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WHC-SD-W100-TI-003 Rev. 0<br />

Waste Form Qualification Testing<br />

Statement of Work W-277587<br />

May 14, 1992<br />

suitable immobilization technologies is a critical element in the completion<br />

of the WRAP 2A conceptual design effort.<br />

3.0 SCOPE OF WORK<br />

The scope of work includes the following work elements:<br />

a.d-- Prepare- a- plan--tc perfarm-all elements of the work described for<br />

approval by WHC prior to the start of work.<br />

3.2 Prepare a quality assurance plan for approval by WHC prior to the<br />

start of work.<br />

3.3 Develop optimum formulations for the immobilization of the<br />

surrogate wastes supplied by WHC.<br />

3.4 Prepare waste form qualification specimens as necessary to<br />

complete all required laboratory tests.<br />

31 5 --Dprform laboratory qualif3caxien testing and analyses of °<br />

immobilized waste forms.<br />

3.6 Support the conceptual design effort for the WRAP 2A polymer<br />

immobilization process facilities.<br />

3.7 Prepare progress reports and a final report to fully document all<br />

development and testing activities associated with this work.<br />

4.0 DESCRIPTION OF TESTING<br />

Thirty-j36j pounds each of the four surrogate waste simulants will be prepared<br />

and furnished by WHC for use in the testing. Table 1 summarizes the<br />

approximate chemical compositions of the surrogate wastes. The surrogates<br />

will be prepared by dissolving the required salts in water and evaporating to<br />

the desired moisture content. A complete description of the procedures used<br />

to prepare the surrogates, and full chemical analysis of each surrogate waste<br />

shal-l-be-supplied-by-WHC,--including-material-safety-data-sheets for all<br />

ingredients used to prepare the surrogates. The surrogate wastes will not<br />

contain any radionuclides.<br />

The contractor shall be responsible for developing the optimum formulation to<br />

be used for preparing the qualification specimens. Qualification testing<br />

specimens shall then be prepared using the optimum formulation for each<br />

surrogate waste type.<br />

A-minimum o-f-ei-ght quaT1firation specimens shall be prepared from each of the<br />

su{-rugat^ wastes suppiied 'ey WHC. All qualification specimens shall be<br />

prepared from a single batch of processed waste. The minimum batch size shall<br />

3<br />

A-4

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