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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 1 AnaLiS ID: 901206-046 Customer SuuLe ID: N-124 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite ID: 07596 Samp~le Matrix: SOIL instrument ID: 597002 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 5-DEC-1990 VOA - Volatile organic Compounds (TCL) Date Extracted/Prepared: Date Analyzed: 10-DEC- 1990 Preparation Procedure Numb~er: PURGE & TRAP Analysis Procedure Number: VGA (CLP) MOP Percent Moisture: 7 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: SL STAFFORD Associated Blank: 901210-025 OA File Number: NA El: Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 74-87-3 Chtoromethane 11U 79-00-5 1,1,2-Trichloroethane 5U 74-83-9 Uromomethane 11U 71-43-2 Benzene 5U 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1,3-Dichtoropropene SU 75-00-3 Chloroethane 11U 75-25-2 Bromoform 5U 75-09-2 Methylene Chloride £ dt0 LA 108-10-1 4-Methyl-2-pentanone 111) 67-64-1 Acetone 25 -& (A 591-78-6 2-Hexanone 11U 75-15-0 Carbon Disulfide 5U 127-18-4 Tetrachioroethene S1) 75-35-4 1,1-Dichioroethene 5U 79-34-5 1,1,2,2-Tetrachioroethane 5U 75-34-3 1,1-Dichloroethane SU 108-88-3 Toluene 5U 540-59-0 1,2-Dichtoroethene (total) 5U 108-90-7 ChLorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-Dichloroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone 11U 1330-20-7 Xylene (total) 5U 71-55-6 1,1,1-Trichloroethane 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate 11U 75-27-4 BromodichLoromethane 5U 78-87-5 1,2-Dichtoropropane 5U 10061-01-5 cis-1,3-Dichtoropropene 5U 79-01-6 Trichloroethene 5U 124-48-1 Dibromochtoromethane 5U Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-112
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of 2 AnaLlS ID: 901206-047 Customer Sample ID: N-125 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: )14476 Sample Matrix: SOIL Instrum~ent ID: MP-5985 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 5-DEC-1990 SNA -Base/NeutraL/Acid Compounds CTCL) Date Extracted/Prepared: 13-DEC-1990 Date Analyzed: 2-JAN-1991 Preparation Procedure Number: Analysis Procedure Numb~er: INA (CLP) NOP Percent Moisture: 6.5 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK HEADRICK Associated Blank: 901214-083 CA Fite Numiber: NA [I : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 108-95-2 Phenol R 1000U 106-47-8 4-Chloroaniline R 1000U 111-44-4 bis(2-Chtoroethyl)ether R I 000U 87-68-3 Hexachtorobutadiene R 100OU 95-57-8 2-Chtorophenol ft 1000U 59-50-7 4-Chloro-3-methylphenol ft 1000U 541-73-1 1,3-Dichlorobenzene ft I00OU 91-57-6 2-Methylnaphthalene ft IOOOU 106-46-7 1,4-Dichlorobenzene R I1000t) 77-47-4 Hexachlorocyclopentadiene R 1000U 100-51-6 Benzyl Alcohol R 1000U 88-06-2 2.4,6-Trichlorophenol t R OOOU 95-50-1 1,2-Oichlorobenzene R IOOOU 95-95-4 2,4.5-Trichlorophenol ft 5100U 95-48-7 2-Methytphenol R 100OU 91-58-7 2-ChLoronaphthatene R 1000U 108-60-1 bis(2-Chloroisopropyl)ether ft I000U 88-74-4 2-Nitroaniline R 5100U 106-44-5 4-Methytphenol ft 1000U 131-11-3 Dimethylphthalate R 100OU 621-64-7 N-Nitroso-di-n-propylamine R 1000U 208-96-8 Acenaphthylene R 1000U 67-72-1 Nexachloroethane R 1000U 99-09-2 3-Nitroaniline ft 5100U 98-95-3 Nitrobenzene ft 100OU 83-32-9 Acenaphthene R 1000W 78-59-1 Isophorone R 1000U 51-28-5 2,4-Dinitrophenol ft 5100tJ 88-75-5 2-Nitrophenol ft 100WU 100-02-7 4-Nitrophenol ft 5100U 105-67-9 2,4-Dimethytphenol ft IOOOU 132-64-9 Dibenzofuran ft 1000U 65-85-0 Benzoic Acid R 5100U 121-14-2 2,4-Dinitrotoluene ft 1000U 111-91-1 bis(2-Chloroethoxy)methane ft 1000U 606-20-2 2,6-Dinitrotoluene R 1000U 120-83-2 2,4-Dichlorophenol R 100WU 84-66-2 Diethylphthalate R 1000U 120-82-1 1,2,4-Trichlorobenzene R 100OW 7005-72-3 4-Chtorophenyl-phenytether R 1000W 91-20-3 Naphthalene R 100WU 86-73-7 Fluorene ft IOOOU Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The numb~er is the attainable detection limit for the sample. B - Anulyte was found in the reagent blank as well as the sample. J- Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D- 113
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P.O. Box 1970 Rfichland. WA 99352 W
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