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WHC-SD-W100-TI-003 Rev. 0 The third set of waste forms were the large cylinders, 30.5 cm (12 in.) high with a 15-cm (6-in.) diameter. The large cylinder waste forms were allowed to cure for 28 days before they were compressive strength tested. The large cylinder test results are shown in Table 4-2. Radiation Stability Two identical waste form cubes for each waste type were irradiated to a total dose of 108 radiation in a gamma irradiation faci_lity,_ Each_cube- was then compressive strength tested. Weights for each of the ten samples were recorded before and after irradiation. No weight change was observed and no visual change in color or appearance was observed. The compressive strength test results are shown in Table 4-2. Biodegradation Ten waste form cubes, two duplicate cubes for each waste type, were subject to ideal growth conditions for bacteria, for a period of 21 days. After this incubation period, the waste forms were tested for compressive strength. The results are shown in Table 4-2. T Leachability Index Cube samples for each waste type were subject to the leachability index test. The test results are shown in Table 4-2. Water Immersion Three cube samples for each waste type were stored in moist conditions over a period of time. After 14 days, one of the cubes for each of the waste types was compressive strength tested. After 42 days, the second cube sample was compressive-strength tested. _After 90 days, the third sample was tested. The results are shown in Table 4-2. Thermal Cycling Two cube samples for each waste stream were heated to +60 °C (140 °F), cooled, frozen to -40 °C (-40 °F), and then thawed. The cycle was repeated 30 times and then a compressive strength test was performed on each cube sample. Results are shown in Table 4-2. Free Liquid The samples were prepared by pouring the slurry mix into 13 cmZ (2-in 2) plastic bottles to a 5-cm (2-in.) height, for each of the waste types. Duplicate samples for each waste type were prepared. At the end of a 24-hour period each sample was visually inspected for the presence of liquid. The amount of liquid, if any, was measured. The results are shown in Table 4-1. EPA (TCLP) Tests The test involves obtaining an extract from the waste form and analyzing the extract for toxic constituents. The test results for the TCLP tests are summarized in Table 4-3. 4-8
WHC-SD-W100-TI-003 Rev. 0 Table 4-3. TCLP Results for WRAP 2A Cement Waste Forms. Sample Specie Type 5 0riginal Cont. TCLP Cont. Limit Pass/fail Chromium 50 ppm 0.07 ppm 5 ppm Pass Copper 1.7% 0.09 ppm No limit N/A Type 6 Chromium 50 ppm
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Page 15 and 16: WHC-SD-W100-TI-003 Rev. 0 LIST OF T
Page 17 and 18: WHC-SD-W100-TI-003 Rev. 0 WASTE REC
Page 19 and 20: WHC-SD-W100-TI-003 Rev. 0 1.2.1 Fee
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Page 25 and 26: 2.1 REGULATORY FRAMEWORK WHC-SD-W10
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Page 39 and 40: 4.1 SCREENING TEST RESULTS WHC-SD-W
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Page 57 and 58: 1.0 INTRODUCTION WHC-SD-W100-TI-003
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Page 65 and 66: WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
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Page 69 and 70: Scope WHC-SD-W100-TI-003 Rev. 0 Sup
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Page 73 and 74: WHC-SD-W100-TI-003 Rev. 0 Laborator
Page 75 and 76: WHC-SD-WIOO-TI-003 Rev. 0 APPENDIX
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Page 91 and 92: -. LeachantSolution: Specimen Diame
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;=. .:^;. WHC-SD-W100-TI-003 Rev< 0
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(.7 ..^^ -„n f^. [Y^. Waste Type:
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Date: _ Leachability Time Point Lea
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23 Ninety ( 90) Day Immersion Test
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ty ,.. ='`F r...,, b Ly.. Specimen
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25 BIODEGRADATION TEST PROCEDURE St
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Date: WHC-SD-W100-TI-003 Rev. 0 BIO
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^_... ..^^ C:i1 Date: WHC-SD-W100-T
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Date: WHC-SD-W100-TI-003 Rev. 0 --
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f-^ -- WHC-SD-W100-TI-003 Rev. 0 2.
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^-..., 3•0 ASSAY FOR MEI'ALS 3.1
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
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19 SCOPE AND APPLICATION WHC-SD-W10
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L:^3 ll Q. 4 AA :'ILTEP.S WHC-0-W10
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4_T tJrD o,...Ys j ^,.,. WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 -, Proced
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WHC-SD-W100-TI-003 Rev. 0 Procedure
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(FM WHC-SD-W100-TI-003 Rev. 0 Proce
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C... 6 Wet Waste Sample Contains no
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^' . WHC-SD-W100-T1-003 Rev. 0 TABL
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WHC-SD-W100-TI-003 Rev. 0 Dow Chemi
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WHC-SD-W100-TI-003 Rev. 0 Daw M.. u
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CHARACTERIZATION DATA Part A: Overv
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Grit Specie or MaterialOverall Cont
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WHC-SD-W100-TI-003 Rev. 0 The incin
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WHC-SD-W100-TI-003 Rev. 0 183-H BAS
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WHC-SD-W100-TI-003 Rev. 0 June - Se
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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^- WHC-SD-W100-TI-003 Rev. 0 BASIN
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WHC-SD-W100-TI-003 Rev. 0 ---------
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J. L. Westcott Page 3 June 1, 1992
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u...^^, WHC-SD-W100-TI-003 Rev. 0 I
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•N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
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CONTAINER /NFORMATlO N: `d"-C-Sn-'w
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ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
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LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
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LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
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.:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
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LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
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PHYSICAL DESCR/PTTON: V-r-S?-W100-T
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,.: Westinoause Harlford COMM WHC-S
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O I tA SHEETII.XLS ;, LOT WRAP2A.2
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CONTAINER /NFORMAT/ON: DOSE: SIZE:
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PU33-11-1992 09:48 FROM EDS/qRI$ir
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LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
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qN i: 105N-89-1097 105N-89-1098 105
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SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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WHC-SD-W100-TI-003 Rev. 0 Westtngho
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LOT WRAP A2.14 SHEET 18.XLS RECOMME
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---- - LOT WRAP ZA.13 SHEET 17.XLS
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--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
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WHC-SD-W100-TI-003 Rev. 0 Westingho
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Table 1 Candidate Waste Forms Absor
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--- -Aauaspt and Pe-liroset WHC-SD-
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- '^ - qev. r' Literature Search WR
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Dow Polymer WHC-SD-W100-TI-003 Rev.
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L im e Literature Search WRAP 2A Pa
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The report compares the 7eachabilit
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J. L. Westcott Page 2 May 29, 1992
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Package #1: Package #2: WHC-SD-W100
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WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
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f ..;' WHC-SD-W100-TI-003 Rev. 0 A
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 Bibliogra
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WHC-SD-W100-TI-003 Rev. 0 A. P. Tos
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OAK R1DGE NATIONAL LABORATORY OPERA
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 A report
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WHC-SD-W100-TI-003 Rev. 0 impermeab
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WHC-SD-W100-TI-003 Rev. 0 reprocess
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WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
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Contained under four reports: WHC-S
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^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
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WHC-SD-W100-TI-003 Rev. 0 The techn
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Stock Equipment Company WHC-SD-WI00
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^ i w STOCK EOUIPMENT COMPANY 14-OC
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\. . 1 .: lh,lf^ LEACH / IMMERSIONI
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Sanp)a ID L781 Elamant STRONTIUM Ma
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.^ "-; SampI81D L3B2 Z e"- ^.;;. Sa
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Sample 10 L3B1 Elsmant CESIUM Matri
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Sample ID W B1 Elemant STRONIIUM Ma
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Westinghouse Hanford Company 2355 S
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--- - ftCR-e4Uip1P1eFf Company WHC-
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WHC-SD-W100-TI-003 Rev. 0 Russ Czel
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Stock Equipment Company 3:0 -SCFIED
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THERMAL CYCLING SAMPLES BEFORE THE
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BIODEGRADATION SAMPLES BEFORE THE S
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Stock Equipment Company 1.0 SUMMARY
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Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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T 1 OI 80 70 U 60 VJ w 50 w 0 40 30
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WHC-SD-W100-TI-003 Rev. 0 _QVrDvrru
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^-_- .,:... WHC-SD-W100-TI-003 Rev.
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Ceramics and glass WHC-SD-W200-TI-0
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,. ., Extruder/melter WHC-SD-W100-T
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