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WIIC-S-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of 2 AnaLIS ID: 901206-019 Customer Sample 10: N-101 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite ID: 10646 Saimpte Matrix: SOIL Instrument ID: 597093 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 BRA -*ase/Neutrat/Acid Compounds (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 13-DEC-1990 Preparation Procedure Nuber: Analysis Procedure Nuber: BRA (CLP) MOP Percent Moisture: 5.7 Dilution Factor: 1.0 Percent moisture (decanted): Analyst: C MEEHAN Associated Blank: 901213-028 OA File Mumber: NA El: Result has been Corrected for Spike CAS uglKg CAS Ug/Kg 108-95-2 Phenol 980tJ 106-47-8 4-Chloroanitine 98OU 111-44-4 bis(2-Chloroethyl)ether 980U 87-68-3 Hexachlorobutadiene, 980U 95-57-8 2-Chtorophenol 980U 59-50-7 4-Chloro-3-methyLpheno. 980U 541-73-1 1,3-Dichtorobenzene 980U 91-57-6 2-MethyinaphthaLene 984. 106-46-7 l.4-Dichlorobenzene 980U 77-4.7-4 HexachlorocycLopentadiene 980U 100-51-6 UenzyL Alcohol 980U 88-06-2 2,I..6-Trichtorophenot 980U 95-50-1 1,2-Dichlorobenzene 98OU 95-95-4 2.4,5-Trichtorophenot 4700u 95-48-7 2-MethylphenoL 980U 91-58-7 2-Chtoronaphthalene 980u 108-60-1 bis(2-ChLoroisopropyt)ether 980U 88-74-4 2-Mitroanitine 4700U 106-44-5 4-MethyLphenot 980U 131-11-3 Dimethytphthalate 980U 621-64-7 M-Mitroso-di-n-propyanine 980U 208-96-8 Acenaphthylene 980U 67-72-1 Hexachtoroethane 980U 99-09-2 3-Mitroaniline 470OU 98-95-3 Nitrobenzene 980U 83-32-9 Acenaphthene 980U 78-59-1 Isophorone 980U 51-28-5 2,4-Dinitrophenol 470OU 88-75-5 2-NitrophenoL 980U 100-02-7 is-Mitrophenot 4700U 105-67-9 2,4-Dimethytphenol 980U 132-64-9 Dibenzofuran 980U 65-85-0 Benz *oic Acid 4700U 121-14-2 2.I.-Dinitrotoluene 980U 111-91-1 bisC2-Chloroethoxy)methane 980U 606-20-2 2,6-DinitrotoLuene 980U 120-83-2 2,4-Dichlorophenol 980U 84-66-2 Diethylphthalate 180 4iQ do (A 120-82-1 1,2,4-TrichLorobenzene 980U 7005-72-3 4-ChLorophenyL-phenylether 980u 91-20-3 Naphthalene 980U 86-73-7 Fluorene 980U Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. i - indicates an estimated value. ND - Not detected./ A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D- 16
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLIS ID: 901206-019 Customer Sample ID: N-101 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNERIR. SHUCK Fite ID: 10646 Samp~le Matrix: SOIL instrument ID: 597093 Requisition Number: Authorized By: D. C. Canada Date Samrple Received: 6-DEC-1990 UNA - Base/Neutral/Acid Comrpou~nds (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 13-DEC-1990 Preparation Procedure Number: Analysis Procedure Number: SNA (CLP) NDP Percent Moisture: 5.7 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEEHAN Associated Blank: 901213-028 CA File Number: NA El : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 100-01-6 4-Nitroaniline 470OU 53-70-3 Dibenz(ah)anthracene 98OU 534-52-1 4,6-Dinitro-2-methytphenol 4700U 191-24-2 Benzo(ghi)perytene 980U 86-30-6 N-itrosodiphenylamine 9S0U 101-55-3 4-Bromopheny-phenylether 98OU 118-74-1 Nexachlorobenzene 980U 87-86-5 Pentachtorophenot 4700U 85-01-8 Phenanthrene 980U 120-12-7 Anthracene 980Ui 84-74-2 Di -n-butylphthalate 42006 IA 206-44-0 Fluoranthene 980t 129-00-0 Pyrene 98WU 85-68-7 Butylbenzylphthalate 98OU 91-94-1 3,3'-Dichlorobenzidine 1900U 56-55-3 Benzo~a)anthracene 980U 117-81-7 bis(2-Ethythexyl)phthalate *00 9 80 L-. 218-01-9 Chrysene 98OW 117-84-0 DI-ui-octylphthalate 98WU 205-99-2 Benzo(b)fluoranthene 98WU 207-08-9 Benzo~k)fluorenthene 98WU 50-32-8 Benzo(a)pyren. 98WU 193-39-5 Indeno(1,2,3-cd)pyrene 98WU Data Reporting Qualifiers: U - Comrpound was analyzed for but not detected. The numb~er is the attainable detection limit for the samrple. * - Analyte was found in the reagent blank as well as the samrple. J - indicates an estimated value. ND - Not detected. A -Aldol condensation product. o - Secondary dilution. E - Exceeds Initial calibration range. D-17
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