Smartline Autosampler 3900 Manual / Handbuch V 1508 03/2007

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Troubleshooting 59 Fig. 49: No injection NO INJECTION Leakage inside Injection Valve Disconnect the needle tubing and the buffer tubing. Blockage in Flow Path Connect port 1 to an HPLC pump Block port 6. Start the pump at a low flow Start manual wash Disconnect Buffer tubing from valve Start manual wash Disconnect Buffer tubing from Syringe valve Start manual wash Disconnect needle from Valve Solvent flowing out of inj. port No Solvent out of open end No Solvent out of syringe valve Check for over tightened connections in the entire Flow Path & Check the syringe valve Observe ports 3 and 4 for leakage No No Recheck with manual valve Yes Yes Yes Yes Check needle Check rotor seal Check buffer tubing Check rotor seal
60 Troubleshooting Fig. 50: Bad reproducibility BAD REPRODUCIBILITY Air in Flow Path Start manual wash Air in Syringe Leaking Syringe Leaking Syringe Valve Rotor seal worn out Dead volumes in tubing connections Remove Syringe and fill manually with wash solvent Replace plunger tip or Syringe Replace Valve Replace seal Check Stator Redo connections with new Ferrules and nuts
Page 1 and 2:
Smartline Autosampler 3900 Manual /
Page 3 and 4:
2 Maintenance 47 Injection valve 47
Page 5 and 6:
4 Wartung 121 Injektionsventil 121
Page 7 and 8:
6 Quick Start AS 3900 • After tur
Page 9 and 10: 8 Quick Start AS 3900 Press keys: D
Page 11 and 12: 10 Programming Chart Programming Ch
Page 13 and 14: 12 About AS 3900 Side-port needle:
Page 15 and 16: 14 Injection Principle 1. P2- I/O c
Page 17 and 18: 16 Injection Principle Fig. 8 Full
Page 19 and 20: 18 Injection Principle Fig. 15 Part
Page 21 and 22: 20 Installation Installation Fig. 2
Page 23 and 24: 22 Installation Fluid connections R
Page 25 and 26: 24 Installation - With a syringe v
Page 27 and 28: 26 Installation Do not use the 10-C
Page 29 and 30: 28 Installation Table 3: Connector
Page 31 and 32: 30 Operation Operation Typographic
Page 33 and 34: 32 Operation In the Ready screen th
Page 35 and 36: 34 Operation Turn the tray cooling
Page 37 and 38: 36 Operation Table 4: Syringe speed
Page 39 and 40: 38 Operation For information how to
Page 41 and 42: 40 Operation A wash comprises two p
Page 43 and 44: 42 Operation Mix program After pres
Page 45 and 46: 44 Operation Should a method consis
Page 47 and 48: 46 Operation With the Next Injectio
Page 49 and 50: 48 Maintenance • Pull the valve o
Page 51 and 52: 50 Maintenance Following is the pro
Page 53 and 54: 52 Maintenance Body Shaft Assembly
Page 55 and 56: 54 Maintenance Sample needle 1 Ferr
Page 57 and 58: 56 Maintenance Fig. 46: Changing th
Page 59: 58 Troubleshooting Analytical probl
Page 63 and 64: 62 APPENDIX A: List of Accessories
Page 65 and 66: 64 APPENDIX B: Error Codes Vials ER
Page 67 and 68: 66 APPENDIX C: Test Procedure Inspe
Page 69 and 70: 68 APPENDIX C: Test Procedure Serie
Page 71 and 72: 70 APPENDIX C: Test Procedure After
Page 73 and 74: 72 APPENDIX C: Test Procedure TEST
Page 75 and 76: 74 APPENDIX D: AS 3900, Preparative
Page 77 and 78: 76 APPENDIX D: AS 3900, Preparative
Page 79 and 80: 78 Hinweise zum Gebrauch des Handbu
Page 81 and 82: 80 Schnellstart des AS 3900 Beispie
Page 83 and 84: 82 Schnellstart des AS 3900 Beispie
Page 85 and 86: 84 Programmübersicht Programmüber
Page 87 and 88: 86 AS 3900, allgemeine Beschreibung
Page 89 and 90: 88 Injektionsprinzip 1. P2- I/O Ans
Page 91 and 92: 90 Injektionsprinzip Abb. 9 Vollsch
Page 93 and 94: 92 Injektionsprinzip Abb. 15 Partie
Page 95 and 96: 94 Installation Installation Abb. 2
Page 97 and 98: 96 Installation BRANDGEFAHR! VERWEN
Page 99 and 100: 98 Installation Zur Füllung der Sp
Page 101 and 102: 100 Installation Verwenden sie kein
Page 103 and 104: 102 Installation Tabelle 3: Anschlu
Page 105 and 106: 104 Betrieb Betrieb Typographische
Page 107 and 108: 106 Betrieb [Menu]: [MENU] READY (X
Page 109 and 110: 108 Betrieb Im Falle der installier
Page 111 and 112:
110 Betrieb Tabelle 4: Spritzengesc
Page 113 and 114:
112 Betrieb Injektionsvolumen des A
Page 115 and 116:
114 Betrieb Waschprogramm METHOD N
Page 117 and 118:
116 Betrieb Mischprogramm Nach dem
Page 119 and 120:
118 Betrieb Der Wert kann für lee
Page 121 and 122:
120 Betrieb Fernsteuerung Nach dem
Page 123 and 124:
122 Wartung Abb. 38: Ventileinbau
Page 125 and 126:
124 Wartung Wartung Bei normalem Ge
Page 127 and 128:
126 Wartung • Setzen Sie den Stat
Page 129 and 130:
128 Wartung Pufferschlauch: Tabelle
Page 131 and 132:
130 Wartung Abb. 46: Auswechseln de
Page 133 and 134:
132 Troubleshooting Analytische Pro
Page 135 and 136:
134 Troubleshooting Schlechte Repro
Page 137 and 138:
136 ANHANG A: Zubehör Artikelnr. B
Page 139 and 140:
138 ANHANG B: Fehlermeldungen Vials
Page 141 and 142:
140 ANHANG C: Test Prozeduren Abb.
Page 143 and 144:
142 ANHANG C: Test Prozeduren Serie
Page 145 and 146:
144 ANHANG C: Test Prozeduren 4. Mi
Page 147 and 148:
146 ANHANG C: Test Prozeduren TEST
Page 149 and 150:
148 ANHANG D: AS 3900, Prep Install
Page 151 and 152:
150 ANHANG D: AS 3900, Prep EPROM A
Page 153 and 154:
152 Gewährleistungsbedingungen War
Page 155 and 156:
154 INDEX(english) INDEX(english) A
Page 157 and 158:
156 INDEX(deutsch) INDEX(deutsch)
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Smartline Autosampler 3900 Manual / Handbuch V 1508 03/2007

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