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W1dC-SD-EN-TI-136,-Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department INA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnSLIS ID: 901206-031 Customer Sample ID: N-1ll Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SNUCK Sample Matrix: SOIL File ID: 10660 Level: (tow/mod): LOW Date Received: 6-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 14-DEC-1990 % Moisture: not dec. 6.1 dec. _____Date Extracted: 12-DEC-1990 Extraction: (SepF/Cont/Sonc) SoxH pH: ____ GPC Cleanup: CT/N) N Concentration Units Number TICs found: 15 (ug/L or ug/Kg): u2LKI ICAS NUMBER COMPOUND NAM4E I RT jEST. CONC. a 1. 123-42-21 2-Pentanone. 4-hydroxy-4-methy j 5.3' ''' I! I2. 872-50-41 2-Pyrrolidinone. 1-methyl- 9 .ZI[ 44 do~I I3. 25013-16-51 Phenol.(1.1-dimethylethyl)-4-m i6I -W44-49______ I4. 1 Unknown (sat'd Hydrocarbon) 19.42 I830 1 ' I5. Unknown (Atkyl Hydrocarbon) J 1.69Isee M I6. Unknown (sat'd Hydrocarbon) j 22.73 _ I410_ __ _6 I7. jUnknown (Hydrocarbon) 43j7 se . do a .______ Unknown (sat'd Hydrocarbon) I9. Unknown (Hydrocarbon) 110. Unknown (sat'd Hydrocarbon) it1. IUnknown I 156 25.89 j850 V6 - 27.53 I660 9.O20#-4 is J .1 00 J J . 1 'I 12. IUnknown (Hydrocarbon) MR 65 09- 113. IUnknown I 29.39! ~ 470 1 1 14. I15. 116. IUnknown (sat'd Hydrocarbon) IUnknown (Hydrocarbon) I I 32.59 I420 33.51 I IJ 1500 I I 117. 1 I 118. 119. II_ _ _ _ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _I_ _I_ _ _ _ _ I 120. 121. 122. 123. II_ II_____ _ _ _ i__ _ _ _ j__ _ _ _ _ _ _ _ _ _I_ _ _ _ _ _ _ _I_ _ _t_ _ _ _ _I_ _ ____ __ _ _ _ I I 125. II_ _ _ _ _ _I_ _ _ _ _ _ _ _ 126. __ _ _ _ _I_ _ _ _ _I_ _ _ I 127. ___________I__ _ 128.I __ _ _ _I_ _ _ _ I__ _ 129. II_ _ _ _ _I_ _ _ _ _I_ _ _ 130. ______I_____ Data Reporting Qualifiers: U -Compound was analyzed for but not detected. The number Is the attainable detection limit for the sample. 8 - Analyte was found in the reagent blank as well as the sample. J1 - Indicates an estimated value. NO H ot detected. A -Aldol condensation product. D -Secondary dilution. E -Exceeds Initial calibration range. P - Probable Identification. D-56
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of I AnaLIS ID: 901206-031 Custom'er Sample ID: N-111 Laboratory: File 10: Organic Mass Spectroscopy Laboratory 07615 Customer: SUam3lS Matrix: J1. XESSMER/R. SOIL SHUCK Instrument 10: 5970#2 Requisition Number: Authorized By: 0. C. Canada Date Sample Received: 6-DEC-1990 VOA - Volatile Organic Compound &CTCL) Date Extracted/Prepared: Date Analyzed: 11-DEC-1990 Preparation Procedure Numb~er: PURGE & TRAP Analysis Procedure Number: VOA (CLP) MOP Percent Moisture: 6 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: GL MUDDLESTON Associated Blank: 901211-004 GA File Nuumber: NA II:Result has been Corrected for Spike CAS ug/Kg CAS uglKg ......... .............................. .......... ........... .............................. .......... 74-87-3 Chloromethane 11U 79-00-5 1,1,2-Trichloroethane 5U 74-83-9 Bromomethane liii 71-43-2 Benzene 5U 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1,3-Dichloropropene SU 75-00-3 Chtoroethane 11U 75-25-2 Bromoform 5U 75-09-2 Methylene Chloride £ t--LA 108-10-1 4-Methyl-2-pentanone 11U 67-64-1 Acetone 11U 591-78-6 2-Hexanone 11U 75-15-0 Carbon Disulfide SU 127-18-4 Tetrachtoroethene 5U 75-35-4 1,1-Dichloroethene SU 79-34-5 1,1,2,2-Tetrachloroethane 5U 75-34-3 1,1-Dichloroethane SU 108-88-3 Toluene 5U 540-59-0 1,2-Dichloroethene (total) 511 108-90-7 Chlorobenzene 5U t67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-Dichloroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xylene (total) 5U 71-55-6 1,1,1-Trichloroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate 11U 75-27-4 Bromodichloromethane 5U 78-87-5 1,2-Dichioropropane 5U 10061-01-5 cis-i,3-Dichloropropene SU 79-01-6 Trichloroethene 5U 124-48-1 Dibromochtoramethane SU Data Reporting Qualifiers: U -cowpotwi was analyzed for but not detected. The number is the attainable detection limit for the sample. B Analyte was found in the reagent blank as well as the sample. .1 Indicates an estimated value. ND -Not detected. A -Aldol conidensation product. O Secondary dilution. E -Exceeds initial calibration range. D-57
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