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WHC-SD-W100-TI-003 Rev. 0 From: Chemical Process Engineering JWB-183H-001 Phone: 6-1778 L5-31 --- Date: .June 25, 1go2 Subject: 183-H Solar Basin Waste Characterization To: J.L. Wescott H2-58 cc: D.A. Burbank H1-60 W.O. Greenhalgh L5-31 J.A. Hunter L5-31 C.A. Petersen H1-60 J.G. Riddelle H2-58 K.M. Weingardt H1-60 E.A. McDaniel ORNL Attached is the "to date" characterization data for the 183-H Basin wastes. With the characterization data is a summary chronology, as best as can be determined, of events involved in the cleanup of the 183-H Basins. The information contained in the attachment was gathered from several sources. The primary source for the characterization data was the 183-H Solar Evaporization Basins Closure/Post-Closure Plan (Rev. 2). Other information was obtained from various letters and field notes generated during the cleanup operations. Since some of the information is 6 to 7 years old it is very difficult to verify any of the information. Therefore, all data should be viewed with some degree of uncertainty. As- more inforrttatien is fourd lt wrl te trammitted as an updaie to this letter. It Biglin D-8
WHC-SD-W100-TI-003 Rev. 0 183-H BASINS CLEANUP CHRONOLOGY Oct 1984 Basin 1 sampled Wet sludge ( inner basin) Dry crystalline ( outer basin) Liquid phase 6-25-92 BASIN 1 SOLID SAMPLES CONTSTITUENTS GREATER THAN 19'. (Table I .A-5 183-H Basin Closu re Plan) ' Inner' Basin 'Outer' Basin Sludge content ( Y) Sludge co ntent (Y.) Constituent A v e ra ge Ranoe Samole 0-0 Samole 0-9 = Sodium 20.0 17.7 - 23.5 20.5 22 . 9 Co;,per -- 11.9* 10.0 - I1.-2 - 5.4 Zirconium 3.2 1.9 - 3.9 1.6 1.8 Flouride ion 6.0 5.4 - 6.4 7.1 6.7 Nitrate ion 8.0 6.1 - 10.4 1.4 1.6 Sulfate ion 20.2 17.7 - 23.5 35.5 32.7 Water ( dried to 105- C) 22.2 18.7 - 24.5 22.8 23.1 Silicon
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R 2.1 199^ ^.EN GINEERING DATA TRAN
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Date Received% • I INFORMATION RE
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. SUPPORTING DOCUMENT 1. Total Page
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WHC-SD-W100-TI-003 Rev. 0 EXECUTIVE
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WHC-SD-W100-TI-003 Rev. 0 been achi
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F`= WHC-SD-W100-TI-003 Rev. 0 DESCR
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WHC-SD-W100-TI-003 Rev. 0 LIST OF T
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WHC-SD-W100-TI-003 Rev. 0 WASTE REC
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WHC-SD-W100-TI-003 Rev. 0 1.2.1 Fee
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^s. WHC-SD-W100-TI-003 Rev. 0 conta
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2.1 REGULATORY FRAMEWORK WHC-SD-W10
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^..." ;_:.. :.^ .^.y^ WHC-SD-W100-T
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WHC-SD-W100-TI-003 Rev. 0 which the
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kIHC-Sû-Wi"v"u-Ti-u03 Rev. V ,--,,
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WHC-SD-W100-TI-003 Rev. 0 Type 1 wa
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3.3 TESTING APPROACH WHC-SD-W100-TI
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^.: fi WNC-SD-W100-TI-003 Rev. 0 Fi
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4.1 SCREENING TEST RESULTS WHC-SD-W
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WHC-SD-W100-TI-003 Rev. 0 4.1.3 The
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p Sam le Compressive Radiation stre
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WHC-SD-W100-TI-003 Rev. 0 Table 4-3
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..., TESTING RESULTS .^.CSSD-W-1OO-
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--- ....ti s..` WHC-SD-WI00-TI-003
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1.0 INTRODUCTION WHC-SD-W100-TI-003
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WHC-SD-W100-TI-003 Rev. 0 Waste For
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^-: -- ^ Component Waste Type 1 LET
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.^x. --1vHC-SD iii00- T i-003 Rev.
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WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
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,..^ c:-- z ,.E ^=t ^^ln^l WHC-SD-W
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Scope WHC-SD-W100-TI-003 Rev. 0 Sup
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00 V F-' Activity and Miltstone Cha
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WHC-SD-W100-TI-003 Rev. 0 Laborator
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WHC-SD-WIOO-TI-003 Rev. 0 APPENDIX
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16490 Chiaccothe Itoad Chagrin Fall
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ca-. tY•^_E Q . - - StoGkE4uip+!n
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^.. WHC-SD-W100-TI-003 Rev. 0 . , I
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Waste Type: WHC-SD-W100-TI-003 Rev.
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Stock E quipment Company A Unit of
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G' ,.,. d,_ s WHC-0-W100-TI-003 Rev
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Cx U: r°... .• , .ti Waste Type:
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-. LeachantSolution: Specimen Diame
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c^1, WHC-SD-W100-TI-003 Rev. 0 THER
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..... lry" - Stock E a uipment Comp
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;=. .:^;. WHC-SD-W100-TI-003 Rev< 0
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(.7 ..^^ -„n f^. [Y^. Waste Type:
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Date: _ Leachability Time Point Lea
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23 Ninety ( 90) Day Immersion Test
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ty ,.. ='`F r...,, b Ly.. Specimen
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25 BIODEGRADATION TEST PROCEDURE St
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Date: WHC-SD-W100-TI-003 Rev. 0 BIO
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^_... ..^^ C:i1 Date: WHC-SD-W100-T
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Date: WHC-SD-W100-TI-003 Rev. 0 --
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f-^ -- WHC-SD-W100-TI-003 Rev. 0 2.
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^-..., 3•0 ASSAY FOR MEI'ALS 3.1
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
Page 125 and 126: WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
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Page 169 and 170: WHC-SD-W100-TI-003 Rev. 0 APPENDIX
Page 171 and 172: CHARACTERIZATION DATA Part A: Overv
Page 173 and 174: Grit Specie or MaterialOverall Cont
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Page 179 and 180: WHC-SD-W100-TI-003 Rev. 0 June - Se
Page 181 and 182: WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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Page 189 and 190: J. L. Westcott Page 3 June 1, 1992
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Page 193 and 194: •N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
Page 195 and 196: CONTAINER /NFORMATlO N: `d"-C-Sn-'w
Page 197 and 198: ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
Page 199 and 200: LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
Page 201 and 202: LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
Page 203 and 204: .:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
Page 205 and 206: LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
Page 207 and 208: PHYSICAL DESCR/PTTON: V-r-S?-W100-T
Page 209 and 210: ,.: Westinoause Harlford COMM WHC-S
Page 211 and 212: O I tA SHEETII.XLS ;, LOT WRAP2A.2
Page 213 and 214: CONTAINER /NFORMAT/ON: DOSE: SIZE:
Page 215 and 216: PU33-11-1992 09:48 FROM EDS/qRI$ir
Page 217 and 218: LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
Page 219 and 220: qN i: 105N-89-1097 105N-89-1098 105
Page 221 and 222: SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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Page 225 and 226: LOT WRAP A2.14 SHEET 18.XLS RECOMME
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---- - LOT WRAP ZA.13 SHEET 17.XLS
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--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
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WHC-SD-W100-TI-003 Rev. 0 Westingho
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Table 1 Candidate Waste Forms Absor
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--- -Aauaspt and Pe-liroset WHC-SD-
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- '^ - qev. r' Literature Search WR
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Dow Polymer WHC-SD-W100-TI-003 Rev.
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L im e Literature Search WRAP 2A Pa
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The report compares the 7eachabilit
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J. L. Westcott Page 2 May 29, 1992
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Package #1: Package #2: WHC-SD-W100
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WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
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f ..;' WHC-SD-W100-TI-003 Rev. 0 A
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WHC-SD-W100-TI-003 Revo 0 Bibliogra
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OAK R1DGE NATIONAL LABORATORY OPERA
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 A report
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WHC-SD-W100-TI-003 Rev. 0 reprocess
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WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
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Contained under four reports: WHC-S
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^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
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WHC-SD-W100-TI-003 Rev. 0 The techn
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Stock Equipment Company WHC-SD-WI00
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\. . 1 .: lh,lf^ LEACH / IMMERSIONI
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Sample 10 L3B1 Elsmant CESIUM Matri
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Sample ID W B1 Elemant STRONIIUM Ma
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Westinghouse Hanford Company 2355 S
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--- - ftCR-e4Uip1P1eFf Company WHC-
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WHC-SD-W100-TI-003 Rev. 0 Russ Czel
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Stock Equipment Company 3:0 -SCFIED
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THERMAL CYCLING SAMPLES BEFORE THE
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BIODEGRADATION SAMPLES BEFORE THE S
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C/ 0D OC M1 0, ^yII i..) d tl ^ a I
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Stock Equipment Company 1.0 SUMMARY
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Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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TI V 40 IN s i s : s ^l l i " p p l
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 _QVrDvrru
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^-_- .,:... WHC-SD-W100-TI-003 Rev.
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Ceramics and glass WHC-SD-W200-TI-0
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,. ., Extruder/melter WHC-SD-W100-T
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