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RESULTS Compressive Strengths Wi1C-SD-W100-TI-003 Rev. 0 The first set of waste forms tested were 5 cm by 5 cm by 5 cm (2 in. by 2 in. by 2 in.) cubes. The compressive strength tests were performed on two cube samples for each waste type. The first cube for each waste type was tested after 14 days of curing, the second cube for each waste type was tested after 28 days of curing. The results are shown on Table 4-1. 3he second-set of waste forms were small cyiinders, 15 cm ( 6 in.) high with a 7.6-cm ( 3-in.) diameter. The cylinders were allowed to cure for 28 days before the compressive strength tests were performed. The small cylinder results are shown in Table 4-2. Sample Solidifier Typ e 5 Type 5 Portland ^ype Iii Table 4-1. WRAP 2A Waste Form Characteristics. Compressive strength Dens ity F ree li qu id (g/cc) (vol.%) 14 day 28 day (lbf/inZ) (lbf/in 2) Portland Type I and II 2.5 0 2.5 - ------ 0------ 6,800 5,000 4,600 5,600 ( 28d) (42d) Slag Type 6 Cement/portland 2.4 0 3,800 3,000 Type III Type , Portland Type III 1.7 0 1,000 1,300 Siag . . Type 8- Cement/portland - 1.7 0 3,100 1,800 Type III I Type 1 Environstone* I 1.5 2.6 at 1 day 1.6 at 2 day 0.0 at 3 day (Liquid oH_is 6) 70 60 - *Envirostone is a trademar o t e United States Gvosum Comoanv_ 4-6
p Sam le Compressive Radiation strength stability Small Large Compressive cylinder (l bf / i n 2 ) cylinder ( lbf /in `^ ) strength ( lbf/in 2 ) ^ _"' . ^ws{ J 7' Table 4-2. WRAP 2A Cement Waste Form Tests Results. Biodegradation Compressive strength (sample/control) (lbf/in ) h Was e immersion Thermal cycling Compressive strength Leachability Index 14d (lbf/in) 42d 90d C ompress iv e strength / Z) (lbf in Control 7,400 4,500 -- -- -- - - Type 5 7,100 5,400 8,500/9,100 Type 6 3,500 4,200 3,800/4,800 Type 7 2,800 2,100 2,500/2,000 Type 8 3,400 2,400 4,100/3,900 Type 1 50 9.9 (Ce) No data (Sr) 8900 3900 8400 5500/8000 5300 2600 5500 4000/4400 2400 1100 3000 2200/2400 3900 2500 4380 2900/3100 Failed
Page 1 and 2: R 2.1 199^ ^.EN GINEERING DATA TRAN
Page 3 and 4: Date Received% • I INFORMATION RE
Page 5 and 6: . SUPPORTING DOCUMENT 1. Total Page
Page 7 and 8: WHC-SD-W100-TI-003 Rev. 0 EXECUTIVE
Page 9 and 10: WHC-SD-W100-TI-003 Rev. 0 been achi
Page 11 and 12: __ _ _ MHC-SIL-yJ3,00-TI-D03 Rev. 0
Page 13 and 14: F`= WHC-SD-W100-TI-003 Rev. 0 DESCR
Page 15 and 16: WHC-SD-W100-TI-003 Rev. 0 LIST OF T
Page 17 and 18: WHC-SD-W100-TI-003 Rev. 0 WASTE REC
Page 19 and 20: WHC-SD-W100-TI-003 Rev. 0 1.2.1 Fee
Page 21 and 22: ^s. WHC-SD-W100-TI-003 Rev. 0 conta
Page 23 and 24: __-'°'2 WHC-SD-W100-TI-003 Rev. 0
Page 25 and 26: 2.1 REGULATORY FRAMEWORK WHC-SD-W10
Page 27 and 28: ^..." ;_:.. :.^ .^.y^ WHC-SD-W100-T
Page 29 and 30: WHC-SD-W100-TI-003 Rev. 0 which the
Page 31 and 32: kIHC-Sû-Wi"v"u-Ti-u03 Rev. V ,--,,
Page 33 and 34: WHC-SD-W100-TI-003 Rev. 0 Type 1 wa
Page 35 and 36: 3.3 TESTING APPROACH WHC-SD-W100-TI
Page 37 and 38: ^.: fi WNC-SD-W100-TI-003 Rev. 0 Fi
Page 39 and 40: 4.1 SCREENING TEST RESULTS WHC-SD-W
Page 41 and 42: ,^. ----- -- WHC-SD-W100-TI-003 Rev
Page 43: WHC-SD-W100-TI-003 Rev. 0 4.1.3 The
Page 47 and 48: WHC-SD-W100-TI-003 Rev. 0 Table 4-3
Page 49 and 50: ..., TESTING RESULTS .^.CSSD-W-1OO-
Page 51 and 52: A I w ^^',; ^^ ;J ?1Fasf^.}: "q -?
Page 53 and 54: ;..;: .^:. WHC-SD-W100-TI-003 Rev.
Page 55 and 56: --- ....ti s..` WHC-SD-WI00-TI-003
Page 57 and 58: 1.0 INTRODUCTION WHC-SD-W100-TI-003
Page 59 and 60: WHC-SD-W100-TI-003 Rev. 0 Waste For
Page 61 and 62: ^-: -- ^ Component Waste Type 1 LET
Page 63 and 64: .^x. --1vHC-SD iii00- T i-003 Rev.
Page 65 and 66: WHC-SD-W: JV-TI-VVJ ^cv. v APPENDIX
Page 67 and 68: ,..^ c:-- z ,.E ^=t ^^ln^l WHC-SD-W
Page 69 and 70: Scope WHC-SD-W100-TI-003 Rev. 0 Sup
Page 71 and 72: 00 V F-' Activity and Miltstone Cha
Page 73 and 74: WHC-SD-W100-TI-003 Rev. 0 Laborator
Page 75 and 76: WHC-SD-WIOO-TI-003 Rev. 0 APPENDIX
Page 77 and 78: 16490 Chiaccothe Itoad Chagrin Fall
Page 79 and 80: ca-. tY•^_E Q . - - StoGkE4uip+!n
Page 81 and 82: ^.. WHC-SD-W100-TI-003 Rev. 0 . , I
Page 83 and 84: Waste Type: WHC-SD-W100-TI-003 Rev.
Page 85 and 86: Stock E quipment Company A Unit of
Page 87 and 88: G' ,.,. d,_ s WHC-0-W100-TI-003 Rev
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Page 91 and 92: -. LeachantSolution: Specimen Diame
Page 93 and 94: c^1, WHC-SD-W100-TI-003 Rev. 0 THER
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..... lry" - Stock E a uipment Comp
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;=. .:^;. WHC-SD-W100-TI-003 Rev< 0
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(.7 ..^^ -„n f^. [Y^. Waste Type:
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Date: _ Leachability Time Point Lea
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23 Ninety ( 90) Day Immersion Test
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ty ,.. ='`F r...,, b Ly.. Specimen
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25 BIODEGRADATION TEST PROCEDURE St
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Date: WHC-SD-W100-TI-003 Rev. 0 BIO
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^_... ..^^ C:i1 Date: WHC-SD-W100-T
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Date: WHC-SD-W100-TI-003 Rev. 0 --
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f-^ -- WHC-SD-W100-TI-003 Rev. 0 2.
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^-..., 3•0 ASSAY FOR MEI'ALS 3.1
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^c. v 3 0 w.3 cn a v t[ACeRUtIIY IO
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WHC-SD-W100-TI-003 Rev. 0 APPENDIX
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WHC-SD-W100-TI-003 Rev. 0 STOCK EQU
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19 SCOPE AND APPLICATION WHC-SD-W10
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L:^3 ll Q. 4 AA :'ILTEP.S WHC-0-W10
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4_T tJrD o,...Ys j ^,.,. WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 -, Proced
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WHC-SD-W100-TI-003 Rev. 0 Procedure
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(FM WHC-SD-W100-TI-003 Rev. 0 Proce
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C... 6 Wet Waste Sample Contains no
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^..., . ,.y^ h:.r WHC-SD-WI00-Ti-00
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:. WHC-SD-W100-TI-003 Rev. 0 TA3i.E
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^' . WHC-SD-W100-T1-003 Rev. 0 TABL
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^- ^-> ^ C^Jl I I^t ^.: l WHC-St]-W
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c. 03 00 r=3 ^t C^' II 6.0 II Calib
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LY; ^ C=l . ^.^ .^,..,, €:^. MHC-
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R: C=1 rIj s^ ^ ^.. WHC-SD-YlI00-TI
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.,,_..1 ---^ - - i-•_E ?*^^ Mater
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WHC-SD-W100-TI-003 Rev. 0 Dow Chemi
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WHC-S®-hi1.00-T'.-00?, Rev. Dow Ch
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t;7_7 ,...:: ----------- WHC-SD-W10
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WHC-SD-W100-TI-003 Rev. 0 Daw M.. u
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^ ^..rYfl VF •UIYb 1 1 AGA GllS.
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CHARACTERIZATION DATA Part A: Overv
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Grit Specie or MaterialOverall Cont
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WHC-SD-W100-TI-003 Rev. 0 The incin
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WHC-SD-W100-TI-003 Rev. 0 183-H BAS
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WHC-SD-W100-TI-003 Rev. 0 June - Se
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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WHC-SD-W100-TI-003 Rev. 0 BASINS 3
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^- WHC-SD-W100-TI-003 Rev. 0 BASIN
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WHC-SD-W100-TI-003 Rev. 0 ---------
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J. L. Westcott Page 3 June 1, 1992
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u...^^, WHC-SD-W100-TI-003 Rev. 0 I
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•N`^C-Sf1-"d100-71-003 Rev. 0 ,S'
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CONTAINER /NFORMATlO N: `d"-C-Sn-'w
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ONTANVER BVFORMA SI7 E: AMOUN=i 8 G
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LOT WRAP 2A.4 SHEET 7.XLS RECOMMEND
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LOT WRAP 2A.5 SHEET 8.XLS RECOMMEND
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.:•n-,,, LOT WRAP 2A.6 SHEET 9.XL
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LOT WRAP 2A.7 SHEET 10.XLS RECOMMEN
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PHYSICAL DESCR/PTTON: V-r-S?-W100-T
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,.: Westinoause Harlford COMM WHC-S
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O I tA SHEETII.XLS ;, LOT WRAP2A.2
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CONTAINER /NFORMAT/ON: DOSE: SIZE:
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PU33-11-1992 09:48 FROM EDS/qRI$ir
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LOT WRAP 2A 10 Slf-EET 14.)C,S RECO
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qN i: 105N-89-1097 105N-89-1098 105
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SIZE: DOSE: 5 GAL 1 1@15 Mr 30 GAL
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WHC-SD-W100-TI-003 Rev. 0 Westtngho
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LOT WRAP A2.14 SHEET 18.XLS RECOMME
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---- - LOT WRAP ZA.13 SHEET 17.XLS
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n .-.^..-n..^^- .. ... .dJ. ^ ShIEE
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--^ WHC-SD-W100-TI-003 Rev. 0 APPEN
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WHC-SD-W100-TI-003 Rev. 0 Westingho
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Table 1 Candidate Waste Forms Absor
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--- -Aauaspt and Pe-liroset WHC-SD-
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- '^ - qev. r' Literature Search WR
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Dow Polymer WHC-SD-W100-TI-003 Rev.
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L im e Literature Search WRAP 2A Pa
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The report compares the 7eachabilit
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J. L. Westcott Page 2 May 29, 1992
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Package #1: Package #2: WHC-SD-W100
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WHC-SD-W100-TI-003 Rev. 0 SURVEY OF
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f ..;' WHC-SD-W100-TI-003 Rev. 0 A
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 Bibliogra
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WHC-SD-W100-TI-003 Rev. 0 A. P. Tos
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OAK R1DGE NATIONAL LABORATORY OPERA
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WHC-SD-W100-TI-003 Rev. 0 commercia
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WHC-SD-W100-TI-003 Revo 0 A report
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WHC-SD-W100-TI-003 Rev. 0 impermeab
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WHC-SD-W100-TI-003 Rev. 0 reprocess
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WHC-SD-W100-TI-003 Rev. 0 STR?.THGI
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Contained under four reports: WHC-S
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^.yo F-SD-W"00-7-003 Rev. 0 THERMOS
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WHC-SD-W100-TI-003 Rev. 0 The techn
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loomi^^lC& 111111111111F .^^.\ West
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û9^c ?fi. ...^ .._-, WHC-SD-W100-T
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Stock Equipment Company WHC-SD-WI00
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^ i w STOCK EOUIPMENT COMPANY 14-OC
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\. . 1 .: lh,lf^ LEACH / IMMERSIONI
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^;- v.4'? Sampls ID L781 Elsment CO
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4.a
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Sanp)a ID L781 Elamant STRONTIUM Ma
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.^ "-; SampI81D L3B2 Z e"- ^.;;. Sa
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Sample 10 L3B1 Elsmant CESIUM Matri
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Sample ID W B1 Elemant STRONIIUM Ma
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Westinghouse Hanford Company 2355 S
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--- - ftCR-e4Uip1P1eFf Company WHC-
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WHC-SD-W100-TI-003 Rev. 0 Russ Czel
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Stock Equipment Company 3:0 -SCFIED
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THERMAL CYCLING SAMPLES BEFORE THE
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BIODEGRADATION SAMPLES BEFORE THE S
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C/ 0D OC M1 0, ^yII i..) d tl ^ a I
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T 1 A w ^ • $ ^py yf ; pp V ^ py
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en a-. p g aQ i ^ rr it - l r rF e^
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' iO`F*'P\^ Westinghouse Hanford Co
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Stock Equipment Company 1.0 SUMMARY
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Stock Equipment Company WHC-SD-W100
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2a0 SCHEDULE Activitv - Prepare Wor
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T 1 o+ THERMAL CYCLWG SAMPLES BEFOR
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T 1 OI 80 70 U 60 VJ w 50 w 0 40 30
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^ °' cn l .:. U CD w a: w r' i ^ I
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SAMPLE ID Li-117 L1-118 L1-19 L3-17
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TI V 40 IN s i s : s ^l l i " p p l
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WHC-SD-W100-TI-003 Rev. 0 _QVrDvrru
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^-_- .,:... WHC-SD-W100-TI-003 Rev.
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Ceramics and glass WHC-SD-W200-TI-0
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,. ., Extruder/melter WHC-SD-W100-T
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