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WHC-SD-W100-TI-003 Rev. 0 This page intentionally left blank. C-94
WHC-SD-W100-TI-003 Rev. 0 APPENDIX D CHARACTERIZATION DATA A. An overview of characterization data used in this stage of Waste Form Qua7ification testing. B. Two memos prepared by WHC Chemical Process Engineering Group. The first summarizes the "to date" characterization data on the 183H Basin wastes - the largest volume of the currently stored low level mixed waste types. The second memo describes the recommended waste forms for the various basin wastes and some to the future generated waste streams (LETF and Incinerator Ash). memo i: JBW-183-I701 Memo 2: CPE-WOG-002 C. Four WHC generated Internal Letter Reports reviewing the records of the contents of all currently stored low-level mixed waste at the <strong>Hanford</strong> <strong>Site</strong>. The characterization data and the EPA waste codes were used to group the containers into lots of similar waste types for processing. A technical evaluation was then performed (by a solidification technology expert) as to the best treatment approach for each lot. The rationale for the treatment selection is included. Memo numbers: 87330-92-MLS-023, -025, -026, and -028. D-1
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R 2.1 199^ ^.EN GINEERING DATA TRAN
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Date Received% • I INFORMATION RE
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. SUPPORTING DOCUMENT 1. Total Page
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WHC-SD-W100-TI-003 Rev. 0 EXECUTIVE
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WHC-SD-W100-TI-003 Rev. 0 been achi
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__ _ _ MHC-SIL-yJ3,00-TI-D03 Rev. 0
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F`= WHC-SD-W100-TI-003 Rev. 0 DESCR
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WHC-SD-W100-TI-003 Rev. 0 LIST OF T
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WHC-SD-W100-TI-003 Rev. 0 WASTE REC
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WHC-SD-W100-TI-003 Rev. 0 1.2.1 Fee
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^s. WHC-SD-W100-TI-003 Rev. 0 conta
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__-'°'2 WHC-SD-W100-TI-003 Rev. 0
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2.1 REGULATORY FRAMEWORK WHC-SD-W10
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^..." ;_:.. :.^ .^.y^ WHC-SD-W100-T
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WHC-SD-W100-TI-003 Rev. 0 which the
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kIHC-Sû-Wi"v"u-Ti-u03 Rev. V ,--,,
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WHC-SD-W100-TI-003 Rev. 0 Type 1 wa
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3.3 TESTING APPROACH WHC-SD-W100-TI
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^.: fi WNC-SD-W100-TI-003 Rev. 0 Fi
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4.1 SCREENING TEST RESULTS WHC-SD-W
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,^. ----- -- WHC-SD-W100-TI-003 Rev
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WHC-SD-W100-TI-003 Rev. 0 4.1.3 The
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p Sam le Compressive Radiation stre
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WHC-SD-W100-TI-003 Rev. 0 Table 4-3
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..., TESTING RESULTS .^.CSSD-W-1OO-
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;..;: .^:. WHC-SD-W100-TI-003 Rev.
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--- ....ti s..` WHC-SD-WI00-TI-003
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1.0 INTRODUCTION WHC-SD-W100-TI-003
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WHC-SD-W100-TI-003 Rev. 0 Waste For
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^-: -- ^ Component Waste Type 1 LET
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.^x. --1vHC-SD iii00- T i-003 Rev.
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WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
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,..^ c:-- z ,.E ^=t ^^ln^l WHC-SD-W
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Scope WHC-SD-W100-TI-003 Rev. 0 Sup
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00 V F-' Activity and Miltstone Cha
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WHC-SD-W100-TI-003 Rev. 0 Laborator
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WHC-SD-WIOO-TI-003 Rev. 0 APPENDIX
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16490 Chiaccothe Itoad Chagrin Fall
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ca-. tY•^_E Q . - - StoGkE4uip+!n
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^.. WHC-SD-W100-TI-003 Rev. 0 . , I
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Waste Type: WHC-SD-W100-TI-003 Rev.
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Stock E quipment Company A Unit of
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G' ,.,. d,_ s WHC-0-W100-TI-003 Rev
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Cx U: r°... .• , .ti Waste Type:
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-. LeachantSolution: Specimen Diame
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c^1, WHC-SD-W100-TI-003 Rev. 0 THER
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..... lry" - Stock E a uipment Comp
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;=. .:^;. WHC-SD-W100-TI-003 Rev< 0
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(.7 ..^^ -„n f^. [Y^. Waste Type:
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Date: _ Leachability Time Point Lea
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23 Ninety ( 90) Day Immersion Test
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ty ,.. ='`F r...,, b Ly.. Specimen
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25 BIODEGRADATION TEST PROCEDURE St
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Date: WHC-SD-W100-TI-003 Rev. 0 BIO
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^_... ..^^ C:i1 Date: WHC-SD-W100-T
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Date: WHC-SD-W100-TI-003 Rev. 0 --
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f-^ -- WHC-SD-W100-TI-003 Rev. 0 2.
Page 117 and 118: ^-..., 3•0 ASSAY FOR MEI'ALS 3.1
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Page 121 and 122: ^c. v 3 0 w.3 cn a v t[ACeRUtIIY IO
Page 123 and 124: WHC-SD-W100-TI-003 Rev. 0 APPENDIX
Page 125 and 126: WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
Page 127 and 128: 19 SCOPE AND APPLICATION WHC-SD-W10
Page 129 and 130: L:^3 ll Q. 4 AA :'ILTEP.S WHC-0-W10
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Page 133 and 134: WHC-SD-W100-TI-003 Rev. 0 -, Proced
Page 135 and 136: WHC-SD-W100-TI-003 Rev. 0 Procedure
Page 137 and 138: (FM WHC-SD-W100-TI-003 Rev. 0 Proce
Page 139 and 140: C... 6 Wet Waste Sample Contains no
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Page 143 and 144: :. WHC-SD-W100-TI-003 Rev. 0 TA3i.E
Page 145 and 146: ^' . WHC-SD-W100-T1-003 Rev. 0 TABL
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Page 149 and 150: c. 03 00 r=3 ^t C^' II 6.0 II Calib
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Page 153 and 154: R: C=1 rIj s^ ^ ^.. WHC-SD-YlI00-TI
Page 155 and 156: .,,_..1 ---^ - - i-•_E ?*^^ Mater
Page 157 and 158: WHC-SD-W100-TI-003 Rev. 0 Dow Chemi
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Page 161 and 162: WHC-S®-hi1.00-T'.-00?, Rev. Dow Ch
Page 163 and 164: t;7_7 ,...:: ----------- WHC-SD-W10
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Page 167: ^ ^..rYfl VF •UIYb 1 1 AGA GllS.
Page 171 and 172: CHARACTERIZATION DATA Part A: Overv
Page 173 and 174: Grit Specie or MaterialOverall Cont
Page 175 and 176: WHC-SD-W100-TI-003 Rev. 0 The incin
Page 177 and 178: WHC-SD-W100-TI-003 Rev. 0 183-H BAS
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Page 181 and 182: WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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Page 189 and 190: J. L. Westcott Page 3 June 1, 1992
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Page 193 and 194: •N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
Page 195 and 196: CONTAINER /NFORMATlO N: `d"-C-Sn-'w
Page 197 and 198: ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
Page 199 and 200: LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
Page 201 and 202: LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
Page 203 and 204: .:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
Page 205 and 206: LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
Page 207 and 208: PHYSICAL DESCR/PTTON: V-r-S?-W100-T
Page 209 and 210: ,.: Westinoause Harlford COMM WHC-S
Page 211 and 212: O I tA SHEETII.XLS ;, LOT WRAP2A.2
Page 213 and 214: CONTAINER /NFORMAT/ON: DOSE: SIZE:
Page 215 and 216: PU33-11-1992 09:48 FROM EDS/qRI$ir
Page 217 and 218: LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
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qN i: 105N-89-1097 105N-89-1098 105
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SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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WHC-SD-W100-TI-003 Rev. 0 Westtngho
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LOT WRAP A2.14 SHEET 18.XLS RECOMME
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---- - LOT WRAP ZA.13 SHEET 17.XLS
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--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
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WHC-SD-W100-TI-003 Rev. 0 Westingho
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Table 1 Candidate Waste Forms Absor
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--- -Aauaspt and Pe-liroset WHC-SD-
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- '^ - qev. r' Literature Search WR
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Dow Polymer WHC-SD-W100-TI-003 Rev.
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L im e Literature Search WRAP 2A Pa
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The report compares the 7eachabilit
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J. L. Westcott Page 2 May 29, 1992
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Package #1: Package #2: WHC-SD-W100
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WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
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f ..;' WHC-SD-W100-TI-003 Rev. 0 A
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 Bibliogra
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WHC-SD-W100-TI-003 Rev. 0 A. P. Tos
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OAK R1DGE NATIONAL LABORATORY OPERA
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 A report
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WHC-SD-W100-TI-003 Rev. 0 impermeab
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WHC-SD-W100-TI-003 Rev. 0 reprocess
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WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
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Contained under four reports: WHC-S
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^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
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WHC-SD-W100-TI-003 Rev. 0 The techn
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loomi^^lC& 111111111111F .^^.\ West
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Stock Equipment Company WHC-SD-WI00
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^ i w STOCK EOUIPMENT COMPANY 14-OC
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\. . 1 .: lh,lf^ LEACH / IMMERSIONI
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^;- v.4'? Sampls ID L781 Elsment CO
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4.a
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Sanp)a ID L781 Elamant STRONTIUM Ma
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.^ "-; SampI81D L3B2 Z e"- ^.;;. Sa
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Sample 10 L3B1 Elsmant CESIUM Matri
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Sample ID W B1 Elemant STRONIIUM Ma
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Westinghouse Hanford Company 2355 S
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--- - ftCR-e4Uip1P1eFf Company WHC-
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WHC-SD-W100-TI-003 Rev. 0 Russ Czel
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Stock Equipment Company 3:0 -SCFIED
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THERMAL CYCLING SAMPLES BEFORE THE
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BIODEGRADATION SAMPLES BEFORE THE S
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' iO`F*'P\^ Westinghouse Hanford Co
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Stock Equipment Company 1.0 SUMMARY
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Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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T 1 OI 80 70 U 60 VJ w 50 w 0 40 30
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SAMPLE ID Li-117 L1-118 L1-19 L3-17
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TI V 40 IN s i s : s ^l l i " p p l
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 _QVrDvrru
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^-_- .,:... WHC-SD-W100-TI-003 Rev.
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Ceramics and glass WHC-SD-W200-TI-0
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,. ., Extruder/melter WHC-SD-W100-T
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