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WHC-SD-W100-TI-003 Rev. 0 Table 4-6. Summary of Polymer Waste Form Testing Results. Waste form Acceptance Test results characteristic criteria Type 1 Type 2 Type 3 Type 4 Compressive strength Leachability index Strength.. >500 psi 2,472 psi 1,085 psi 1,411 psi 942 psi Leach index >6 Cs 7.7/7.4 7.0/7.0 7.3/7.2 7.1/7.1 Demin/sea water Co Sr 8.2/7.9 8.9/8.7 9.2/9.3 9.3/9.1 10.1/10.3 10.2/9.4 7.5/7.7 9.1/9.0 No growth, No growth No growth No growth No growth Bi o d egra d a ti on s t reng th -' >506 psi 2,247 psi 3,710 psi 994 psi 1,114 psi Thermal cycling Radiation stability Immersion Free liquids Strength >500 psi after 30 thermal cycles Strength >500 psi after irradiation to 10 rad Strength >500 psi after 90-day immersion Free liquid
A I w ^^',; ^^ ;J ?1Fasf^.}: "q -? : ll .(„ F ^d^.ie J. .. Table 4-7. Follow-On Testing Results. Acceptance Test results Waste form criteria Wast.e type 1 Waste type 2 Waste type 4 characteristic Sample preparation method* A B C A B C A B C Toxicity characteristics Ba 0.022 0.320 N/A N/A N/A 0.268 100 N/A N/A N/A pass pass pass TCLP leachable Cd 1 . 0 N/A N/A N/A N/A N/A N/A N/A N/A N/A metals below EPA limits Cr 5.0 0.275 P ass 0.844 P ass 1.056 p ass 1.76 P ass 4.37 P ass 4.82 P ass 2.03 pass 2.19 pass 2.46 pass (parts per million) Hg 0.2 0.182 pass 0.385 fail 0.350 fail 0.194 pass 0.270 fail 0.245 fail N/A N/A N/A 0.045 0.040 0.066 A9 N/A N/A N/A 5.0 pass pass pass *Method A= Pellets; Method B= Crushing; Method C= Crush, discard fines. N/A = not applicable. TCLP = Toxicity Characteristic Leaching Procedure. N/A N/A N/A x ^ ^^c E 0 0 -d M ^ 0 0w Am < 0
Page 1 and 2: R 2.1 199^ ^.EN GINEERING DATA TRAN
Page 3 and 4: Date Received% • I INFORMATION RE
Page 5 and 6: . SUPPORTING DOCUMENT 1. Total Page
Page 7 and 8: WHC-SD-W100-TI-003 Rev. 0 EXECUTIVE
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Page 13 and 14: F`= WHC-SD-W100-TI-003 Rev. 0 DESCR
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Page 17 and 18: WHC-SD-W100-TI-003 Rev. 0 WASTE REC
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Page 25 and 26: 2.1 REGULATORY FRAMEWORK WHC-SD-W10
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Page 47 and 48: WHC-SD-W100-TI-003 Rev. 0 Table 4-3
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Page 57 and 58: 1.0 INTRODUCTION WHC-SD-W100-TI-003
Page 59 and 60: WHC-SD-W100-TI-003 Rev. 0 Waste For
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Page 65 and 66: WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
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Page 69 and 70: Scope WHC-SD-W100-TI-003 Rev. 0 Sup
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Page 73 and 74: WHC-SD-W100-TI-003 Rev. 0 Laborator
Page 75 and 76: WHC-SD-WIOO-TI-003 Rev. 0 APPENDIX
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Page 91 and 92: -. LeachantSolution: Specimen Diame
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Date: _ Leachability Time Point Lea
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23 Ninety ( 90) Day Immersion Test
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ty ,.. ='`F r...,, b Ly.. Specimen
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25 BIODEGRADATION TEST PROCEDURE St
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Date: WHC-SD-W100-TI-003 Rev. 0 BIO
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^_... ..^^ C:i1 Date: WHC-SD-W100-T
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Date: WHC-SD-W100-TI-003 Rev. 0 --
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f-^ -- WHC-SD-W100-TI-003 Rev. 0 2.
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^-..., 3•0 ASSAY FOR MEI'ALS 3.1
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
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19 SCOPE AND APPLICATION WHC-SD-W10
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L:^3 ll Q. 4 AA :'ILTEP.S WHC-0-W10
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4_T tJrD o,...Ys j ^,.,. WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 -, Proced
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WHC-SD-W100-TI-003 Rev. 0 Procedure
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(FM WHC-SD-W100-TI-003 Rev. 0 Proce
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C... 6 Wet Waste Sample Contains no
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^' . WHC-SD-W100-T1-003 Rev. 0 TABL
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c. 03 00 r=3 ^t C^' II 6.0 II Calib
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WHC-SD-W100-TI-003 Rev. 0 Dow Chemi
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WHC-S®-hi1.00-T'.-00?, Rev. Dow Ch
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WHC-SD-W100-TI-003 Rev. 0 Daw M.. u
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CHARACTERIZATION DATA Part A: Overv
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Grit Specie or MaterialOverall Cont
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WHC-SD-W100-TI-003 Rev. 0 The incin
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WHC-SD-W100-TI-003 Rev. 0 183-H BAS
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WHC-SD-W100-TI-003 Rev. 0 June - Se
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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^- WHC-SD-W100-TI-003 Rev. 0 BASIN
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WHC-SD-W100-TI-003 Rev. 0 ---------
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J. L. Westcott Page 3 June 1, 1992
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u...^^, WHC-SD-W100-TI-003 Rev. 0 I
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•N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
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CONTAINER /NFORMATlO N: `d"-C-Sn-'w
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ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
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LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
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LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
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.:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
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LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
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PHYSICAL DESCR/PTTON: V-r-S?-W100-T
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,.: Westinoause Harlford COMM WHC-S
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O I tA SHEETII.XLS ;, LOT WRAP2A.2
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CONTAINER /NFORMAT/ON: DOSE: SIZE:
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PU33-11-1992 09:48 FROM EDS/qRI$ir
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LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
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qN i: 105N-89-1097 105N-89-1098 105
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SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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WHC-SD-W100-TI-003 Rev. 0 Westtngho
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LOT WRAP A2.14 SHEET 18.XLS RECOMME
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---- - LOT WRAP ZA.13 SHEET 17.XLS
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n .-.^..-n..^^- .. ... .dJ. ^ ShIEE
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--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
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WHC-SD-W100-TI-003 Rev. 0 Westingho
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Table 1 Candidate Waste Forms Absor
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--- -Aauaspt and Pe-liroset WHC-SD-
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- '^ - qev. r' Literature Search WR
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Dow Polymer WHC-SD-W100-TI-003 Rev.
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L im e Literature Search WRAP 2A Pa
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The report compares the 7eachabilit
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J. L. Westcott Page 2 May 29, 1992
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Package #1: Package #2: WHC-SD-W100
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WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
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f ..;' WHC-SD-W100-TI-003 Rev. 0 A
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 Bibliogra
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WHC-SD-W100-TI-003 Rev. 0 A. P. Tos
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OAK R1DGE NATIONAL LABORATORY OPERA
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 A report
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WHC-SD-W100-TI-003 Rev. 0 impermeab
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WHC-SD-W100-TI-003 Rev. 0 reprocess
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WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
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Contained under four reports: WHC-S
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^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
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WHC-SD-W100-TI-003 Rev. 0 The techn
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loomi^^lC& 111111111111F .^^.\ West
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Stock Equipment Company WHC-SD-WI00
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^ i w STOCK EOUIPMENT COMPANY 14-OC
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\. . 1 .: lh,lf^ LEACH / IMMERSIONI
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4.a
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Sanp)a ID L781 Elamant STRONTIUM Ma
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Sample 10 L3B1 Elsmant CESIUM Matri
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Sample ID W B1 Elemant STRONIIUM Ma
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Westinghouse Hanford Company 2355 S
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--- - ftCR-e4Uip1P1eFf Company WHC-
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WHC-SD-W100-TI-003 Rev. 0 Russ Czel
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Stock Equipment Company 3:0 -SCFIED
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THERMAL CYCLING SAMPLES BEFORE THE
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BIODEGRADATION SAMPLES BEFORE THE S
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Stock Equipment Company 1.0 SUMMARY
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Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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Ceramics and glass WHC-SD-W200-TI-0
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,. ., Extruder/melter WHC-SD-W100-T
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