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n DEVELOP FORMULATIONS o Screeninp tests - Chemical compatibility - Free Water generation - Solid monolith o Surropate Performance Testing - Chemical surrogates ^ - TCLP, ANS16.1, Compressive strength, etc. o Laboratory Parametric studies - Formulation ranges and limits o Laboratory Parametric tests - Physical surrogates - Measure mixing process parameters - Determine effect on performance o Mixing Equipment tests - Full scale ( 55-gal) mixing equipment - Scale-up of mixing process o Full Scale Parametric studies - Equipment operating ranges and limits - Process Control Parameteirs - Operability / studies i i HOT DEMONS S$Q^ TION o Laboratory IHot uerification - Verify formulations o Pilot hot deinom:iration - Verify imixin+o oroce o Cold testing - Verify process o Hot testing - nualified Wast ^ ^ c A w .r _w IA PF ^ ^ 0 A= ca^ -n CI w er 0 z CA ^ a m ^ ^ (/^1 QI î 0 w ^< 0
^.: fi WNC-SD-W100-TI-003 Rev. 0 Figure 3-2. WRAP 2A Process Development Waste Form Qualification Project Logic. 3-7
Page 1 and 2: R 2.1 199^ ^.EN GINEERING DATA TRAN
Page 3 and 4: Date Received% • I INFORMATION RE
Page 5 and 6: . SUPPORTING DOCUMENT 1. Total Page
Page 7 and 8: WHC-SD-W100-TI-003 Rev. 0 EXECUTIVE
Page 9 and 10: WHC-SD-W100-TI-003 Rev. 0 been achi
Page 11 and 12: __ _ _ MHC-SIL-yJ3,00-TI-D03 Rev. 0
Page 13 and 14: F`= WHC-SD-W100-TI-003 Rev. 0 DESCR
Page 15 and 16: WHC-SD-W100-TI-003 Rev. 0 LIST OF T
Page 17 and 18: WHC-SD-W100-TI-003 Rev. 0 WASTE REC
Page 19 and 20: WHC-SD-W100-TI-003 Rev. 0 1.2.1 Fee
Page 21 and 22: ^s. WHC-SD-W100-TI-003 Rev. 0 conta
Page 23 and 24: __-'°'2 WHC-SD-W100-TI-003 Rev. 0
Page 25 and 26: 2.1 REGULATORY FRAMEWORK WHC-SD-W10
Page 27 and 28: ^..." ;_:.. :.^ .^.y^ WHC-SD-W100-T
Page 29 and 30: WHC-SD-W100-TI-003 Rev. 0 which the
Page 31 and 32: kIHC-Sû-Wi"v"u-Ti-u03 Rev. V ,--,,
Page 33 and 34: WHC-SD-W100-TI-003 Rev. 0 Type 1 wa
Page 35: 3.3 TESTING APPROACH WHC-SD-W100-TI
Page 39 and 40: 4.1 SCREENING TEST RESULTS WHC-SD-W
Page 41 and 42: ,^. ----- -- WHC-SD-W100-TI-003 Rev
Page 43 and 44: WHC-SD-W100-TI-003 Rev. 0 4.1.3 The
Page 45 and 46: p Sam le Compressive Radiation stre
Page 47 and 48: WHC-SD-W100-TI-003 Rev. 0 Table 4-3
Page 49 and 50: ..., TESTING RESULTS .^.CSSD-W-1OO-
Page 51 and 52: A I w ^^',; ^^ ;J ?1Fasf^.}: "q -?
Page 53 and 54: ;..;: .^:. WHC-SD-W100-TI-003 Rev.
Page 55 and 56: --- ....ti s..` WHC-SD-WI00-TI-003
Page 57 and 58: 1.0 INTRODUCTION WHC-SD-W100-TI-003
Page 59 and 60: WHC-SD-W100-TI-003 Rev. 0 Waste For
Page 61 and 62: ^-: -- ^ Component Waste Type 1 LET
Page 63 and 64: .^x. --1vHC-SD iii00- T i-003 Rev.
Page 65 and 66: WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
Page 67 and 68: ,..^ c:-- z ,.E ^=t ^^ln^l WHC-SD-W
Page 69 and 70: Scope WHC-SD-W100-TI-003 Rev. 0 Sup
Page 71 and 72: 00 V F-' Activity and Miltstone Cha
Page 73 and 74: WHC-SD-W100-TI-003 Rev. 0 Laborator
Page 75 and 76: WHC-SD-WIOO-TI-003 Rev. 0 APPENDIX
Page 77 and 78: 16490 Chiaccothe Itoad Chagrin Fall
Page 79 and 80: ca-. tY•^_E Q . - - StoGkE4uip+!n
Page 81 and 82: ^.. WHC-SD-W100-TI-003 Rev. 0 . , I
Page 83 and 84: Waste Type: WHC-SD-W100-TI-003 Rev.
Page 85 and 86: Stock E quipment Company A Unit of
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G' ,.,. d,_ s WHC-0-W100-TI-003 Rev
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Cx U: r°... .• , .ti Waste Type:
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-. LeachantSolution: Specimen Diame
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c^1, WHC-SD-W100-TI-003 Rev. 0 THER
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..... lry" - Stock E a uipment Comp
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;=. .:^;. WHC-SD-W100-TI-003 Rev< 0
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(.7 ..^^ -„n f^. [Y^. Waste Type:
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Date: _ Leachability Time Point Lea
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23 Ninety ( 90) Day Immersion Test
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ty ,.. ='`F r...,, b Ly.. Specimen
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25 BIODEGRADATION TEST PROCEDURE St
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Date: WHC-SD-W100-TI-003 Rev. 0 BIO
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^_... ..^^ C:i1 Date: WHC-SD-W100-T
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Date: WHC-SD-W100-TI-003 Rev. 0 --
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f-^ -- WHC-SD-W100-TI-003 Rev. 0 2.
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^-..., 3•0 ASSAY FOR MEI'ALS 3.1
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t..f f....,.. P....^ .-- ^ : .^ ^-.
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^c. v 3 0 w.3 cn a v t[ACeRUtIIY IO
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
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19 SCOPE AND APPLICATION WHC-SD-W10
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L:^3 ll Q. 4 AA :'ILTEP.S WHC-0-W10
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4_T tJrD o,...Ys j ^,.,. WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 -, Proced
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WHC-SD-W100-TI-003 Rev. 0 Procedure
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(FM WHC-SD-W100-TI-003 Rev. 0 Proce
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C... 6 Wet Waste Sample Contains no
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^..., . ,.y^ h:.r WHC-SD-WI00-Ti-00
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:. WHC-SD-W100-TI-003 Rev. 0 TA3i.E
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^' . WHC-SD-W100-T1-003 Rev. 0 TABL
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^- ^-> ^ C^Jl I I^t ^.: l WHC-St]-W
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c. 03 00 r=3 ^t C^' II 6.0 II Calib
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LY; ^ C=l . ^.^ .^,..,, €:^. MHC-
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R: C=1 rIj s^ ^ ^.. WHC-SD-YlI00-TI
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.,,_..1 ---^ - - i-•_E ?*^^ Mater
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WHC-SD-W100-TI-003 Rev. 0 Dow Chemi
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^ ±.£:a [7.p -;^ --- --------- WH
Page 161 and 162:
WHC-S®-hi1.00-T'.-00?, Rev. Dow Ch
Page 163 and 164:
t;7_7 ,...:: ----------- WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 Daw M.. u
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^ ^..rYfl VF •UIYb 1 1 AGA GllS.
Page 169 and 170:
Page 171 and 172:
CHARACTERIZATION DATA Part A: Overv
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Grit Specie or MaterialOverall Cont
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WHC-SD-W100-TI-003 Rev. 0 The incin
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WHC-SD-W100-TI-003 Rev. 0 183-H BAS
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WHC-SD-W100-TI-003 Rev. 0 June - Se
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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^- WHC-SD-W100-TI-003 Rev. 0 BASIN
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WHC-SD-W100-TI-003 Rev. 0 ---------
Page 189 and 190:
J. L. Westcott Page 3 June 1, 1992
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u...^^, WHC-SD-W100-TI-003 Rev. 0 I
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•N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
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CONTAINER /NFORMATlO N: `d"-C-Sn-'w
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ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
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LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
Page 201 and 202:
LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
Page 203 and 204:
.:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
Page 205 and 206:
LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
Page 207 and 208:
PHYSICAL DESCR/PTTON: V-r-S?-W100-T
Page 209 and 210:
,.: Westinoause Harlford COMM WHC-S
Page 211 and 212:
O I tA SHEETII.XLS ;, LOT WRAP2A.2
Page 213 and 214:
CONTAINER /NFORMAT/ON: DOSE: SIZE:
Page 215 and 216:
PU33-11-1992 09:48 FROM EDS/qRI$ir
Page 217 and 218:
LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
Page 219 and 220:
qN i: 105N-89-1097 105N-89-1098 105
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SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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WHC-SD-W100-TI-003 Rev. 0 Westtngho
Page 225 and 226:
LOT WRAP A2.14 SHEET 18.XLS RECOMME
Page 227 and 228:
---- - LOT WRAP ZA.13 SHEET 17.XLS
Page 229 and 230:
n .-.^..-n..^^- .. ... .dJ. ^ ShIEE
Page 231 and 232:
--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
Page 233 and 234:
WHC-SD-W100-TI-003 Rev. 0 Westingho
Page 235 and 236:
Table 1 Candidate Waste Forms Absor
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--- -Aauaspt and Pe-liroset WHC-SD-
Page 239 and 240:
- '^ - qev. r' Literature Search WR
Page 241 and 242:
Dow Polymer WHC-SD-W100-TI-003 Rev.
Page 243 and 244:
L im e Literature Search WRAP 2A Pa
Page 245 and 246:
The report compares the 7eachabilit
Page 247 and 248:
J. L. Westcott Page 2 May 29, 1992
Page 249 and 250:
Package #1: Package #2: WHC-SD-W100
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WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
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f ..;' WHC-SD-W100-TI-003 Rev. 0 A
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 Bibliogra
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WHC-SD-W100-TI-003 Rev. 0 A. P. Tos
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OAK R1DGE NATIONAL LABORATORY OPERA
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 A report
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WHC-SD-W100-TI-003 Rev. 0 impermeab
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WHC-SD-W100-TI-003 Rev. 0 reprocess
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WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
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Contained under four reports: WHC-S
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^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
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WHC-SD-W100-TI-003 Rev. 0 The techn
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loomi^^lC& 111111111111F .^^.\ West
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û9^c ?fi. ...^ .._-, WHC-SD-W100-T
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Stock Equipment Company WHC-SD-WI00
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^ i w STOCK EOUIPMENT COMPANY 14-OC
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\. . 1 .: lh,lf^ LEACH / IMMERSIONI
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^;- v.4'? Sampls ID L781 Elsment CO
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4.a
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Sanp)a ID L781 Elamant STRONTIUM Ma
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.^ "-; SampI81D L3B2 Z e"- ^.;;. Sa
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Sample 10 L3B1 Elsmant CESIUM Matri
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Sample ID W B1 Elemant STRONIIUM Ma
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Westinghouse Hanford Company 2355 S
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--- - ftCR-e4Uip1P1eFf Company WHC-
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WHC-SD-W100-TI-003 Rev. 0 Russ Czel
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Stock Equipment Company 3:0 -SCFIED
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THERMAL CYCLING SAMPLES BEFORE THE
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BIODEGRADATION SAMPLES BEFORE THE S
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C/ 0D OC M1 0, ^yII i..) d tl ^ a I
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' iO`F*'P\^ Westinghouse Hanford Co
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Stock Equipment Company 1.0 SUMMARY
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Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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T 1 OI 80 70 U 60 VJ w 50 w 0 40 30
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SAMPLE ID Li-117 L1-118 L1-19 L3-17
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WHC-SD-W100-TI-003 Rev. 0 _QVrDvrru
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^-_- .,:... WHC-SD-W100-TI-003 Rev.
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Ceramics and glass WHC-SD-W200-TI-0
Page 365 and 366:
,. ., Extruder/melter WHC-SD-W100-T
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