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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page Z of 2 AnaLIS ID: 901206-037 Customer Samrple ID: N-117 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: )-14466 Sample Matrix: SOIL Instrument ID: HP-5985 Requisition Number: Authorized By: 0. C. Canada Date Samrple Received: 5-DEC-1990 BRA - lass/Neutral/Acid Compounids (TCL) Date Extracted/Prepared: 13-DEC- 1990 Date Analyzed: 2-JAN-1991 Preparation Procedure Nuber: Analysis Procedure Number: SNA (CLP) MOP Percent Moisture: 6.5 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AX KEADRICK Associated Blank: 901214-083 CA File Number. NA [3 Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 100-01-6 4-Nltroanitine Rt 4800Ui 53-70-3 Dibenz~a,h)anthracene ft 990U 534-52-1 4,6-Dinitro-2-methylphenot Rt 4800U 191-24-2 Benzo(g~hi)peryLene R 990U 86-30-6 N-itrosodiphenylaenine R 990t.1 101-55-3 4-Bromophenyt-pihenylether ft 99OU 118-74-1 Nexachlorobenzene ft 990U 87-86-5 Pentachlorophenot ft 4800U 85-01-8 Phenanthrene ft 990Ui 120-12-7 Anthracene Rt 990U) 84-74-2 Di-n-butylpihthaLate 1400-S, LA 206-44-0 Fluoranthene R 990U 129-00-0 Pyrene Rt 990U 85-68-7 *utylbenzylphthalate ft 990U 91-94-1 3,3'-Dichtorobenzidine ft 2001U 56-55-3 *enzo(a)anthrcrie R 991. 117-81-7 bisC2-Ethylhexyi)phthalate ft 990U. 218-01-9 Chrysene ft 9901J 117-84-0 Di-n-octylphthalate ft 990U 205-99-2 Benzo(b)fluoranthene Rt 99OU 207-08-9 genzo~k)fluoranthene ft 991. 50-32-8 Benzo(a)pyrene ft 990U 193-39-5 Indeno(1*2,3-cd)pyrene Rt 990U Data Reporting Qualifiers: U -Compound was analyzed for but not detected. The numbier is the attainable detection limit for the sample. 0 Analyte was found in the reagent blank as well as the samiple. J1 - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-80
WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department SNA CTCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUND S AnaLlS 10: 901206-037 Customer Samvple ID: N-117 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Samp~le Matrix: SOIL File ID: ),14466 Level: Clow/med): LOW Date Received: 5-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 2-JAN-1991 % Moisture: not dec. .6.5 dec. _____Date Extracted: 13-DEC-1990 Extraction: (SepF/ContlSonc) SoxH PH: GPC Cleanup: (YIN) N Concentration Units Number TiCs foun~d: 18 Cug/L or ug/Kg): _uLK CAS NUMBER ICOMPOUND NAME RT EST. CONC. a I1. I2. I3. 123-42-21 2-Pentenone. 4-hydroxy-4-methy 1UNKNOWN 1 UNKNOWN ALCOHOL j ;0 60 6.i :9 3 iO Ii90- 4. 1._____ UNKNOWN ALCOHOL ;39 2899 1 d o I5. 1 UNKNOWN -3 6. I7. 1 UNKNOWN 1UNKNOWN HYDROCARBON ;99 2OV9 *15)7 500I w T9 J3 I8. jUNKNOWN HYDROCARBON J 23.92 44 I~ "9 I9. 10. jUNKNOWN PHTHALATE ESTER jUNKNOWN HYDROCARBON 1 ;4.4 24.a7 I750 /,a I' J" I 1 I11. I12. I13. I14. I15. I16. jUNKNOWN HYDROCARBON JUNKNOWN HYDROCARBON jUNKNOWN HYDROCARBON JUNKNOWN HYDROCARBONJ £UNKNOWN HYDROCARBON £UNKNOWN HYDROCARBON j I j j j 6.2 3I!! 2. 0'I V.83 I )0.09 I" FI70 .19- 0 'OIO o~ I.odO I 17. jUNKNOWN ALKOXY COMPOUND 5!0 10 4eg 0 -; la. 119. ____ 120.1I 121. ____ jUNKNOWN HYDROCARBON I !1.90 1200 I a 122.1 123.1II III I 124. III 125.1I II 126.1I I 128.1- I 129. . ~30. I I Data Reporting Qualifiers: U - Comvpound was analyzed for but not detected. The number is the attainable detection limit for the sample. 8 - Anolyte was founid in the reagent blank as well as the saple. J -Indicates an estimated value. NOD Not detected. A - Aldol condensation product. 0 - Secondary dilution. E -Exceeds initial calibration range. P - Probable Identification. D-81
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