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2.2.4 Stock E q uipment Company A Unit of General Signal Ge,n E499-50-91e6 WHC-SD-W100-TI-003 Rev. 0 PROCEDURE 90110-0 223.7 If the leachant solution contains a precipitate, the entire precipitate will be collected by filtration. The filter paper will be either a Whatman 2 or Whatman 5 qualitative filter paper. The precipitate will be gravity filtered and will not be washed. 223.8 After the filtration step, the precipitate will be oven dried at 50-60'C for at lea.st three (3) hours. The precipitate will then be weighed, the mass of solids determined and recorded on the Leachant Sample Preparation Data Sheet at the end of this section. After weighing, the dried precipitate will be stored in a four (4) ounce polyethylene bottle. The bottle will be tightly capped and labeled with the following information: a. Leach specimen label b. Leachant solution (sea water or distilled water) c. Date and time sample obtained d. Mass of sample 223.9 The filtered leachant solution will then be discarded. Leachability Specimen Compressive Strength Test Upon completion of ninety (90) day leachability testing the leachability - test spe citnens will be com^r•«i ,,. _.... ^.,.. ^ r._ ^sted per Section 2.1 Compressive Strength Test Procedure. Compression test results will be recorded on the Leachability Test Compressive Strength Data Sheet at the end of Section 2.1. C-24 Pa,c I? of? ^ y
(.7 ..^^ -„n f^. [Y^. Waste Type: Solidification Size: Specimen Label: LeaehancSoluuon: YIHC-SD-W100-TI-003 Rev. 0 SPECIMEN DATA SHEET olon PROCEDURE 90110-0 Leachant Heieht (em) Diameter (cm) Surface Area (cmZ) Volume(ml) Time Point Record Additional Observations on Reserve Technician Date Technician Date Stock Equipment Company A Unit of General Signal •a.. s.sa-eo-61ee -C-25 Page 14 of 37
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R 2.1 199^ ^.EN GINEERING DATA TRAN
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Date Received% • I INFORMATION RE
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. SUPPORTING DOCUMENT 1. Total Page
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WHC-SD-W100-TI-003 Rev. 0 EXECUTIVE
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WHC-SD-W100-TI-003 Rev. 0 been achi
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__ _ _ MHC-SIL-yJ3,00-TI-D03 Rev. 0
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F`= WHC-SD-W100-TI-003 Rev. 0 DESCR
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WHC-SD-W100-TI-003 Rev. 0 LIST OF T
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WHC-SD-W100-TI-003 Rev. 0 WASTE REC
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WHC-SD-W100-TI-003 Rev. 0 1.2.1 Fee
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^s. WHC-SD-W100-TI-003 Rev. 0 conta
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__-'°'2 WHC-SD-W100-TI-003 Rev. 0
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2.1 REGULATORY FRAMEWORK WHC-SD-W10
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^..." ;_:.. :.^ .^.y^ WHC-SD-W100-T
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WHC-SD-W100-TI-003 Rev. 0 which the
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kIHC-Sû-Wi"v"u-Ti-u03 Rev. V ,--,,
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WHC-SD-W100-TI-003 Rev. 0 Type 1 wa
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3.3 TESTING APPROACH WHC-SD-W100-TI
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^.: fi WNC-SD-W100-TI-003 Rev. 0 Fi
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4.1 SCREENING TEST RESULTS WHC-SD-W
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,^. ----- -- WHC-SD-W100-TI-003 Rev
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WHC-SD-W100-TI-003 Rev. 0 4.1.3 The
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p Sam le Compressive Radiation stre
Page 47 and 48: WHC-SD-W100-TI-003 Rev. 0 Table 4-3
Page 49 and 50: ..., TESTING RESULTS .^.CSSD-W-1OO-
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Page 53 and 54: ;..;: .^:. WHC-SD-W100-TI-003 Rev.
Page 55 and 56: --- ....ti s..` WHC-SD-WI00-TI-003
Page 57 and 58: 1.0 INTRODUCTION WHC-SD-W100-TI-003
Page 59 and 60: WHC-SD-W100-TI-003 Rev. 0 Waste For
Page 61 and 62: ^-: -- ^ Component Waste Type 1 LET
Page 63 and 64: .^x. --1vHC-SD iii00- T i-003 Rev.
Page 65 and 66: WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
Page 67 and 68: ,..^ c:-- z ,.E ^=t ^^ln^l WHC-SD-W
Page 69 and 70: Scope WHC-SD-W100-TI-003 Rev. 0 Sup
Page 71 and 72: 00 V F-' Activity and Miltstone Cha
Page 73 and 74: WHC-SD-W100-TI-003 Rev. 0 Laborator
Page 75 and 76: WHC-SD-WIOO-TI-003 Rev. 0 APPENDIX
Page 77 and 78: 16490 Chiaccothe Itoad Chagrin Fall
Page 79 and 80: ca-. tY•^_E Q . - - StoGkE4uip+!n
Page 81 and 82: ^.. WHC-SD-W100-TI-003 Rev. 0 . , I
Page 83 and 84: Waste Type: WHC-SD-W100-TI-003 Rev.
Page 85 and 86: Stock E quipment Company A Unit of
Page 87 and 88: G' ,.,. d,_ s WHC-0-W100-TI-003 Rev
Page 89 and 90: Cx U: r°... .• , .ti Waste Type:
Page 91 and 92: -. LeachantSolution: Specimen Diame
Page 93 and 94: c^1, WHC-SD-W100-TI-003 Rev. 0 THER
Page 95 and 96: ..... lry" - Stock E a uipment Comp
Page 97: ;=. .:^;. WHC-SD-W100-TI-003 Rev< 0
Page 101 and 102: Date: _ Leachability Time Point Lea
Page 103 and 104: 23 Ninety ( 90) Day Immersion Test
Page 105 and 106: ty ,.. ='`F r...,, b Ly.. Specimen
Page 107 and 108: 25 BIODEGRADATION TEST PROCEDURE St
Page 109 and 110: Date: WHC-SD-W100-TI-003 Rev. 0 BIO
Page 111 and 112: ^_... ..^^ C:i1 Date: WHC-SD-W100-T
Page 113 and 114: Date: WHC-SD-W100-TI-003 Rev. 0 --
Page 115 and 116: f-^ -- WHC-SD-W100-TI-003 Rev. 0 2.
Page 117 and 118: ^-..., 3•0 ASSAY FOR MEI'ALS 3.1
Page 119 and 120: t..f f....,.. P....^ .-- ^ : .^ ^-.
Page 121 and 122: ^c. v 3 0 w.3 cn a v t[ACeRUtIIY IO
Page 123 and 124: WHC-SD-W100-TI-003 Rev. 0 APPENDIX
Page 125 and 126: WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
Page 127 and 128: 19 SCOPE AND APPLICATION WHC-SD-W10
Page 129 and 130: L:^3 ll Q. 4 AA :'ILTEP.S WHC-0-W10
Page 131 and 132: 4_T tJrD o,...Ys j ^,.,. WHC-SD-W10
Page 133 and 134: WHC-SD-W100-TI-003 Rev. 0 -, Proced
Page 135 and 136: WHC-SD-W100-TI-003 Rev. 0 Procedure
Page 137 and 138: (FM WHC-SD-W100-TI-003 Rev. 0 Proce
Page 139 and 140: C... 6 Wet Waste Sample Contains no
Page 141 and 142: ^..., . ,.y^ h:.r WHC-SD-WI00-Ti-00
Page 143 and 144: :. WHC-SD-W100-TI-003 Rev. 0 TA3i.E
Page 145 and 146: ^' . WHC-SD-W100-T1-003 Rev. 0 TABL
Page 147 and 148: ^- ^-> ^ C^Jl I I^t ^.: l WHC-St]-W
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c. 03 00 r=3 ^t C^' II 6.0 II Calib
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LY; ^ C=l . ^.^ .^,..,, €:^. MHC-
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R: C=1 rIj s^ ^ ^.. WHC-SD-YlI00-TI
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.,,_..1 ---^ - - i-•_E ?*^^ Mater
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WHC-SD-W100-TI-003 Rev. 0 Dow Chemi
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^ ±.£:a [7.p -;^ --- --------- WH
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WHC-S®-hi1.00-T'.-00?, Rev. Dow Ch
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t;7_7 ,...:: ----------- WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 Daw M.. u
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^ ^..rYfl VF •UIYb 1 1 AGA GllS.
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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CHARACTERIZATION DATA Part A: Overv
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Grit Specie or MaterialOverall Cont
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WHC-SD-W100-TI-003 Rev. 0 The incin
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WHC-SD-W100-TI-003 Rev. 0 183-H BAS
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WHC-SD-W100-TI-003 Rev. 0 June - Se
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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^- WHC-SD-W100-TI-003 Rev. 0 BASIN
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WHC-SD-W100-TI-003 Rev. 0 ---------
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J. L. Westcott Page 3 June 1, 1992
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u...^^, WHC-SD-W100-TI-003 Rev. 0 I
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•N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
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CONTAINER /NFORMATlO N: `d"-C-Sn-'w
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ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
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LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
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LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
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.:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
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LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
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PHYSICAL DESCR/PTTON: V-r-S?-W100-T
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,.: Westinoause Harlford COMM WHC-S
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O I tA SHEETII.XLS ;, LOT WRAP2A.2
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CONTAINER /NFORMAT/ON: DOSE: SIZE:
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PU33-11-1992 09:48 FROM EDS/qRI$ir
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LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
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qN i: 105N-89-1097 105N-89-1098 105
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SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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WHC-SD-W100-TI-003 Rev. 0 Westtngho
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LOT WRAP A2.14 SHEET 18.XLS RECOMME
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---- - LOT WRAP ZA.13 SHEET 17.XLS
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n .-.^..-n..^^- .. ... .dJ. ^ ShIEE
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--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
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WHC-SD-W100-TI-003 Rev. 0 Westingho
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Table 1 Candidate Waste Forms Absor
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--- -Aauaspt and Pe-liroset WHC-SD-
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- '^ - qev. r' Literature Search WR
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Dow Polymer WHC-SD-W100-TI-003 Rev.
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L im e Literature Search WRAP 2A Pa
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The report compares the 7eachabilit
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J. L. Westcott Page 2 May 29, 1992
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Package #1: Package #2: WHC-SD-W100
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WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
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f ..;' WHC-SD-W100-TI-003 Rev. 0 A
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 Bibliogra
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WHC-SD-W100-TI-003 Rev. 0 A. P. Tos
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OAK R1DGE NATIONAL LABORATORY OPERA
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 A report
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WHC-SD-W100-TI-003 Rev. 0 impermeab
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WHC-SD-W100-TI-003 Rev. 0 reprocess
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WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
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Contained under four reports: WHC-S
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^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
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WHC-SD-W100-TI-003 Rev. 0 The techn
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loomi^^lC& 111111111111F .^^.\ West
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û9^c ?fi. ...^ .._-, WHC-SD-W100-T
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Stock Equipment Company WHC-SD-WI00
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^ i w STOCK EOUIPMENT COMPANY 14-OC
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\. . 1 .: lh,lf^ LEACH / IMMERSIONI
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^;- v.4'? Sampls ID L781 Elsment CO
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4.a
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Sanp)a ID L781 Elamant STRONTIUM Ma
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.^ "-; SampI81D L3B2 Z e"- ^.;;. Sa
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Sample 10 L3B1 Elsmant CESIUM Matri
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Sample ID W B1 Elemant STRONIIUM Ma
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Westinghouse Hanford Company 2355 S
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--- - ftCR-e4Uip1P1eFf Company WHC-
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WHC-SD-W100-TI-003 Rev. 0 Russ Czel
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Stock Equipment Company 3:0 -SCFIED
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THERMAL CYCLING SAMPLES BEFORE THE
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BIODEGRADATION SAMPLES BEFORE THE S
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C/ 0D OC M1 0, ^yII i..) d tl ^ a I
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T 1 A w ^ • $ ^py yf ; pp V ^ py
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T 1 A ^ !^^ + ^ i •^^w^:rwwwwrpR^
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'i A v lf^. j^^ u e e - - I I I a i
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0 > d C.) O O F- 0 0 3 G NI U 3 ^ c
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en a-. p g aQ i ^ rr it - l r rF e^
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' iO`F*'P\^ Westinghouse Hanford Co
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Stock Equipment Company 1.0 SUMMARY
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Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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T 1 OI 80 70 U 60 VJ w 50 w 0 40 30
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^ °' cn l .:. U CD w a: w r' i ^ I
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SAMPLE ID Li-117 L1-118 L1-19 L3-17
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T °,w ^ - : C s 0 n a ^^ s ^ i ^-
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71 I V y,,} ^ • 5il i ^ ^^ ^ ^ ^
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0 a^ on O O M F- 1OCD 3 1 G N^ U il
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O > W C f.) O O 1-- ^ O HI 6./ 3 ^
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0 > ar oe M 0 c C3, I O c V 3 Î d
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TI V 40 IN s i s : s ^l l i " p p l
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 _QVrDvrru
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^-_- .,:... WHC-SD-W100-TI-003 Rev.
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Ceramics and glass WHC-SD-W200-TI-0
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,. ., Extruder/melter WHC-SD-W100-T
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