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WHC-SD-W100-TI-003 Rev. 0 Waste Form Qualification Testing Statement of Work W-277587 May 14, 1992 TABLE 2 Key Process Parameters PARAMETER UNITS Mixer s p eed revolutions p er minute Mixer- p ower watts - Batch wei g ht g rams Batch volume cubic centimeters Curin g exotherm de g rees Centi g rade Waste loadin g wei ht p ercent Matrix chemistry wei ht percent 7 A-8
.^x. --1vHC-SD iii00- T i-003 Rev. 0 Waste Form Qualification Testing Statement of Work W-277587 May 14, 1992 TABLE 3 Immobilized Waste Testing Requirements Waste Form Characteristic Test Method Acce tance Criteria Com pressive Stren gth ASTM D695 Stren g th > 60 p si Leachability Index ANS 16.1 Leach Index > 6 Biodegradation ASTM G21 & G22, No growth, ASTM D695 Stren th > 60 p si Thermal Cycling ASTM B553, Strength > 60 psi after 30 ASTM 0695 thermal c y cles Radiation Stability ASTM D695 Strength > 60 psi after irradiation to 108 rad Immersion ASTM 0695 Strength > 60 psi after 90day water immersion Free Li q uids ANS 55.1 Free li uid < 0.5% Hazardous Characteristics 40 CFR 261 Not ignitible, not corrosive, not reactive Toxicity Characteristics EPA 1311 (TCLP), TCLP leachable constituents €FA 6010 bel ow EPA l imi tsc°' ce' -(")Basin-waste-texit-ctu!stituentzare_AgBa,-Be,-Cd,Cr,_-Cu, Hg, and Ni. LETr' toxic constituents are Cr, Cu, Hg, and Ni. cWEPA limits as described in 40 CFR 268.41, Table CCWE. 8 A-9
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R 2.1 199^ ^.EN GINEERING DATA TRAN
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Date Received% • I INFORMATION RE
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. SUPPORTING DOCUMENT 1. Total Page
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WHC-SD-W100-TI-003 Rev. 0 EXECUTIVE
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WHC-SD-W100-TI-003 Rev. 0 been achi
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Page 25 and 26: 2.1 REGULATORY FRAMEWORK WHC-SD-W10
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Page 57 and 58: 1.0 INTRODUCTION WHC-SD-W100-TI-003
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Page 65 and 66: WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
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Page 69 and 70: Scope WHC-SD-W100-TI-003 Rev. 0 Sup
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Page 73 and 74: WHC-SD-W100-TI-003 Rev. 0 Laborator
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Page 91 and 92: -. LeachantSolution: Specimen Diame
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Page 101 and 102: Date: _ Leachability Time Point Lea
Page 103 and 104: 23 Ninety ( 90) Day Immersion Test
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Page 107 and 108: 25 BIODEGRADATION TEST PROCEDURE St
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Date: WHC-SD-W100-TI-003 Rev. 0 --
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f-^ -- WHC-SD-W100-TI-003 Rev. 0 2.
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^-..., 3•0 ASSAY FOR MEI'ALS 3.1
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
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19 SCOPE AND APPLICATION WHC-SD-W10
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L:^3 ll Q. 4 AA :'ILTEP.S WHC-0-W10
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4_T tJrD o,...Ys j ^,.,. WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 -, Proced
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WHC-SD-W100-TI-003 Rev. 0 Procedure
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(FM WHC-SD-W100-TI-003 Rev. 0 Proce
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C... 6 Wet Waste Sample Contains no
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^..., . ,.y^ h:.r WHC-SD-WI00-Ti-00
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:. WHC-SD-W100-TI-003 Rev. 0 TA3i.E
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^' . WHC-SD-W100-T1-003 Rev. 0 TABL
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^- ^-> ^ C^Jl I I^t ^.: l WHC-St]-W
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c. 03 00 r=3 ^t C^' II 6.0 II Calib
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LY; ^ C=l . ^.^ .^,..,, €:^. MHC-
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.,,_..1 ---^ - - i-•_E ?*^^ Mater
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WHC-SD-W100-TI-003 Rev. 0 Dow Chemi
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WHC-S®-hi1.00-T'.-00?, Rev. Dow Ch
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WHC-SD-W100-TI-003 Rev. 0 Daw M.. u
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^ ^..rYfl VF •UIYb 1 1 AGA GllS.
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CHARACTERIZATION DATA Part A: Overv
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Grit Specie or MaterialOverall Cont
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WHC-SD-W100-TI-003 Rev. 0 The incin
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WHC-SD-W100-TI-003 Rev. 0 183-H BAS
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WHC-SD-W100-TI-003 Rev. 0 June - Se
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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^- WHC-SD-W100-TI-003 Rev. 0 BASIN
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WHC-SD-W100-TI-003 Rev. 0 ---------
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J. L. Westcott Page 3 June 1, 1992
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•N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
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CONTAINER /NFORMATlO N: `d"-C-Sn-'w
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ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
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LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
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LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
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.:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
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LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
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PHYSICAL DESCR/PTTON: V-r-S?-W100-T
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,.: Westinoause Harlford COMM WHC-S
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O I tA SHEETII.XLS ;, LOT WRAP2A.2
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CONTAINER /NFORMAT/ON: DOSE: SIZE:
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PU33-11-1992 09:48 FROM EDS/qRI$ir
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LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
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qN i: 105N-89-1097 105N-89-1098 105
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SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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WHC-SD-W100-TI-003 Rev. 0 Westtngho
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LOT WRAP A2.14 SHEET 18.XLS RECOMME
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---- - LOT WRAP ZA.13 SHEET 17.XLS
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n .-.^..-n..^^- .. ... .dJ. ^ ShIEE
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--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
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WHC-SD-W100-TI-003 Rev. 0 Westingho
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Table 1 Candidate Waste Forms Absor
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--- -Aauaspt and Pe-liroset WHC-SD-
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- '^ - qev. r' Literature Search WR
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Dow Polymer WHC-SD-W100-TI-003 Rev.
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L im e Literature Search WRAP 2A Pa
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The report compares the 7eachabilit
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J. L. Westcott Page 2 May 29, 1992
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Package #1: Package #2: WHC-SD-W100
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WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
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f ..;' WHC-SD-W100-TI-003 Rev. 0 A
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 Bibliogra
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WHC-SD-W100-TI-003 Rev. 0 A. P. Tos
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OAK R1DGE NATIONAL LABORATORY OPERA
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 A report
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WHC-SD-W100-TI-003 Rev. 0 impermeab
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WHC-SD-W100-TI-003 Rev. 0 reprocess
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WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
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Contained under four reports: WHC-S
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^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
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WHC-SD-W100-TI-003 Rev. 0 The techn
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loomi^^lC& 111111111111F .^^.\ West
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û9^c ?fi. ...^ .._-, WHC-SD-W100-T
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Stock Equipment Company WHC-SD-WI00
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^ i w STOCK EOUIPMENT COMPANY 14-OC
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\. . 1 .: lh,lf^ LEACH / IMMERSIONI
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^;- v.4'? Sampls ID L781 Elsment CO
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4.a
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Sanp)a ID L781 Elamant STRONTIUM Ma
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.^ "-; SampI81D L3B2 Z e"- ^.;;. Sa
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Sample 10 L3B1 Elsmant CESIUM Matri
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Sample ID W B1 Elemant STRONIIUM Ma
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Westinghouse Hanford Company 2355 S
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--- - ftCR-e4Uip1P1eFf Company WHC-
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WHC-SD-W100-TI-003 Rev. 0 Russ Czel
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Stock Equipment Company 3:0 -SCFIED
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THERMAL CYCLING SAMPLES BEFORE THE
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BIODEGRADATION SAMPLES BEFORE THE S
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C/ 0D OC M1 0, ^yII i..) d tl ^ a I
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Stock Equipment Company 1.0 SUMMARY
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Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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T 1 OI 80 70 U 60 VJ w 50 w 0 40 30
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WHC-SD-W100-TI-003 Rev. 0 _QVrDvrru
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^-_- .,:... WHC-SD-W100-TI-003 Rev.
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Ceramics and glass WHC-SD-W200-TI-0
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,. ., Extruder/melter WHC-SD-W100-T
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