02.04.2013 Views

Science of Water : Concepts and Applications

Science of Water : Concepts and Applications

Science of Water : Concepts and Applications

SHOW MORE
SHOW LESS

Create successful ePaper yourself

Turn your PDF publications into a flip-book with our unique Google optimized e-Paper software.

Environmental Biomonitoring, Sampling, <strong>and</strong> Testing 257<br />

Mixer switch<br />

Probe body<br />

Mixer<br />

FIGURE 8.15 Dissolved oxygen-lab probe.<br />

Cable to meter<br />

Membrane<br />

Temperature sensor<br />

methods available for calibration: saturated water, saturated air, <strong>and</strong> the Winkler method. It is<br />

important to note that if the Winkler method is not used for routine calibration method, periodic<br />

checks using this method are recommended.<br />

Procedure<br />

It is important to keep in mind that the meter <strong>and</strong> probe supplier’s operating procedures should<br />

always be followed. Normally, the manufacturer’s recommended procedure will include the following<br />

generalized steps:<br />

1. Turn the DO meter on, <strong>and</strong> allow 15 min for it to warm up.<br />

2. Turn the meter switch to zero, <strong>and</strong> adjust as needed.<br />

3. Calibrate the meter using the saturated air, saturated water, or Winkler azide procedure for<br />

calibration.<br />

4. Collect the sample in a 300-mL bottle, or place the fi eld electrode directly in the stream.<br />

5. Place the laboratory electrode in a BOD bottle without trapping air against the membrane,<br />

<strong>and</strong> turn on the stirrer.<br />

6. Turn the meter switch to temperature setting, <strong>and</strong> measure temperature.<br />

7. Turn the meter switch to DO mode, <strong>and</strong> allow 10 s for the meter reading to stabilize.<br />

8. Read the DO mg/L from meter, <strong>and</strong> record the results.<br />

No calculation is necessary using this method because results are read directly from the meter.<br />

DO meters are expensive compared to fi eld kits that use the titration method. Meter/probe combinations<br />

run between $500 <strong>and</strong> $1200, including a long cable to connect the probe to the meter.

Hooray! Your file is uploaded and ready to be published.

Saved successfully!

Ooh no, something went wrong!