Smartline Autosampler 3900 Manual / Handbuch V 1508 03/2007

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Konformitätserklärung 153 Declaration of conformity Konformitätserklärung Manufacturer’s name and address: Herstellername und -adresse Wissenschaftliche Gerätebau Dr. Ing. Herbert KNAUER GmbH Hegauer Weg 38 14163 Berlin, Germany Smartline Autosampler 3900 in different versions Order Numbers, Bestellnummern: A 1508x complies with the following requirements and product specifications: ● Low Voltage Ordinance (73/23/EWG) EN 61010-1 (08/2002) ● Engineering Guidelines (89/392/EWG) ● EMC Ordinance (89/336/EWG) EN 6100-3-2 (10/2006) EN 61326-1 (10/2006) entspricht den folgenden Anforderungen und Produktspezifikationen: ● Niederspannungverordnung (73/23/EWG) EN 61010-1 (08/2002) ● Maschinenrichtlinie (89/392/EWG) ● EMV-Verordnung (89/336/EWG) EN 6100-3-2 (10/2006) EN 61326-1 (10/2006) The product was tested in a typical configuration. Das Produkt wurde in einer typischen Konfiguration geprüft. Berlin, 2007-03-30 Alexander Bünz (Managing Director) The CE Shield is attached to the rear of the instrument. Das Konformitätszeichen ist auf der Rückwand des Gerätes angebracht.
154 INDEX(english) INDEX(english) A Air needle................................................. 55 Air segment ............................................. 35 Analysis time ........................................... 39 AS 3900 logbook ..................................... 34 AS 3900, preparative............................... 73 B Buffer tubing ............................................ 53 C Calibration vials ....................................... 44 Column thermostat .................................. 33 Control I/O connections..................... 27–28 Contact closure output connector (P1) 27 RS232 connector ................................ 27 TTL input connector (P2) .................... 27 Copy a method ........................................ 34 D Destination vials ...................................... 44 Device identifier ....................................... 37 Direct control functions Maintenance........................................ 32 Manual wash ....................................... 32 Needle arm movement........................ 32 Serial communication mode................ 32 Temperature control............................ 33 Direct Control functions ........................... 32 Direct functions........................................ 31 E Erase a method ....................................... 34 Error codes .............................................. 63 F Firmware.................................................. 75 Fluid connections..................................... 22 HPLC connections .............................. 23 Syringe ................................................ 24 Wash solvent....................................... 23 Waste tubing ....................................... 23 Flush volume ........................................... 39 Freeze input............................................. 28 Freeze input active .................................. 37 Full loop injection............................... 39, 52 Fuses....................................................... 21 H Hard function keys [CL], Clear ........................................... 31 [E], Enter ............................................. 31 [Escape] .............................................. 31 [Hold/Cont.] ......................................... 31 [Menu] ................................................. 31 [Methods]............................................. 31 [Priority] ............................................... 31 [Series] ................................................ 31 [Start/Stop]........................................... 31 [System]............................................... 31 Headspace pressure................................ 35 HPLC connections ................................... 23 I Injection AS 3900, prep...................................... 75 Injection marker pulse length ................... 37 Injection mode µl Pick-up injection............................... 39 Full loop injection................................. 39 Partial loopfill injection ......................... 39 Injection principle ..................................... 14 µl Pick-up injections.......................18–20 Full loop injections .........................15–16 Partial loopfill injections .................16–18 Injection program ..................................... 38 Analysis time........................................ 39 Flush volume ....................................... 39 Injection volume................................... 39 Number of injections per vial ............... 39 Injection valve (Valco).............................. 47 Injection valve replacement ..................... 47 Injection volume .................................39, 52 Input edge next injection .......................... 37 Inspection Intervals .................................. 65 Installation AS 3900, prep...................................... 74 Instrument description Exploded view of AS 3900................... 13 Rear side of AS 3900........................... 14 Instrumentbeschreibung Rückansicht des AS 3900 ................... 14 K Keyboard.................................................. 30 Hard function keys............................... 30 Numeric keys ....................................... 30 Soft function keys ................................ 30 L Linearity.................................................... 68 List of accessories ................................... 61 Loading the sample tray........................... 27 M Maintenance............................................. 32 Manual injection valve switching.............. 32 Manual wash............................................ 32 Method programming............................... 38 Mix program .......................................38, 42 Delete step........................................... 42 Insert step ............................................ 42 Mixture Test ............................................. 69 N Needle arm movement............................. 32 Next injection input.............................28, 45
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Smartline Autosampler 3900 Manual /
Page 3 and 4:
2 Maintenance 47 Injection valve 47
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4 Wartung 121 Injektionsventil 121
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6 Quick Start AS 3900 • After tur
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8 Quick Start AS 3900 Press keys: D
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10 Programming Chart Programming Ch
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12 About AS 3900 Side-port needle:
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14 Injection Principle 1. P2- I/O c
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16 Injection Principle Fig. 8 Full
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18 Injection Principle Fig. 15 Part
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20 Installation Installation Fig. 2
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22 Installation Fluid connections R
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24 Installation - With a syringe v
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26 Installation Do not use the 10-C
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28 Installation Table 3: Connector
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30 Operation Operation Typographic
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32 Operation In the Ready screen th
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34 Operation Turn the tray cooling
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36 Operation Table 4: Syringe speed
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38 Operation For information how to
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40 Operation A wash comprises two p
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42 Operation Mix program After pres
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44 Operation Should a method consis
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46 Operation With the Next Injectio
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48 Maintenance • Pull the valve o
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50 Maintenance Following is the pro
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52 Maintenance Body Shaft Assembly
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54 Maintenance Sample needle 1 Ferr
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56 Maintenance Fig. 46: Changing th
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58 Troubleshooting Analytical probl
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60 Troubleshooting Fig. 50: Bad rep
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62 APPENDIX A: List of Accessories
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64 APPENDIX B: Error Codes Vials ER
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66 APPENDIX C: Test Procedure Inspe
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68 APPENDIX C: Test Procedure Serie
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70 APPENDIX C: Test Procedure After
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72 APPENDIX C: Test Procedure TEST
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74 APPENDIX D: AS 3900, Preparative
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76 APPENDIX D: AS 3900, Preparative
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78 Hinweise zum Gebrauch des Handbu
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80 Schnellstart des AS 3900 Beispie
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82 Schnellstart des AS 3900 Beispie
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84 Programmübersicht Programmüber
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86 AS 3900, allgemeine Beschreibung
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88 Injektionsprinzip 1. P2- I/O Ans
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90 Injektionsprinzip Abb. 9 Vollsch
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92 Injektionsprinzip Abb. 15 Partie
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94 Installation Installation Abb. 2
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96 Installation BRANDGEFAHR! VERWEN
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98 Installation Zur Füllung der Sp
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100 Installation Verwenden sie kein
Page 103 and 104: 102 Installation Tabelle 3: Anschlu
Page 105 and 106: 104 Betrieb Betrieb Typographische
Page 107 and 108: 106 Betrieb [Menu]: [MENU] READY (X
Page 109 and 110: 108 Betrieb Im Falle der installier
Page 111 and 112: 110 Betrieb Tabelle 4: Spritzengesc
Page 113 and 114: 112 Betrieb Injektionsvolumen des A
Page 115 and 116: 114 Betrieb Waschprogramm METHOD N
Page 117 and 118: 116 Betrieb Mischprogramm Nach dem
Page 119 and 120: 118 Betrieb Der Wert kann für lee
Page 121 and 122: 120 Betrieb Fernsteuerung Nach dem
Page 123 and 124: 122 Wartung Abb. 38: Ventileinbau
Page 125 and 126: 124 Wartung Wartung Bei normalem Ge
Page 127 and 128: 126 Wartung • Setzen Sie den Stat
Page 129 and 130: 128 Wartung Pufferschlauch: Tabelle
Page 131 and 132: 130 Wartung Abb. 46: Auswechseln de
Page 133 and 134: 132 Troubleshooting Analytische Pro
Page 135 and 136: 134 Troubleshooting Schlechte Repro
Page 137 and 138: 136 ANHANG A: Zubehör Artikelnr. B
Page 139 and 140: 138 ANHANG B: Fehlermeldungen Vials
Page 141 and 142: 140 ANHANG C: Test Prozeduren Abb.
Page 143 and 144: 142 ANHANG C: Test Prozeduren Serie
Page 145 and 146: 144 ANHANG C: Test Prozeduren 4. Mi
Page 147 and 148: 146 ANHANG C: Test Prozeduren TEST
Page 149 and 150: 148 ANHANG D: AS 3900, Prep Install
Page 151 and 152: 150 ANHANG D: AS 3900, Prep EPROM A
Page 153: 152 Gewährleistungsbedingungen War
Page 157 and 158: 156 INDEX(deutsch) INDEX(deutsch)
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Smartline Autosampler 3900 Manual / Handbuch V 1508 03/2007

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