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WHC-SD-W100-TI-003 Rev. 0 Waste Form Qualification Testing Statement of Work W-277587 May 14, 1992 will be used to mitigate safety hazards. Material safety data sheets for all process reagents shall be submitted with the work plan. 9.0 QUALITY ASSURANCE The contractor shall prepare a quality assurance plan describing the QA/QC activities to be performed during the work. WHC shall review and approve the QA plan prior to the start of testing. The plan shall include, but not be limited to, descriptions of laboratory instrument and equipment calibration, analysis of duplicates and blanks, and statistical validity of analytical results. All reported results shall be fully traceable to the original data sources. The testing laboratory shall follow QA/QC procedures that conform to d•'-. the requirements of the testing methods in Table 3. 10.0 SCHEDULE The schedule for performance of this work is shown in Figure 1. The --^_--- ----iAntraCtiSi"-s-ifiail--suf"im-it the-iv0rk plan and quality assurance plan within two weeks after award of contract. WHC review and approval of these documents will require one week. The contractor shall submit interim progress reports - on the work at four week intervals following approval of the work plan and release to proceed. The second progress report should contain the results of all laboratory testing with the exception of the long-term immersion, biodegradation, and leachability testing. Work shall be completed by October 16, with submittal of the final report no later than October 30, 1992. A-6
^-: -- ^ Component Waste Type 1 LETF Salts WHC-SD-W100-TI-003 Reve 0 Waste Form Qualification Testing Statement of Work W-277587 May 14, 1992 TABLE 1 Surrogate Wastes Approximate Composition Waste Type 2 Basins #1,#2 Sludge Waste Type 3 Basins #3,#4 Sludge Silver (ppm) M 190 Waste Type 4 Basin Crystal Solids Barium (pp m ) 24 100 Ber llium m 6 2.3 Cadmium (ppm ) 6 Chromium (pp m ) 187.5 900 390 500 Co pp er (pp m ) 201.0 130,000 112,000 63,000 Mercury (pp m ) 9.2 1.3 Nickel (oom)_ 46.5 100 130 400 SUBTOTAL Ippml 444.20 131,225.30 112,742.30 84,000.00 Ammonium % 22.83 Fluoride % 6.0 1.3 7.1 Nitrate % 1.1 13.5 26 1.6 Sodium ( % ) 20.0 24 22.9 Sulfate_ %) 64.61 __20.2 _3,7 35.5 Water ( % ) 10.0 21.58 25.03 24.5 SUBTOTAL I%) 98.54 81.28 80.03 91.60 Inerts % 1.42 5.6 8.7 2.0 TOTAL 1%1 100.00 100.00 100.00 100.00 A-1
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R 2.1 199^ ^.EN GINEERING DATA TRAN
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Date Received% • I INFORMATION RE
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. SUPPORTING DOCUMENT 1. Total Page
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WHC-SD-W100-TI-003 Rev. 0 EXECUTIVE
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Page 11 and 12: __ _ _ MHC-SIL-yJ3,00-TI-D03 Rev. 0
Page 13 and 14: F`= WHC-SD-W100-TI-003 Rev. 0 DESCR
Page 15 and 16: WHC-SD-W100-TI-003 Rev. 0 LIST OF T
Page 17 and 18: WHC-SD-W100-TI-003 Rev. 0 WASTE REC
Page 19 and 20: WHC-SD-W100-TI-003 Rev. 0 1.2.1 Fee
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Page 25 and 26: 2.1 REGULATORY FRAMEWORK WHC-SD-W10
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Page 35 and 36: 3.3 TESTING APPROACH WHC-SD-W100-TI
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Page 39 and 40: 4.1 SCREENING TEST RESULTS WHC-SD-W
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Page 47 and 48: WHC-SD-W100-TI-003 Rev. 0 Table 4-3
Page 49 and 50: ..., TESTING RESULTS .^.CSSD-W-1OO-
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Page 57 and 58: 1.0 INTRODUCTION WHC-SD-W100-TI-003
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Page 65 and 66: WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
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Page 69 and 70: Scope WHC-SD-W100-TI-003 Rev. 0 Sup
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Page 73 and 74: WHC-SD-W100-TI-003 Rev. 0 Laborator
Page 75 and 76: WHC-SD-WIOO-TI-003 Rev. 0 APPENDIX
Page 77 and 78: 16490 Chiaccothe Itoad Chagrin Fall
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Page 91 and 92: -. LeachantSolution: Specimen Diame
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Page 101 and 102: Date: _ Leachability Time Point Lea
Page 103 and 104: 23 Ninety ( 90) Day Immersion Test
Page 105 and 106: ty ,.. ='`F r...,, b Ly.. Specimen
Page 107 and 108: 25 BIODEGRADATION TEST PROCEDURE St
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^_... ..^^ C:i1 Date: WHC-SD-W100-T
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Date: WHC-SD-W100-TI-003 Rev. 0 --
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f-^ -- WHC-SD-W100-TI-003 Rev. 0 2.
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^-..., 3•0 ASSAY FOR MEI'ALS 3.1
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
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19 SCOPE AND APPLICATION WHC-SD-W10
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L:^3 ll Q. 4 AA :'ILTEP.S WHC-0-W10
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4_T tJrD o,...Ys j ^,.,. WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 -, Proced
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WHC-SD-W100-TI-003 Rev. 0 Procedure
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(FM WHC-SD-W100-TI-003 Rev. 0 Proce
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C... 6 Wet Waste Sample Contains no
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^..., . ,.y^ h:.r WHC-SD-WI00-Ti-00
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:. WHC-SD-W100-TI-003 Rev. 0 TA3i.E
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^' . WHC-SD-W100-T1-003 Rev. 0 TABL
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^- ^-> ^ C^Jl I I^t ^.: l WHC-St]-W
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c. 03 00 r=3 ^t C^' II 6.0 II Calib
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.,,_..1 ---^ - - i-•_E ?*^^ Mater
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WHC-SD-W100-TI-003 Rev. 0 Dow Chemi
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WHC-S®-hi1.00-T'.-00?, Rev. Dow Ch
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WHC-SD-W100-TI-003 Rev. 0 Daw M.. u
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^ ^..rYfl VF •UIYb 1 1 AGA GllS.
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CHARACTERIZATION DATA Part A: Overv
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Grit Specie or MaterialOverall Cont
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WHC-SD-W100-TI-003 Rev. 0 The incin
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WHC-SD-W100-TI-003 Rev. 0 183-H BAS
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WHC-SD-W100-TI-003 Rev. 0 June - Se
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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^- WHC-SD-W100-TI-003 Rev. 0 BASIN
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WHC-SD-W100-TI-003 Rev. 0 ---------
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J. L. Westcott Page 3 June 1, 1992
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u...^^, WHC-SD-W100-TI-003 Rev. 0 I
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•N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
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CONTAINER /NFORMATlO N: `d"-C-Sn-'w
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ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
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LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
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LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
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.:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
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LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
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PHYSICAL DESCR/PTTON: V-r-S?-W100-T
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,.: Westinoause Harlford COMM WHC-S
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O I tA SHEETII.XLS ;, LOT WRAP2A.2
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CONTAINER /NFORMAT/ON: DOSE: SIZE:
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PU33-11-1992 09:48 FROM EDS/qRI$ir
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LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
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qN i: 105N-89-1097 105N-89-1098 105
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SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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WHC-SD-W100-TI-003 Rev. 0 Westtngho
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LOT WRAP A2.14 SHEET 18.XLS RECOMME
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---- - LOT WRAP ZA.13 SHEET 17.XLS
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n .-.^..-n..^^- .. ... .dJ. ^ ShIEE
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--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
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WHC-SD-W100-TI-003 Rev. 0 Westingho
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Table 1 Candidate Waste Forms Absor
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--- -Aauaspt and Pe-liroset WHC-SD-
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- '^ - qev. r' Literature Search WR
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Dow Polymer WHC-SD-W100-TI-003 Rev.
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L im e Literature Search WRAP 2A Pa
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The report compares the 7eachabilit
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J. L. Westcott Page 2 May 29, 1992
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Package #1: Package #2: WHC-SD-W100
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WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
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f ..;' WHC-SD-W100-TI-003 Rev. 0 A
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 Bibliogra
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WHC-SD-W100-TI-003 Rev. 0 A. P. Tos
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OAK R1DGE NATIONAL LABORATORY OPERA
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 A report
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WHC-SD-W100-TI-003 Rev. 0 impermeab
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WHC-SD-W100-TI-003 Rev. 0 reprocess
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WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
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Contained under four reports: WHC-S
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^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
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WHC-SD-W100-TI-003 Rev. 0 The techn
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loomi^^lC& 111111111111F .^^.\ West
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Stock Equipment Company WHC-SD-WI00
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^ i w STOCK EOUIPMENT COMPANY 14-OC
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\. . 1 .: lh,lf^ LEACH / IMMERSIONI
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Sanp)a ID L781 Elamant STRONTIUM Ma
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Sample 10 L3B1 Elsmant CESIUM Matri
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Sample ID W B1 Elemant STRONIIUM Ma
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Westinghouse Hanford Company 2355 S
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--- - ftCR-e4Uip1P1eFf Company WHC-
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WHC-SD-W100-TI-003 Rev. 0 Russ Czel
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Stock Equipment Company 3:0 -SCFIED
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THERMAL CYCLING SAMPLES BEFORE THE
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BIODEGRADATION SAMPLES BEFORE THE S
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Stock Equipment Company 1.0 SUMMARY
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Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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WHC-SD-W100-TI-003 Rev. 0 _QVrDvrru
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Ceramics and glass WHC-SD-W200-TI-0
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,. ., Extruder/melter WHC-SD-W100-T
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