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OP-II-4WATER2METH1STEAM2AOFF3AIR10OFF2HX5HEAT XOFF3EVAP1HEATXOFF4WATERSPLIT1WATER1EVAP2STEAM1MIX1FEED1METH2BURN2RGIBBSMIX2AIR3AIR9HEATERHX1Q2AIR4AIR2OFF1Q5BURN1AIR6HEATXFEED2REFRGIBBSREF1HX2HEAT XHX3HEAT E RAIR1RGIBBSAIR7SPLIT2AIR5REF2Q3WGSAIR8RGIBBSREF3COFF2METHAOFF2QAIR11RST OICQ4HX6HEATERQWASTESPLIT3REF4AOFF1H2AFCSEPREF5HX4HEAT XCFCRGIBBSQ1AIR12QELQReferencesFig. 1. ASPEN model of the integrated methane fuel processor.[1] G. Kolb, Fuel Processing for Fuel Cells, Wiley-VCH, Weinheim, 2008.[2] S. Springmann, M. Bohnet, M. Sommer, M. Himmen, G. Eigenberger, Steady-state and dynamic simulationof an autothermal gasoline reformer, Chem. Eng. Technol. 26 (2003) 790-796.[3] S. Springmann, M. Bohnet, A. Docter, A. Lamm, G. Eigenberger, Cold start simulations of a gasoline basedfuel processor for mobile fuel cell applications, J. Power Sources 128 (2004) 13-24.[4] H. Aoki, H. Mitsui, T. Shimazu, K. Kimura, T. Masui, A numerical study on thermal efficiency of fuel cellsystems combined with reformer, in: H. Aoki, H. Mitsui, T. Shimazu, K. Kimura, T. Masui (eds.), 16thWorld Hydrogen Energy Conference, 2006, Lyon, France, 1-10.[5] Y.-H. Chen, C.-C. Yu, Y.-C. Liu, C.-H. Lee, Start-up strategies of an experimental fuel processor, J. PowerSources 160 (2006) 1275-1286.[6] T. Baier, G. Kolb, Temperature control of the water-gas shift reaction in microstructured reactors, Chem.Eng. Sci. 62 (2007) 4602-4611.[7] Y. Men, G. Kolb, R. Zapf, V. Hessel, H. Löwe, Selective methanation of carbon oxides in a microchannelreactor – primary screening and impact of oxygen additive Catal. Today 125 (2007) 81-87.COFF182
MONITORING OF THE PROGRESS OF AN EXOTHERMICCATALYTIC REACTION IN A TRICKLE BED REACTOR:AN NMR IMAGING STUDYA.A. Lysova 1,2 , I.V. Koptyug 1 , A.V. Kulikov 2 , V.A. Kirillov 2OP-II-51 International Tomography Center SB RAS, str. Institutskaya 3A, Novosibirsk, Russia 630090,fax: +7 383 3333561, e-mail: lysova@tomo.nsc.ru;2 Boreskov Institute of Catalysis SB RAS, pr. Ac. Lavrent’eva 5, Novosibirsk, Russia 630090,e-mail: V.A.Kirillov@catalysis.nsk.suTrickle bed reactors (TBRs) are generally fixed bed catalytic reactors with the cocurrentflow of gas and liquid. The main application of TBRs lies in the petroleum refining industry.The different hydrodynamics, mass transfer and heat transfer parameters influence theperformance of TBR. The experimental data concerning the bed structure, the peculiarities ofgas and liquid flows, the reagent and product concentrations, temperatures, liquid hold-up,mass and heat transfer, wetting efficiency, etc., necessary for modeling of TBRs andenhancing of their performance can be obtained by a modern technique – NMR imaging(MRI).In this work MRI was applied to monitor the progress of an exothermic catalytic reactioncarried out in the TBR. It was shown that the occurrence of the exothermic catalytic reactioninfluenced the distribution of the liquid phase inside an individual catalyst pellet. Moreover,under certain conditions the oscillations of the liquid phase content inside the individualcatalyst pellet and the reciprocating motion of the front of the liquid phase propagation intothe pellet were observed and modeled. The experimental results showed a good agreementwith the results of the mathematical modeling and confirmed that the differences in the ratesof the heat and mass transfer processes and catalytic reaction are responsible for the observedoscillatory behavior of the individual catalyst pellet operation.A special set of the MRI experiments performed on the catalyst bed during the progress ofthe hydrogenation reaction showed that the proceeding of the hydrogenation reactioninfluenced very much the distribution of the liquid phase in the catalyst bed as well. It wasshown that in the absence of the hydrogenation reaction the distribution of the liquid phase inthe bed was uniform at the very low rates of the liquid reagent supply and even underconditions of the total absence of the liquid reagent supply. When the flow of hydrogen wassupplied to the catalyst bed, the bed started drying, when the rate of the liquid reagent supplywas still sufficiently high, and the distribution of the liquid phase in the catalyst bed becamenon-uniform. At the lower rate of the liquid reagent supply the catalyst bed became83
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Boreskov Institute of Catalysis of
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Mikhail G. Slinko,Honour ChairmanVa
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PLENARY LECTURES
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PL-1built up from an intrinsic cont
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PL-3DEVELOPMENT OF ZEOLITE-COATED M
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PL-4processes in order to evaluate
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PL-5CATALYTIC PARTIAL OXIDATION OF
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KEY-NOTE PRESENTATIONS
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KN-2GETTING TO THE POINT: FROM MOLE
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KN-3PROBLEMS AND PROSPECTS FOR IMRO
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KN-4remain out of the sight of rese
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KN-5SSITKA allows to study not only
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KN-6individual reaction stages with
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Section 1.Kinetics of catalytic rea
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OP-I-1-specialthat Г s /f changed
Page 32 and 33: OP-I-3-specialKINETIC MODELING OF L
Page 34 and 35: OP-I-4PARTIAL OXIDATION OF TOLUENE
Page 36 and 37: OP-I-5Also, the approach to modelin
Page 38 and 39: OP-I-6starch granules, but after a
Page 40 and 41: OP-I-8KINETICS OF CARBON MONOXIDE O
Page 42 and 43: OP-I-9CHAOTIC DYNAMICS IN THE THREE
Page 44 and 45: OP-I-10ADSORPTION OF COMPLEX MOLECU
Page 46 and 47: OP-I-11KINETIC ASPECTS OF METHANE O
Page 48 and 49: OP-I-12KINETIC STUDIES IN STRUCTURE
Page 50 and 51: OP-I-13A STUDY ON THERMAL COMBUSTIO
Page 52 and 53: OP-I-14KINETICS OF THE CONVERSION O
Page 54 and 55: OP-I-15HYDROCRACKING OF LONG CHAIN
Page 56 and 57: OP-I-16KINETICS IN THE HYDROGENATIO
Page 58 and 59: OP-I-17MECHANISM OF FORMATION OF ET
Page 60 and 61: OP-I-18KINETIC STUDIES OF PROPANE D
Page 62 and 63: OP-I-19ACTIVITY AND DEACTIVATION OF
Page 64 and 65: OP-I-20GAS PHASE OXIDATION OF FORMA
Page 66 and 67: OP-I-21Where k A is the rate consta
Page 68 and 69: OP-I-22al., 2008; Monolith, 2008).
Page 70 and 71: OP-I-23Fig. 1. Scheme of the FIM ma
Page 72 and 73: OP-I-24Θ DZ centersdeactivationr D
Page 74 and 75: OP-I-25equation [2] to nitrogen iso
Page 76 and 77: OP-II-1CHEMICAL NANOREACTORS AS BAS
Page 78 and 79: OP-II-2gas model use, there is no n
Page 80 and 81: OP-II-3Taking into account these pr
Page 84 and 85: OP-II-5completely dry, at the same
Page 86 and 87: OP-II-6Many factors have been found
Page 88 and 89: OP-II-7mechanistic and kinetic stud
Page 90 and 91: OP-II-9MODELLING OF DIESEL PARTICUL
Page 92 and 93: Section 3.Catalytic processesí dev
Page 94 and 95: OP-III-1BIC’s catalyst for N 2 О
Page 96 and 97: OP-III-2powder sample with the same
Page 98 and 99: OP-III-3Analysis of the results sho
Page 100 and 101: OP-III-4Exhaustaftertreatmenttechno
Page 102 and 103: OP-III-6SOME PROPERTIES OF PEROVSKI
Page 104 and 105: OP-III-7with the conventional react
Page 106 and 107: OP-III-8resistance is the membrane
Page 108 and 109: OP-III-9mass dispersion and to anal
Page 110 and 111: OP-III-11PROCESS INTENSIFICATION US
Page 112 and 113: OP-III-12ETHYL ACETATE SYNTHESIS BY
Page 114 and 115: OP-III-12products are vaporized and
Page 116 and 117: OP-III-13The reforming reaction was
Page 118 and 119: OP-III-14reactivity (compared to ot
Page 120 and 121: OP-III-15Fig. 2. The spent Smopex-1
Page 122 and 123: OP-III-16Numbers of curves are acco
Page 124 and 125: OP-III-17perimeter were determined.
Page 126 and 127: OP-III-18of 2. MSR has been coupled
Page 128 and 129: OP-III-19chemisorption heat and pro
Page 130 and 131: OP-III-20In the experiments, total
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OP-III-21obtained by the new techno
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OP-III-22reactor wall from the two-
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OP-III-23and parameters of synthesi
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OP-III-24Results and discussionThe
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OP-IV-1DEEP DESULPHURIZATION OF PET
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OP-IV-2LACTIC ACID AS A BACKGROUND
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OP-IV-3CO REMOVAL FROM H 2 -rich GA
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OP-IV-4REFORMING OF ETHANOL OVER ME
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OP-IV-5MODELING OF HYDROGEN PRODUCT
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OP-IV-6PRODUCTION OF HYDROGEN FROM
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OP-IV-7SYNTHESIS GAS PRODUCTION FRO
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OP-IV-8HYDROGEN PRODUCTION FROM MET
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OP-IV-9A NEW GENERATION OF SUPER-TH
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OP-IV-10EXERGY ANALYSIS OF ENZYMATI
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OP-IV-11ADVANCEMENT OF SLURRY BUBBL
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OP-IV-12Pd-DOPED PEROVSKITE CATALYS
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OP-IV-13HYDROGEN PRODUCTION VIA MET
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Section 5.Catalytic processing of r
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OP-V-1Scheme 1. The developing path
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OP-V-2An example of the model compo
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OP-V-3catalysts were shown to be su
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OP-V-4Catalyst deactivation was mor
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OP-V-53) Study of the FFAs esterifi
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OP-V-6In the present work, a compre
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OP-V-7Ca 2 Fe 2 O 5 , MgFe 2 O 4 an
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OP-V-8cellulose components decompos
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OP-V-9sintering a couple of spirale
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OP-V-10Catalyst preparationA series
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OP-V-11Catalysts characterizationIn
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OP-V-12Kinetic ExperimentsHexadecan
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OP-V-13DESIGN OF PILOT REACTOR AND
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OP-V-14DEVELOPMENT OF A LAB SCALE C
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OP-V-15DEVELOPMENT OF TWO-STAGE PRO
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OP-V-15The data of Table 2 show, th
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OP-V-17ENERGY PRODUCTION FROM BIOMA
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OP-V-18CATALYTIC PARTIAL OXIDATION
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OP-V-19A PHOTOCATALYTIC REACTOR FOR
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OP-V-20BIOMASS GASIFICATION IN A CA
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OP-V-21ESTIMATION OF OPTIMAL REACTO
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POSTER PRESENTATIONSSection 1. Kine
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PP-I-1CONVERSION OF ETHANOL OVER CO
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PP-I-2LATERAL INTERACTIONS, FINITE
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PP-I-3UTILIZATION OF TAFT EQUATION:
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PP-I-4SELECTIVE HYDROGENATION OF CI
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PP-I-5NON OXIDATIVE REGENERATION ME
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PP-I-6Table 1. Parameters in kineti
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PP-I-7where: k nc , k 1 , k a , k b
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PP-I-8After each adsorption or deso
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PP-I-9The increase in pressure, in
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PP-I-10The analysis of the composit
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PP-I-11The network of βP oxidation
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PP-I-12order of magnitude lower. Th
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PP-I-13ab1,01,0Isotope fraction0,5[
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PP-I-14Relations ‘rate vs alcohol
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PP-I-15[EEAA] t , M[EEAA] t -1 , M
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PP-I-17NEW OSCILLATING REACTION:CAR
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PP-I-18NEW OSCILLATING REACTIONS OF
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PP-I-19KINETICS OF GAS-LIQUID PROCE
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PP-I-20COMPLETE OXIDATION OF HARMFU
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PP-I-21THEORETICAL RESEARCH OF SURF
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PP-I-22INFLUENCE OF ORGANIC HELATES
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PP-I-23The equation of the reaction
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PP-I-25SELECTIVE OXIDATION OF METHA
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PP-I-26coefficients of the equation
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PP-I-27into propionic acid. The giv
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PP-I-28In the studied range of temp
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PP-I-29Table. Reaction temperature
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PP-I-30other in both direction of t
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PP-I-31Reynolds number. The boundar
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PP-I-32NANOPARTICLES AND CATALYSISI
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Section 2.Physico-chemical and math
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PP-II-1For investigation, we used n
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PP-II-2criterion «Zn dissolved in
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PP-II-3exist around the steady stat
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PP-II-4in range 0-1. In our case n
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PP-II-5at comparable activity, the
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PP-II-7CFD-CALCULATION OF MALDISTRI
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PP-II-8INVESTIGATION OF NONLINEAR P
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PP-II-8reactivity. There is a small
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PP-II-10CALCULATION OF INDUSTRIAL C
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PP-II-11type of reactors a catalyst
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PP-II-13MATHEMATTICAL MODELLING OF
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PP-II-13where I Э , M 1Э , M 2Э
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PP-II-14where TOC 0 is the initial
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PP-II-16AUTOCATALYTIC REACTION FRON
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Section 3.Catalytic processesí dev
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PP-III-1for the traditional scheme
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PP-III-2Initial conditions: С i (0
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PP-III-3Afterward, a 30% aqueous hy
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PP-III-4The influence of the water
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PP-III-5Vanadium oxide was grafted
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PP-III-6(T p ) was taken as an inde
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PP-III-7dCdτLABdCNABdτdCdτdCdτd
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PP-III-8O 2 , balanced by He, at a
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PP-III-9Solution of system (3) for
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PP-III-10HDT330ºCHDT350ºCHDT370º
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PP-III-11The activity of Au/support
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PP-III-1249775 m 3 /h0,65Initial te
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PP-III-13through one layer of ACC w
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PP-III-14the runs was always higher
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PP-III-15The experimental data for
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PP-III-16Catalytic hydrogenation of
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PP-III-17The following parameters a
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PP-III-18Figure 1 - Dependence of t
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PP-III-19Our method has some advant
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PP-III-20Furthermore, Ayude et al.
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PP-III-22OPTIMIZATION OF THE METHAN
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PP-III-23EXPERIMENTAL INVESTIGATION
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PP-III-24CATALYTIC REACTORS WITH HY
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PP-III-25ACTIVITY OF Cu/ZSM-5 CATAL
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PP-III-26SIMULATION AND OPTIMISATIO
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PP-III-27model of plug flow reactor
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PP-III-28Calculations were experime
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PP-III-29continuous and pressurized
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PP-III-30adequacy of multistage mod
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PP-III-31+CH 3 OHH 2 O + HO-(CH(CH
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PP-III-32procedure presented by Mar
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PP-III-33HPA-x + 2 H + + Pd 0 ⎯
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PP-III-34of the process as well as
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PP-III-35This study was financially
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PP-III-36phase. Peroxopolyoxometall
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PP-III-37performed under atmospheri
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PP-III-38orders of magnitude larger
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PP-III-39CATALYTIC REACTORS WITH ST
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PP-III-40THE OXIDATIVE DEHYDROGENAT
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PP-III-41MODELLING AND DESIGN OF TH
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PP-III-42COMPLEX TECHNOLOGY OF TREA
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PP-III-43PHOTO ELECTROCHEMISTRY APP
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PP-III-45MODELING OF CATALYTIC α-O
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PP-III-46steady states. It was show
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PP-III-47Results and discussion:The
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PP-III-49FIBROUS PALLADIUM-SUPPORTE
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Section 4.Catalytic technologies in
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PP-IV-1method is adiabatic or autot
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PP-IV-2It had been established that
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PP-IV-4INTERACTION OF ACTIVATED ALU
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PP-IV-5ENVIRONMENTALLY FRIENDLY PRO
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PP-IV-6THE 5%Ni-2%Au/Al 3 CrO 6 SYS
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PP-IV-7MESOPOROUS ANODES BASED ON Y
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PP-IV-8ADVANCED OXIDATION PROCESS F
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PP-IV-9PROCESSING OF POLYMERIC CORD
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PP-IV-10EFFECT OF SULPHUR ON THE CA
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PP-IV-11OXIDATIVE CONVERSION OF MET
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PP-IV-13CATALYTIC FLUE GAS CONDITIO
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PP-IV-14RIBBON POROUS NICKEL BASED
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PP-IV-15ETHANOL CONVERSION TO HYDRO
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PP-IV-16A HIGH-EFFICIENT MICROREACT
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PP-IV-17DIRECT DECOMPOSITION OF NIT
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PP-IV-18NICKEL CATALYSTS BASED ON P
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PP-IV-19SELECTION OF FAVOURABLE FEE
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PP-IV-20FORMALDEHYDE FORMATION DURI
Page 434 and 435:
PP-IV-21PRODUCTION OF HYDROGEN-RICH
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PP-IV-22INFLUENCE OF COMPOSITION OF
Page 438 and 439:
PP-IV-24ONE-STAGE CATALYTIC CONVERS
Page 440 and 441:
PP-IV-25THE STUDY OF METHANE DEHYDR
Page 442 and 443:
PP-IV-26MCM-41-SUPPORTED PdNi CATAL
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PP-IV-27IMPROVING THE FLOW SHEET OF
Page 446 and 447:
PP-IV-29THE PARTIAL OXIDATION OF CH
Page 448 and 449:
PP-IV-30PRODUCTION OF CO-FREE HYDRO
Page 450 and 451:
PP-IV-31PHOTOCATALYTICAL ACTIVITY O
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PP-IV-32NEW ELECTRODE MATERIALSFOR
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PP-IV-33THE CATALYTIC HYDROGENATION
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PP-IV-34W 0, μmol O 2/min0,25 1. 1
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PP-V-1INFLUENCE OF ICE ON MEAs OF P
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PP-V-2DIRECT OILS HYDROGENATION TO
Page 462 and 463:
PP-V-3DEVELOPMENT OF Pd/SIBUNIT CAT
Page 464 and 465:
PP-V-4Pt NANOPARTICLE-HOLLOW POROUS
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PP-V-5THE PROCESS FOR PRODUCING ORG
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PP-V-6water removing. This method p
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PP-V-7ResultsThe presented technolo
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PP-V-8the most effective catalysts.
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PP-V-9Neither the low sulphur conte
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PP-V-10composition (methyl esters,
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PP-V-11reactor we can see that its
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PP-V-12Recent studies lead in this
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PP-V-13catalysts (e.g. Pt or Pd), t
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PP-V-14Alkali catalyst. For a basic
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PP-V-15obtaining the related profil
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PP-V-16reaction parameters, not rep
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PP-V-18STUDY OF THE CATALYTIC ACTIV
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PP-V-19BIOMORPHIC CATALYSTS ON THE
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PP-V-20Al,Cu-PILLARED CLAYS AS CATA
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PP-V-21KINETICS OF THE HYDROXYMATAI
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PP-V-22THE NEW METHOD OF OBTAINING
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PP-V-23containing mono- and di-subs
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AUTOCLAVE ENGINEERS COMPANYSYSTEMAT
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CATACON CATACON CATACON CATACON CAT
Page 506 and 507:
Page 508 and 509:
Page 510 and 511:
George AvgouropoulosFoundation for
Page 512 and 513:
Leonid BykovJSC «Chemphyst-Alloy L
Page 514 and 515:
Debora FinoPolitecnico di TorinoCor
Page 516 and 517:
Jenő HancsókUniversity of Pannoni
Page 518 and 519:
Andrey KhudoshinLomonosov Moscow St
Page 520 and 521:
Cristian LedesmaEnergetic Technique
Page 522 and 523:
Uri Matatov-MeytalDepartment of Che
Page 524 and 525:
Karina OjedaIndustrial University o
Page 526 and 527:
Yuri PyatnitskyPisarzhevsky Institu
Page 528 and 529:
Vera ScmachkovaBoreskov Institute o
Page 530 and 531:
Peter StrizhakPisarzhevsky Institut
Page 532 and 533:
Nadezhda VernikovskayaBoreskov Inst
Page 534 and 535:
Nataliya ZubritskayaRSC «Applied C
Page 536 and 537:
ORAL PRESENTATIONS.................
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OP-I-21Saeedizad M., Sahebdelfar S.
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OP-III-9Nekhamkina O., Sheintuch M.
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OP-IV-5Hernández L., Kafarov V.V.M
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OP-V-13Sadykov V., Mezentseva N., V
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PP-I-15PP-I-16PP-I-17PP-I-18PP-I-19
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PP-II-9 Nikiforov A., Paek U-Hyon,
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PP-III-17 Vernikovskaya N.V., Kashk
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PP-III-42 Goshu Y.W., Tsaryov Y.V.,
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PP-IV-17 Ohnishi C.H., Yoshino H.,
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PP-V-9 Hancsók J., Magyar S., Kall
Page 558:
XVIII International Conference on C
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