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W:C-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of I AnaLIS ID: 901206-029 Customer Sample ID: N-109 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 07613 Sample Matrix: SOIL Instrument ID: 597002 Requisition Numb~er: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 VOA -Volatile Organic Compounmds CTCL) Date Extracted/Prepared: Date Analyzed: 11-DEC-1990 Preparation Procedure Numb~er: PURGE & TRAP Analysis Procedure Numb~er: VOA (CLP) MOP Percent moisture: 8 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: GL NUDDLESTON Associated Blank: 901211-004 QA File Number: NA CI:Result has been Corrected for Spike CAS ug/Kg CAS uglKg 74-87-3 Chioromethane 11U 79-00-5 1,1*2-Trichloroethane 5U 74-83-9 Bromomthane 11U 71-43-2 Benzene 5U 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1,3-Dichtoropropene 5U 75-00-3 ChLoroethane 75-09-2 Methylene Chloride 11U .5t-*- LA 75-25-2 Bromoform 108-10-1 4-Methyl-2-pentanone SU 11U 67-64-1 Acetone 15 IA 591-78-6 2-Hexanone I 1U 75-15-0 Carbon Disulfide 5U 127-18-4 Tetrachtoroethene SU 75-35-4 *1-Dichtoroethene SU 79-34-5 1,1,2,2-Tetrachloroethane 5U 75-34-3 ,1-DlchLoroethane 5U 108-88-3 Toluene 5U 540-59-0 1,2-Dichtoroethene (total) 5U 108-90-7 Chlorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-DichLoroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xylene (total) 5U 71-55-6 1,11-TrichLoroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4 vinyl Acetate 11U 75-27-4 Iromodichloromethane 5U 78-87-5 1,2-Dichloropropane 5U 10061-01-5 cis-13-OichLoropropene 79-01-6 Trichtoroethene 5U 5U I J69 124-48-1 Dibromochioromethane SU Data Reporting Qualifiers: U -Comrpounrd was analyzed for but not detected. The number is the attainable detection limit for the sample. B Analyte was found in the reagent blank as well as the sample. J -Indicates an estimated value. ND -Not detected. A -Aldol condensation product. D Secondary dilution. E -Exceeds initial calibration range. D-48
WIIC-S-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 2 AnaLIS IN: 901206-030 Customer Samuple ID: N-110 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fit@ ID: 10659 Sample Matrix: SOIL instrument tD: 597093 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 DNA -Base/Neutral/Acid Compounmds (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 14-DEC-1990 Preparation Procedure Numiber: Analysis Procedure Numb~er: DNA CCLP) WOP Percent Moisture: 7.4 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEEHAN Associated Btank: 901213-028 QA File Number: NA [] : Result has been Corrected for Spike CAS iig/Kg CAS ug/Kg 108-95-2 Phenol 990U 106-47-8 4-Chloroanitine 990U 111-44-4 bis(2-Chloroethyt)ether 99OU a7-68-3 Nexachiorobutadiene 990U 95-57-8 2-Chtorophenol 99OU 59-50-7 4-Chioro-3-methytphenol 990U 541-73-1 1,3-Dichtorobenzene 990U 91-57-6 2-MethytnaphthaLene 990U 106-46-7 1.4-Olchlorobenzene 990U 77-47-4 HexachLorocyclopentadiene 990U 100-51-6 BenzyL Alcohol 990U 88-06-2 2,4,6-TrichlorophenoL 990U 95-50-1 1,2-Dichtorobenzene 990U 95-95-4 2,4,5-TrichtorophenoL 4800U 95-48-7 2-Methytplienol 990U 91-58-7 2-Chtoronsphthalene 990U 108-60-1 bis(2-Chtoroisopropyt)ether 990U 88-74-4 2-Nitroaniline 480OU 106-44-5 4-methyLphenol 990U 131-11-3 Dlmethylphthalate 990U 621-64-7 N-Nitroso-di-n-propytamine 99OU 208-96-8 Acenaphthylene 99OU 67-72-1 Hexachloroethane 99W 99-09-2 3-Nitroaniline 480WU 98-95-3 Nitrobenzene 990U 83-32-9 Acenaphthene 99WU 78-59-1 Isophorone 990U 51-28-S 2,4-Dinitrophenot 480OU 88-75-5 2-Nitrophenol 99WU 100-02-7 4-Nitrophenol 4800U 105-67-9 2.4-DimethylphenoL 99W 132-64-9 Oibenzofuran 990U 65-85-0 Benzoic Acid 4"0 40-d41 L)A 121-14-2 2,4-Dinitrotoluene 990W 111-91-1 bis(2-Chtoroethoxy)methane 99W 606-20-2 2,6-Dinitrotoluene 990U 120-83-2 2,4-Dichlorophenol 99W 84-66-2 .Diethytphthatate q0me# L&. 120-82-1 1,2,4-Trichtorobenzene 99W 7005-72-3 4-Chtorophenyl-phenytother 99W 91-20-3 Naphthalene 99W 86-73-7 Fluorene 990U Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The numb~er is the attainable detection limit for the sampLe. B - Analyte was foun~d in the reagent blank as well as the sample. J - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. 11 E - Exceeds Initial calibration range. D-49
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P.O. Box 1970 Rfichland. WA 99352 W
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