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Stock Equipment Company<br />

WHC-SD-W100-TI-003 Rev. 0<br />

Due to combustible considerations the samples prepared for TCLP<br />

were ground-at-Steck prior to submittal to the contracted<br />

laboratory.<br />

Samples L5 and L9 (Type 2 and Type 4) were spiked with cobalt,<br />

cesium, and strontium. Then casted into 1.5" by 2" cylinders.<br />

An exotherm profile on the prepared samples was obtain.<br />

November 16. 1992<br />

The leachability study was started for surrogate waste Types 2<br />

and 4. The following time points have been pulled:<br />

30 seconds,<br />

2 hour,<br />

5 hour,<br />

-24_hnur,<br />

2 day,<br />

3 day,<br />

4 day, and<br />

5 day.<br />

The 90 day sample will be pulled on February 15, 1993. An<br />

amendment to the original report will follow within a week of<br />

the 90 day leach interval for TYPE 2 and TYPE 4 surrogate waste<br />

streams.<br />

All time points up to and including 5 days have been assayed.<br />

Leachability calculations are in progress.<br />

Samples of surrogate wastes TYPE a. and-TYPE-1_were-successfully<br />

solidified in the alternate polymer, exotherm data was<br />

recorded. The formulations are identical to the one used for<br />

the sample preparation for all the testing. I also have done<br />

an exotherm profile on TYPE 4 surrogate waste.<br />

November 23, 1992<br />

TCLP extraction was started on L3, L5, L7 and L9 samples. The<br />

samples will be assayed for their metals.<br />

F-57<br />

--M@---

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