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A Unit of General Signal
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WHC-SD-W100-TI-003 Rev. 0
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10 CFR 61 WASTE FORM
VERIFICATION PROGRAM
1.0 Specimen Preparation . . . . . . . . . .. .. . ... .. .. . . . . . 3
1.1 Lab Scale, One (1) Crellon Specimens . . . . . . . . . . . . 3
2.0 Testing Procedures . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
2.1 Compressive Strength Test Procedure . : . . . . . . . . . . 7
2.2 Leachability Test Procedure . . . . . . . . . . . . . . . . . 13
2.3 Ninety (90) Day Immersion Test Procedure ...... 20
2.4 Thermal Degradation Test Procedure . . . . . . . . . . . 20
2.5 Bibdeqradatiofi-Test Procedure . . . . . . . . . . . . . . . . 23
2.6 Radiation Test Procedure . . . . . . . . . . . . . . . . . . . . 26
2.7 Presence of Free liquid Test Procedure ..... .... 28
3.0 Assay for Metals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
3.1 Instrumentation . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
3.2 Methods Description . . . . . . . . . . . . . . . . . . . . . . . 30
4.0 Leachability Index Calculations . . . : . . . . . . . . . . . . . . . . 33
4.1 Method of Calculating . . . . . . . . . . . ;. . . . . . . . . . 33
4.2 Data Recording . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
Appendix A - ASTM Standards . . . . . . . . . . . . . . . . . . . . . . . 35
Appendix B - Solidificatioe Liossary . . . . . . . . . . . . . . . . . . : .36
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