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,,.. ZA TESTING PROCEDURES WHC-SD-W100-TI-003 Rev. 0 2.1 COMPRESSIVE STRENGTH TEST PROCEDURE PROCEDURE 90110-0 This test will be performed as per ASTM D695 (Appendix A) for those samples requiring compressive strength testing. 2.1.1 Laboratory standard samples shall be chosen at random from the laboratory standard lot and compression tested. The compressive strength test data shall be recorded on the Compression Strength Data Sheet at the end of this section. The average compressive strength and density shall be calculated and recorded. One standard deviation value for the compressive strength and density will also be calculated and recorded on the Compressive Strength Data Sheets at the end of this section. 2.1.2 Prior to beginning the day's compressive strength testing, at least three (3) random samples from the laboratory standard lot shall be compression tested and ----reC3rded-orrthe-COmpresstve-.citr'cnoth Data Sheets at the end of this section. 2.13 For each sample to be tested, the height, diameter, and mass will be determined and recorded on the Compressive Strength Data Sheet at the end of this section. 2.1.4 The samples will be compressed individually using a Detroit testing machine -(Lfodel NTS•1,-number 836)-to-detarnrnethe-tttaximuiztoad.-irrpounds; applied to the specimen. As the compressive strength tests shall be performed throughout the program, the Detroit testing machine shall be calibrated by. -a- sertified calibration technician or by the Stock laboratory technician using a calibration ring. 2.1.5 The compressive strength of each sample will be calculated by the formula. C.S. - load (D2)2>< where C.S. = Compressive Strength, PSI load - maximum load applied, in pounds D = diameter of sample in inches 2.1.6 The density of each sample tested will be calculated by the equation. p = „J(d")Zha wh_e_re p = dcnsitv. Jcc m = mass. h = hei.-Iht. cm -^^--- ^ --- ^ - d = diameter, rm Stock EG lLpment Company A Unit of General Signal =vi* 5a9e•50-9ie6 of 7 ^ ,Y
Stock E quipment Company A Unit of General Signal Fa.n "98•50A1e6 WHC-SD-W100-TI-003 Rev. 0 PROCEDURE 90110-0 2.1.7 The following information will be entered onto the Compressive Strength Data Sheet at the end of this section. a. Specimen Label b. Diameter of Sample, inches/cm c. Height of Sample, cm d. Mass of Sample, g e. Maximum Load Applied, lbs f. Calculated Comoressive Strenath, psi g Densi.., g;w 2.1.8 The average compressive strength and density will be calculated and recorded for each waste form solidification. One (1) standard deviation value will also be calculated and recorded for the compressive strength and density of each waste form solidification. 4 C_l I Page ? of^
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R 2.1 199^ ^.EN GINEERING DATA TRAN
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Date Received% • I INFORMATION RE
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. SUPPORTING DOCUMENT 1. Total Page
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WHC-SD-W100-TI-003 Rev. 0 EXECUTIVE
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WHC-SD-W100-TI-003 Rev. 0 been achi
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__ _ _ MHC-SIL-yJ3,00-TI-D03 Rev. 0
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F`= WHC-SD-W100-TI-003 Rev. 0 DESCR
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WHC-SD-W100-TI-003 Rev. 0 LIST OF T
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WHC-SD-W100-TI-003 Rev. 0 WASTE REC
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WHC-SD-W100-TI-003 Rev. 0 1.2.1 Fee
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^s. WHC-SD-W100-TI-003 Rev. 0 conta
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__-'°'2 WHC-SD-W100-TI-003 Rev. 0
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2.1 REGULATORY FRAMEWORK WHC-SD-W10
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^..." ;_:.. :.^ .^.y^ WHC-SD-W100-T
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WHC-SD-W100-TI-003 Rev. 0 which the
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kIHC-Sû-Wi"v"u-Ti-u03 Rev. V ,--,,
Page 33 and 34: WHC-SD-W100-TI-003 Rev. 0 Type 1 wa
Page 35 and 36: 3.3 TESTING APPROACH WHC-SD-W100-TI
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Page 39 and 40: 4.1 SCREENING TEST RESULTS WHC-SD-W
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Page 43 and 44: WHC-SD-W100-TI-003 Rev. 0 4.1.3 The
Page 45 and 46: p Sam le Compressive Radiation stre
Page 47 and 48: WHC-SD-W100-TI-003 Rev. 0 Table 4-3
Page 49 and 50: ..., TESTING RESULTS .^.CSSD-W-1OO-
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Page 53 and 54: ;..;: .^:. WHC-SD-W100-TI-003 Rev.
Page 55 and 56: --- ....ti s..` WHC-SD-WI00-TI-003
Page 57 and 58: 1.0 INTRODUCTION WHC-SD-W100-TI-003
Page 59 and 60: WHC-SD-W100-TI-003 Rev. 0 Waste For
Page 61 and 62: ^-: -- ^ Component Waste Type 1 LET
Page 63 and 64: .^x. --1vHC-SD iii00- T i-003 Rev.
Page 65 and 66: WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
Page 67 and 68: ,..^ c:-- z ,.E ^=t ^^ln^l WHC-SD-W
Page 69 and 70: Scope WHC-SD-W100-TI-003 Rev. 0 Sup
Page 71 and 72: 00 V F-' Activity and Miltstone Cha
Page 73 and 74: WHC-SD-W100-TI-003 Rev. 0 Laborator
Page 75 and 76: WHC-SD-WIOO-TI-003 Rev. 0 APPENDIX
Page 77 and 78: 16490 Chiaccothe Itoad Chagrin Fall
Page 79 and 80: ca-. tY•^_E Q . - - StoGkE4uip+!n
Page 81 and 82: ^.. WHC-SD-W100-TI-003 Rev. 0 . , I
Page 83: Waste Type: WHC-SD-W100-TI-003 Rev.
Page 87 and 88: G' ,.,. d,_ s WHC-0-W100-TI-003 Rev
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Page 91 and 92: -. LeachantSolution: Specimen Diame
Page 93 and 94: c^1, WHC-SD-W100-TI-003 Rev. 0 THER
Page 95 and 96: ..... lry" - Stock E a uipment Comp
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Page 99 and 100: (.7 ..^^ -„n f^. [Y^. Waste Type:
Page 101 and 102: Date: _ Leachability Time Point Lea
Page 103 and 104: 23 Ninety ( 90) Day Immersion Test
Page 105 and 106: ty ,.. ='`F r...,, b Ly.. Specimen
Page 107 and 108: 25 BIODEGRADATION TEST PROCEDURE St
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Page 117 and 118: ^-..., 3•0 ASSAY FOR MEI'ALS 3.1
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Page 121 and 122: ^c. v 3 0 w.3 cn a v t[ACeRUtIIY IO
Page 123 and 124: WHC-SD-W100-TI-003 Rev. 0 APPENDIX
Page 125 and 126: WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
Page 127 and 128: 19 SCOPE AND APPLICATION WHC-SD-W10
Page 129 and 130: L:^3 ll Q. 4 AA :'ILTEP.S WHC-0-W10
Page 131 and 132: 4_T tJrD o,...Ys j ^,.,. WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 Procedure
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(FM WHC-SD-W100-TI-003 Rev. 0 Proce
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C... 6 Wet Waste Sample Contains no
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^..., . ,.y^ h:.r WHC-SD-WI00-Ti-00
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:. WHC-SD-W100-TI-003 Rev. 0 TA3i.E
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^' . WHC-SD-W100-T1-003 Rev. 0 TABL
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^- ^-> ^ C^Jl I I^t ^.: l WHC-St]-W
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c. 03 00 r=3 ^t C^' II 6.0 II Calib
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LY; ^ C=l . ^.^ .^,..,, €:^. MHC-
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R: C=1 rIj s^ ^ ^.. WHC-SD-YlI00-TI
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.,,_..1 ---^ - - i-•_E ?*^^ Mater
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WHC-SD-W100-TI-003 Rev. 0 Dow Chemi
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^ ±.£:a [7.p -;^ --- --------- WH
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WHC-S®-hi1.00-T'.-00?, Rev. Dow Ch
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t;7_7 ,...:: ----------- WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 Daw M.. u
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^ ^..rYfl VF •UIYb 1 1 AGA GllS.
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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CHARACTERIZATION DATA Part A: Overv
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Grit Specie or MaterialOverall Cont
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WHC-SD-W100-TI-003 Rev. 0 The incin
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WHC-SD-W100-TI-003 Rev. 0 183-H BAS
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WHC-SD-W100-TI-003 Rev. 0 June - Se
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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^- WHC-SD-W100-TI-003 Rev. 0 BASIN
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WHC-SD-W100-TI-003 Rev. 0 ---------
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J. L. Westcott Page 3 June 1, 1992
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u...^^, WHC-SD-W100-TI-003 Rev. 0 I
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•N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
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CONTAINER /NFORMATlO N: `d"-C-Sn-'w
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ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
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LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
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LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
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.:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
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LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
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PHYSICAL DESCR/PTTON: V-r-S?-W100-T
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,.: Westinoause Harlford COMM WHC-S
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O I tA SHEETII.XLS ;, LOT WRAP2A.2
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CONTAINER /NFORMAT/ON: DOSE: SIZE:
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PU33-11-1992 09:48 FROM EDS/qRI$ir
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LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
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qN i: 105N-89-1097 105N-89-1098 105
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SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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WHC-SD-W100-TI-003 Rev. 0 Westtngho
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LOT WRAP A2.14 SHEET 18.XLS RECOMME
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---- - LOT WRAP ZA.13 SHEET 17.XLS
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n .-.^..-n..^^- .. ... .dJ. ^ ShIEE
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--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
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WHC-SD-W100-TI-003 Rev. 0 Westingho
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Table 1 Candidate Waste Forms Absor
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--- -Aauaspt and Pe-liroset WHC-SD-
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- '^ - qev. r' Literature Search WR
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Dow Polymer WHC-SD-W100-TI-003 Rev.
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L im e Literature Search WRAP 2A Pa
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The report compares the 7eachabilit
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J. L. Westcott Page 2 May 29, 1992
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Package #1: Package #2: WHC-SD-W100
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WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
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f ..;' WHC-SD-W100-TI-003 Rev. 0 A
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 Bibliogra
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WHC-SD-W100-TI-003 Rev. 0 A. P. Tos
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OAK R1DGE NATIONAL LABORATORY OPERA
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 A report
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WHC-SD-W100-TI-003 Rev. 0 impermeab
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WHC-SD-W100-TI-003 Rev. 0 reprocess
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WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
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Contained under four reports: WHC-S
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^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
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WHC-SD-W100-TI-003 Rev. 0 The techn
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loomi^^lC& 111111111111F .^^.\ West
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û9^c ?fi. ...^ .._-, WHC-SD-W100-T
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Stock Equipment Company WHC-SD-WI00
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^ i w STOCK EOUIPMENT COMPANY 14-OC
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\. . 1 .: lh,lf^ LEACH / IMMERSIONI
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^;- v.4'? Sampls ID L781 Elsment CO
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4.a
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Sanp)a ID L781 Elamant STRONTIUM Ma
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.^ "-; SampI81D L3B2 Z e"- ^.;;. Sa
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Sample 10 L3B1 Elsmant CESIUM Matri
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Sample ID W B1 Elemant STRONIIUM Ma
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Westinghouse Hanford Company 2355 S
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--- - ftCR-e4Uip1P1eFf Company WHC-
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WHC-SD-W100-TI-003 Rev. 0 Russ Czel
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Stock Equipment Company 3:0 -SCFIED
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THERMAL CYCLING SAMPLES BEFORE THE
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BIODEGRADATION SAMPLES BEFORE THE S
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C/ 0D OC M1 0, ^yII i..) d tl ^ a I
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T 1 A w ^ • $ ^py yf ; pp V ^ py
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T 1 A ^ !^^ + ^ i •^^w^:rwwwwrpR^
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'i A v lf^. j^^ u e e - - I I I a i
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0 > d C.) O O F- 0 0 3 G NI U 3 ^ c
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en a-. p g aQ i ^ rr it - l r rF e^
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' iO`F*'P\^ Westinghouse Hanford Co
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Stock Equipment Company 1.0 SUMMARY
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Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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T 1 OI 80 70 U 60 VJ w 50 w 0 40 30
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^ °' cn l .:. U CD w a: w r' i ^ I
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SAMPLE ID Li-117 L1-118 L1-19 L3-17
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T °,w ^ - : C s 0 n a ^^ s ^ i ^-
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71 I V y,,} ^ • 5il i ^ ^^ ^ ^ ^
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0 a^ on O O M F- 1OCD 3 1 G N^ U il
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O > W C f.) O O 1-- ^ O HI 6./ 3 ^
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0 > ar oe M 0 c C3, I O c V 3 Î d
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TI V 40 IN s i s : s ^l l i " p p l
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 _QVrDvrru
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^-_- .,:... WHC-SD-W100-TI-003 Rev.
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Ceramics and glass WHC-SD-W200-TI-0
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,. ., Extruder/melter WHC-SD-W100-T
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