Smartline Autosampler 3900 Manual / Handbuch V 1508 03/2007
Smartline Autosampler 3900 Manual / Handbuch V 1508 03/2007
Smartline Autosampler 3900 Manual / Handbuch V 1508 03/2007
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Maintenance 55<br />
Syringe<br />
• Check the needle penetration depth, see below and adjust if<br />
necessary.<br />
• Perform a wash routine to clean the new needle by pressing<br />
<br />
Air needle replacement<br />
To replace the air needle proceed as follows (see Fig. 44):<br />
• Remove sample needle as described.<br />
• Remove air needle (10) and install new air needle.<br />
• Reinstall sample needle as described.<br />
Sample needle penetration depth<br />
To keep rest volume small, the sample needle should stop close to the<br />
bottom of the sample vial. If the needle penetration depth needs<br />
adjustment, proceed as follows (see Fig. 45):<br />
• Open keyboard cover.<br />
• Place an uncapped sample vial in position 2 of the tray.<br />
• Lower the sample needle in the vial, therefore:<br />
Program a method with a full loop injection and an analysis time of<br />
at least 10 seconds.<br />
Program a Series with the programmed method and vial 2 as first<br />
and last vial.<br />
Start the Series.<br />
As soon as the sample needle has entered the vial, switch of the<br />
power supply.<br />
• Loosen adjustment screw one turn (counter clockwise).<br />
• Use the needle connection nut (4) as a grip, adjust needle<br />
penetration depth.<br />
Needle should stop not less than 1 mm above the bottom of a<br />
standard vial and not less than 2 mm above the bottom of a conical<br />
vial.<br />
• Fasten adjustment screw (clockwise).<br />
• Re-apply the power, the AS <strong>3900</strong> will initialize and is ready for use.<br />
The AS <strong>3900</strong> is factory equipped with a 250 µl syringe, but can also be<br />
equipped with a 1000 µl syringe.<br />
To install another syringe proceed as follows:<br />
Do not disconnect the power supply of the AS <strong>3900</strong>, it is needed to<br />
move the syringe!