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Stock Equipment Company WHC-SD-W100-TI-003 Rev. 0 WESTINGHOUSE HANFORD COMPANY STnru Fni rrPT,rRTrr rn POLYMER IMMOBILLIZATION TECH. WASTE FORM QUALIFICATION TESTING MONTHLY PROGRESS REPORT NO. 2 THROUGH SEPTEMBER, 1992 Stock Equipment Company Westinghouse <strong>Hanford</strong> Purchase Order No. MMW-SVV-277587 Stock Order No. 6996 F-8 ;;:,:•
û9^c ?fi. ...^ .._-, WHC-SD-W100-TI-003 Rev. 0 TABLE OF CONTENTS Page i0 SUMMARY 1& 2 2.0 SCHEDULE 3 BAR CHART SCHEDULE 4 F-9
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R 2.1 199^ ^.EN GINEERING DATA TRAN
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Date Received% • I INFORMATION RE
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. SUPPORTING DOCUMENT 1. Total Page
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WHC-SD-W100-TI-003 Rev. 0 EXECUTIVE
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WHC-SD-W100-TI-003 Rev. 0 been achi
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__ _ _ MHC-SIL-yJ3,00-TI-D03 Rev. 0
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F`= WHC-SD-W100-TI-003 Rev. 0 DESCR
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WHC-SD-W100-TI-003 Rev. 0 LIST OF T
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WHC-SD-W100-TI-003 Rev. 0 WASTE REC
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WHC-SD-W100-TI-003 Rev. 0 1.2.1 Fee
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^s. WHC-SD-W100-TI-003 Rev. 0 conta
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__-'°'2 WHC-SD-W100-TI-003 Rev. 0
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2.1 REGULATORY FRAMEWORK WHC-SD-W10
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^..." ;_:.. :.^ .^.y^ WHC-SD-W100-T
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WHC-SD-W100-TI-003 Rev. 0 which the
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kIHC-Sû-Wi"v"u-Ti-u03 Rev. V ,--,,
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WHC-SD-W100-TI-003 Rev. 0 Type 1 wa
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3.3 TESTING APPROACH WHC-SD-W100-TI
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^.: fi WNC-SD-W100-TI-003 Rev. 0 Fi
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4.1 SCREENING TEST RESULTS WHC-SD-W
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,^. ----- -- WHC-SD-W100-TI-003 Rev
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WHC-SD-W100-TI-003 Rev. 0 4.1.3 The
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p Sam le Compressive Radiation stre
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WHC-SD-W100-TI-003 Rev. 0 Table 4-3
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..., TESTING RESULTS .^.CSSD-W-1OO-
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A I w ^^',; ^^ ;J ?1Fasf^.}: "q -?
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;..;: .^:. WHC-SD-W100-TI-003 Rev.
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--- ....ti s..` WHC-SD-WI00-TI-003
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1.0 INTRODUCTION WHC-SD-W100-TI-003
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WHC-SD-W100-TI-003 Rev. 0 Waste For
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^-: -- ^ Component Waste Type 1 LET
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.^x. --1vHC-SD iii00- T i-003 Rev.
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WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
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,..^ c:-- z ,.E ^=t ^^ln^l WHC-SD-W
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Scope WHC-SD-W100-TI-003 Rev. 0 Sup
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00 V F-' Activity and Miltstone Cha
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WHC-SD-W100-TI-003 Rev. 0 Laborator
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WHC-SD-WIOO-TI-003 Rev. 0 APPENDIX
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16490 Chiaccothe Itoad Chagrin Fall
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ca-. tY•^_E Q . - - StoGkE4uip+!n
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^.. WHC-SD-W100-TI-003 Rev. 0 . , I
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Waste Type: WHC-SD-W100-TI-003 Rev.
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Stock E quipment Company A Unit of
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G' ,.,. d,_ s WHC-0-W100-TI-003 Rev
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Cx U: r°... .• , .ti Waste Type:
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-. LeachantSolution: Specimen Diame
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c^1, WHC-SD-W100-TI-003 Rev. 0 THER
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..... lry" - Stock E a uipment Comp
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;=. .:^;. WHC-SD-W100-TI-003 Rev< 0
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(.7 ..^^ -„n f^. [Y^. Waste Type:
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Date: _ Leachability Time Point Lea
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23 Ninety ( 90) Day Immersion Test
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ty ,.. ='`F r...,, b Ly.. Specimen
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25 BIODEGRADATION TEST PROCEDURE St
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Date: WHC-SD-W100-TI-003 Rev. 0 BIO
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^_... ..^^ C:i1 Date: WHC-SD-W100-T
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Date: WHC-SD-W100-TI-003 Rev. 0 --
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f-^ -- WHC-SD-W100-TI-003 Rev. 0 2.
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^-..., 3•0 ASSAY FOR MEI'ALS 3.1
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t..f f....,.. P....^ .-- ^ : .^ ^-.
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^c. v 3 0 w.3 cn a v t[ACeRUtIIY IO
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
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19 SCOPE AND APPLICATION WHC-SD-W10
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L:^3 ll Q. 4 AA :'ILTEP.S WHC-0-W10
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4_T tJrD o,...Ys j ^,.,. WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 -, Proced
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WHC-SD-W100-TI-003 Rev. 0 Procedure
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(FM WHC-SD-W100-TI-003 Rev. 0 Proce
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C... 6 Wet Waste Sample Contains no
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^..., . ,.y^ h:.r WHC-SD-WI00-Ti-00
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:. WHC-SD-W100-TI-003 Rev. 0 TA3i.E
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^' . WHC-SD-W100-T1-003 Rev. 0 TABL
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^- ^-> ^ C^Jl I I^t ^.: l WHC-St]-W
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c. 03 00 r=3 ^t C^' II 6.0 II Calib
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LY; ^ C=l . ^.^ .^,..,, €:^. MHC-
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R: C=1 rIj s^ ^ ^.. WHC-SD-YlI00-TI
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.,,_..1 ---^ - - i-•_E ?*^^ Mater
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WHC-SD-W100-TI-003 Rev. 0 Dow Chemi
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^ ±.£:a [7.p -;^ --- --------- WH
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WHC-S®-hi1.00-T'.-00?, Rev. Dow Ch
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t;7_7 ,...:: ----------- WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 Daw M.. u
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^ ^..rYfl VF •UIYb 1 1 AGA GllS.
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CHARACTERIZATION DATA Part A: Overv
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Grit Specie or MaterialOverall Cont
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WHC-SD-W100-TI-003 Rev. 0 The incin
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WHC-SD-W100-TI-003 Rev. 0 183-H BAS
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WHC-SD-W100-TI-003 Rev. 0 June - Se
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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^- WHC-SD-W100-TI-003 Rev. 0 BASIN
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WHC-SD-W100-TI-003 Rev. 0 ---------
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J. L. Westcott Page 3 June 1, 1992
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u...^^, WHC-SD-W100-TI-003 Rev. 0 I
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•N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
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CONTAINER /NFORMATlO N: `d"-C-Sn-'w
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ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
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LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
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LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
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.:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
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LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
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PHYSICAL DESCR/PTTON: V-r-S?-W100-T
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,.: Westinoause Harlford COMM WHC-S
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O I tA SHEETII.XLS ;, LOT WRAP2A.2
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CONTAINER /NFORMAT/ON: DOSE: SIZE:
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PU33-11-1992 09:48 FROM EDS/qRI$ir
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LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
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qN i: 105N-89-1097 105N-89-1098 105
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SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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WHC-SD-W100-TI-003 Rev. 0 Westtngho
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LOT WRAP A2.14 SHEET 18.XLS RECOMME
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---- - LOT WRAP ZA.13 SHEET 17.XLS
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n .-.^..-n..^^- .. ... .dJ. ^ ShIEE
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--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
Page 233 and 234: WHC-SD-W100-TI-003 Rev. 0 Westingho
Page 235 and 236: Table 1 Candidate Waste Forms Absor
Page 237 and 238: --- -Aauaspt and Pe-liroset WHC-SD-
Page 239 and 240: - '^ - qev. r' Literature Search WR
Page 241 and 242: Dow Polymer WHC-SD-W100-TI-003 Rev.
Page 243 and 244: L im e Literature Search WRAP 2A Pa
Page 245 and 246: The report compares the 7eachabilit
Page 247 and 248: J. L. Westcott Page 2 May 29, 1992
Page 249 and 250: Package #1: Package #2: WHC-SD-W100
Page 251 and 252: WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
Page 253 and 254: f ..;' WHC-SD-W100-TI-003 Rev. 0 A
Page 257 and 258: WHC-SD-W100-TI-003 Rev. 0 commercia
Page 259 and 260: WHC-SD-W100-TI-003 Revo 0 Bibliogra
Page 261 and 262: WHC-SD-W100-TI-003 Rev. 0 A. P. Tos
Page 263 and 264: OAK R1DGE NATIONAL LABORATORY OPERA
Page 267 and 268: WHC-SD-W100-TI-003 Rev. 0 commercia
Page 269 and 270: WHC-SD-W100-TI-003 Revo 0 A report
Page 271 and 272: WHC-SD-W100-TI-003 Rev. 0 impermeab
Page 273 and 274: WHC-SD-W100-TI-003 Rev. 0 reprocess
Page 275 and 276: WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
Page 277 and 278: Contained under four reports: WHC-S
Page 279 and 280: ^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
Page 281 and 282: WHC-SD-W100-TI-003 Rev. 0 The techn
Page 283: loomi^^lC& 111111111111F .^^.\ West
Page 287 and 288: Stock Equipment Company WHC-SD-WI00
Page 289 and 290: ^ i w STOCK EOUIPMENT COMPANY 14-OC
Page 291 and 292: \. . 1 .: lh,lf^ LEACH / IMMERSIONI
Page 293 and 294: ^;- v.4'? Sampls ID L781 Elsment CO
Page 295 and 296: 4.a
Page 297 and 298: Sanp)a ID L781 Elamant STRONTIUM Ma
Page 299 and 300: .^ "-; SampI81D L3B2 Z e"- ^.;;. Sa
Page 301 and 302: Sample 10 L3B1 Elsmant CESIUM Matri
Page 303 and 304: Sample ID W B1 Elemant STRONIIUM Ma
Page 305 and 306: Westinghouse Hanford Company 2355 S
Page 307 and 308: --- - ftCR-e4Uip1P1eFf Company WHC-
Page 309 and 310: WHC-SD-W100-TI-003 Rev. 0 Russ Czel
Page 311 and 312: Stock Equipment Company 3:0 -SCFIED
Page 313 and 314: THERMAL CYCLING SAMPLES BEFORE THE
Page 315 and 316: BIODEGRADATION SAMPLES BEFORE THE S
Page 317 and 318: C/ 0D OC M1 0, ^yII i..) d tl ^ a I
Page 319 and 320: T 1 A w ^ • $ ^py yf ; pp V ^ py
Page 321 and 322: T 1 A ^ !^^ + ^ i •^^w^:rwwwwrpR^
Page 323 and 324: 'i A v lf^. j^^ u e e - - I I I a i
Page 325 and 326: 0 > d C.) O O F- 0 0 3 G NI U 3 ^ c
Page 327 and 328: en a-. p g aQ i ^ rr it - l r rF e^
Page 329 and 330: ' iO`F*'P\^ Westinghouse Hanford Co
Page 331 and 332: Stock Equipment Company 1.0 SUMMARY
Page 333 and 334: Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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T 1 OI 80 70 U 60 VJ w 50 w 0 40 30
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^ °' cn l .:. U CD w a: w r' i ^ I
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SAMPLE ID Li-117 L1-118 L1-19 L3-17
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T °,w ^ - : C s 0 n a ^^ s ^ i ^-
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71 I V y,,} ^ • 5il i ^ ^^ ^ ^ ^
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0 a^ on O O M F- 1OCD 3 1 G N^ U il
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O > W C f.) O O 1-- ^ O HI 6./ 3 ^
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0 > ar oe M 0 c C3, I O c V 3 Î d
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TI V 40 IN s i s : s ^l l i " p p l
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WHC-SD-W100-TI-003 Rev. 0 _QVrDvrru
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^-_- .,:... WHC-SD-W100-TI-003 Rev.
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Ceramics and glass WHC-SD-W200-TI-0
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,. ., Extruder/melter WHC-SD-W100-T
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