q . - - StoGkE4uip+!n
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Page 85 and 86: Stock E quipment Company A Unit of
Page 87 and 88: G' ,.,. d,_ s WHC-0-W100-TI-003 Rev
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Page 91 and 92: -. LeachantSolution: Specimen Diame
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Page 95 and 96: ..... lry" - Stock E a uipment Comp
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Page 101 and 102: Date: _ Leachability Time Point Lea
Page 103 and 104: 23 Ninety ( 90) Day Immersion Test
Page 105 and 106: ty ,.. ='`F r...,, b Ly.. Specimen
Page 107 and 108: 25 BIODEGRADATION TEST PROCEDURE St
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Page 123 and 124: WHC-SD-W100-TI-003 Rev. 0 APPENDIX
Page 125 and 126: WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
Page 127 and 128: 19 SCOPE AND APPLICATION WHC-SD-W10
Page 129 and 130: L:^3 ll Q. 4 AA :'ILTEP.S WHC-0-W10
Page 131 and 132: 4_T tJrD o,...Ys j ^,.,. WHC-SD-W10
Page 133 and 134: WHC-SD-W100-TI-003 Rev. 0 -, Proced
Page 135 and 136: WHC-SD-W100-TI-003 Rev. 0 Procedure
Page 137 and 138: (FM WHC-SD-W100-TI-003 Rev. 0 Proce
Page 139 and 140: C... 6 Wet Waste Sample Contains no
Page 141 and 142: ^..., . ,.y^ h:.r WHC-SD-WI00-Ti-00
Page 143 and 144: :. WHC-SD-W100-TI-003 Rev. 0 TA3i.E
Page 145 and 146: ^' . WHC-SD-W100-T1-003 Rev. 0 TABL
Page 147 and 148: ^- ^-> ^ C^Jl I I^t ^.: l WHC-St]-W
Page 149 and 150: c. 03 00 r=3 ^t C^' II 6.0 II Calib
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Page 153 and 154: R: C=1 rIj s^ ^ ^.. WHC-SD-YlI00-TI
Page 155 and 156: .,,_..1 ---^ - - i-•_E ?*^^ Mater
Page 157 and 158: WHC-SD-W100-TI-003 Rev. 0 Dow Chemi
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Page 163 and 164: t;7_7 ,...:: ----------- WHC-SD-W10
Page 165 and 166: WHC-SD-W100-TI-003 Rev. 0 Daw M.. u
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^ ^..rYfl VF •UIYb 1 1 AGA GllS.
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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CHARACTERIZATION DATA Part A: Overv
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Grit Specie or MaterialOverall Cont
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WHC-SD-W100-TI-003 Rev. 0 The incin
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WHC-SD-W100-TI-003 Rev. 0 183-H BAS
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WHC-SD-W100-TI-003 Rev. 0 June - Se
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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^- WHC-SD-W100-TI-003 Rev. 0 BASIN
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WHC-SD-W100-TI-003 Rev. 0 ---------
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J. L. Westcott Page 3 June 1, 1992
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u...^^, WHC-SD-W100-TI-003 Rev. 0 I
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•N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
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CONTAINER /NFORMATlO N: `d"-C-Sn-'w
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ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
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LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
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LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
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.:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
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LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
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PHYSICAL DESCR/PTTON: V-r-S?-W100-T
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,.: Westinoause Harlford COMM WHC-S
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O I tA SHEETII.XLS ;, LOT WRAP2A.2
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CONTAINER /NFORMAT/ON: DOSE: SIZE:
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PU33-11-1992 09:48 FROM EDS/qRI$ir
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LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
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qN i: 105N-89-1097 105N-89-1098 105
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SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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WHC-SD-W100-TI-003 Rev. 0 Westtngho
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LOT WRAP A2.14 SHEET 18.XLS RECOMME
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---- - LOT WRAP ZA.13 SHEET 17.XLS
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n .-.^..-n..^^- .. ... .dJ. ^ ShIEE
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--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
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WHC-SD-W100-TI-003 Rev. 0 Westingho
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Table 1 Candidate Waste Forms Absor
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--- -Aauaspt and Pe-liroset WHC-SD-
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- '^ - qev. r' Literature Search WR
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Dow Polymer WHC-SD-W100-TI-003 Rev.
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L im e Literature Search WRAP 2A Pa
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The report compares the 7eachabilit
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J. L. Westcott Page 2 May 29, 1992
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Package #1: Package #2: WHC-SD-W100
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WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
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f ..;' WHC-SD-W100-TI-003 Rev. 0 A
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 Bibliogra
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WHC-SD-W100-TI-003 Rev. 0 A. P. Tos
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OAK R1DGE NATIONAL LABORATORY OPERA
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 A report
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WHC-SD-W100-TI-003 Rev. 0 impermeab
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WHC-SD-W100-TI-003 Rev. 0 reprocess
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WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
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Contained under four reports: WHC-S
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^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
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WHC-SD-W100-TI-003 Rev. 0 The techn
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loomi^^lC& 111111111111F .^^.\ West
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û9^c ?fi. ...^ .._-, WHC-SD-W100-T
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Stock Equipment Company WHC-SD-WI00
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^ i w STOCK EOUIPMENT COMPANY 14-OC
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\. . 1 .: lh,lf^ LEACH / IMMERSIONI
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^;- v.4'? Sampls ID L781 Elsment CO
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4.a
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Sanp)a ID L781 Elamant STRONTIUM Ma
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.^ "-; SampI81D L3B2 Z e"- ^.;;. Sa
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Sample 10 L3B1 Elsmant CESIUM Matri
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Sample ID W B1 Elemant STRONIIUM Ma
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Westinghouse Hanford Company 2355 S
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--- - ftCR-e4Uip1P1eFf Company WHC-
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WHC-SD-W100-TI-003 Rev. 0 Russ Czel
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Stock Equipment Company 3:0 -SCFIED
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THERMAL CYCLING SAMPLES BEFORE THE
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BIODEGRADATION SAMPLES BEFORE THE S
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C/ 0D OC M1 0, ^yII i..) d tl ^ a I
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T 1 A w ^ • $ ^py yf ; pp V ^ py
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en a-. p g aQ i ^ rr it - l r rF e^
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' iO`F*'P\^ Westinghouse Hanford Co
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Stock Equipment Company 1.0 SUMMARY
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Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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T 1 OI 80 70 U 60 VJ w 50 w 0 40 30
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^ °' cn l .:. U CD w a: w r' i ^ I
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SAMPLE ID Li-117 L1-118 L1-19 L3-17
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O > W C f.) O O 1-- ^ O HI 6./ 3 ^
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0 > ar oe M 0 c C3, I O c V 3 Î d
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TI V 40 IN s i s : s ^l l i " p p l
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 _QVrDvrru
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^-_- .,:... WHC-SD-W100-TI-003 Rev.
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Ceramics and glass WHC-SD-W200-TI-0
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,. ., Extruder/melter WHC-SD-W100-T
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