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WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department BRA CTCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS ID: 901206-033 Customer Sample ID: N-113 Laboratory: Organic Mass Spectroscoy Laboratory Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL Fit* ID: 10662 Level: (low/reed): Low Date Received: 6-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 14-DEC-1990 % Moisture: not dec. . 3.8 dec. Date Extracted: 12-DEC-1990 Extraction: CSepF/Cont/Sonc) SoxH PH: GPC Cleanup: (YIN) N Concentration Uits Number TICs found: 13 Cug/L or uglKg): _LtVg ICAS NUM4BER COMPOUND NAME I RT IEST. CONC. 0 I1. 123-42-21 2-Pentanone. 4-hydroxy-4-methy I2.- 25013-16-51 Phenot.(1.1-dimethylethyt)-4-M I3. 1Unknown (Alkyl Hydrocarbon) 4. 1._____ Unknown (Alkyl Hyrocarbon) I5. 17851-53-51 1.2-gemzenedicarboxylic acid b I 5?.0I99-O i o.45 19.43 I550I N.60 ~ V.80__ ; IJ Ago0 I-~ 0 IJ 6. Unknown (Hydrocarbon) 99 7 .______ Unknown (Hydrocarbon) I 25.90 I800 I . I .jUnknown (sat'd Hyrocarbon) 264 ;Z JOl do 19. 1Iunknown I 27.681 1600 J I10. Unknown (sat'd Hydrocarbon) e i3 I Jo I11. Unknown (Hydrocarbon) I 30.54 I370 1 12. [Unknown (Aikyl Hydrocarbon) I 32.60 J410j 13. [Unknown (Alkyt Hydrocarbon) 1 33.461 1400[ 14. _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ 115. _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ 116. _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ 17. _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~18. _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ 119. _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ j20.____ ___________1____ 121. II____ 122. II____ 123.II_____I______ _ 124. II____ 125. 1_ _ _ _ 1 I 126. I. ____1_______ 127. II____ 128. I. 129. I. 130. I. Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number Is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. NO - Not detected. A -Aldol condensation product. 0 - Secondary dilution. E -Exceeds Initial calibration range. P - Probable Identification. D-64
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of 1 AnaLIS ID: 901206-033 Customer Sample ID: N-113 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 07617 Sample Matrix: SOIL Instrument 10: 597002 Reqiuisition Numb~er: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 VOA -Volatile Organic Compounds CTCL) Date Extracted/Prepared: Date Analyzed: 11-DEC-1990 Preparation Procedure Numb~er: PURGE & TRAP Analysis Procedure Numb~er: VGA (CIP) HOP Percent Moisture: 6 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: GL HUDOLESTON Associated Blank: 901211-004 CA File Number: NA E) : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg .......................... .......... ........... .............................. .......... 74-87-3 Chtoromethane 11t; 79-00-5 1,1,2-Trichloroethone 5U 74-83-9 Bromomethane 11U 71-43-2 Benzene SU 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1.3-Dichioropropene SU 75-00-3 Chloroethane IVU 75-25-2 Bromoform S1) 75-09-2 Methylene Chloride 5U 108-10-1 4-Methyt-2-pentanone Ilt 67-64-1 Acetone 32 LA 591-78-6 2-Hexanone 11U 75-15-0 Carbon Disulfide 5U 127-18-4 Tetrachtoroethene 5U 75-35-4 1,1-Dichloroethene SU 79-34-5 1.1,2,2-Tetrachtoroethane 5U 75-34-3 1.1-Dichtoroethane 5U 108-88-3 Toluene 5U 540-59-0 1,2-Dichioroethene (total) 5U 108-90-7 Chlorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 Ethylbcnzene 5U 107-06-2 1,2-Dichloroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xylene (total) 5U 71-55-6 1,1,1-Trichloroethane 51) 56-23-5 Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate 11t; 75-27-4 Bromodichloromethane 5U 78-87-5 1.2-Dichioropropane 5U 10061-01-5 cis-1,3-Dichlaropropenc 5U 79-01-6 Trichloroethene 5U Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The nuimber is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J9 - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - secondary dilution. E - Exceeds initial calibration range. D-65
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