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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLIS ID: 901206-043 Customer Samrple ID: N-121 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: )14472 Sample Matrix: SOIL Instrument ID: HP-5985 Requisition Number: Authorized By: D. C. Canada Date Samrple Received: 5-DEC-1990 BRA - Base/Neutral/Acid Comrpounmds (TCL) Date Extracted/Prepared: 13-DEC-1990 Date Analyzed: 2-JAN-1991 Preparation Procedure Number: Analysis Procedure Number: BNA CCLP) MOP Percent Moisture: 5.5 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: AK HEADRICKC Associated Blank: 901214-083 OA File Numiber: NA C]:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ...... ........................... .......... ........... .............................. .......... 100-01-6 4-Nitroaniline R 4800U 53-70-3 Dibenz~a~h)anthracene R 980U 534-52-1 4,6-Dinitro-2-methylphenol R 4801U 191-24-2 Benzog,h,I)perylene R 960U 86-30-6 N-Nitrosodiphenylamine R 980U 101-55-3 4-Bromophenyl-phenylether R 980U 118-74-1 Hexachlorobenzene R 980U 87-86-5 Pentachtorophenot R 480OU 85-01-8 Phenanthrene R 98OU 120-12-7 Anthracene R 980U 84-74-2 Di-n-butylphthalate 4300't, U~ 206-44-0 Fluoranthene R 980U 129-00-0 Pyrene R 980U 85-68-7 Butylbenzylphthalate R 980U 91-94-1 3,3'-Dichtorobenzidine R 2000U 56-55-3 Benzo~a)anthracene R 980U 117-81-7 bisC2-EthylhexyL)phthatate R 980U 218-01-9 Chrysene R 980U 117-84-0 Di-n-octylphthalate R 980U 205-99-2 Benzo(b)fluoranthene R 980U 207-08-9 Denzo(k)fLuoranthene R 980U lI 50-32-8 Benzo(a)pyrene R 980U 193-39-5 lndeno(l.2,3-cd)pyrene R 980U Data Reporting Qualifiers: U - Comrpound was analyzed for but not detected. The numiber is the attainable detection limit for the samrple. B - Analyte was founmd in the reagent blank as well as the samrple. J - Indicates an estimated value. RD - Not detected. A - Aldol condensation product. D - Secondary dilution. E -Exceeds initial calibration range. D -98
WHC-SD-EN-TI-136, Rev. 0 oak Ridge K-25 site Analytical Chemistry Department BNA CTCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS ID: 901206-043 Customer Sample ID: N-121 Laboratory: organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL File ID: ),14472 Level: (tow/med): Low Date Received: 5-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 2-JAN-1991 % Moisture: not dec. 5.5 dec. _____Date Extracted: 13-DEC-1990 Extraction: (SepF/Cont/Sonc) SoxH PHt: - GPC Cleanup: (YiN) N Concentration Units Number TICs found: 19 (ugiL or ugiKg): uqLa CAS NUMBER COMPOUND NAME RT IEST. CONC. 0 I1. I2. I3. 4 ._ 123-42-21 2-Pentanone. 4-hydroxy-4-methy 1UNKNOWN ALCOHOL 1UNKNOWN _ _ _ 1 UNKNOW.N 1 5 .;Z 1 109 j-AO.i581 i Z - I.~ - 109 1 e389 -- 4;. 17.2!300 1Ja 5. 6. 1 UNKNOWN 1 UNKNOWN 19i.Z9 1 20.9 17000s + d" -oo--4--de- 7. 1 UNKNOWN PNALATE ESTER j 4.68. So I 48 I I .IUNKNOWN ALKOXY COMPOUND j 24.84j 980O1 10. 11. ______UNKNOWN jANTHRACENEDIONE HYDROCARBON 1 6.05 j Z0.30 ~ 4000-4-49 I 12. 13. 14. 15. 16. UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON UNKNOWN HYDROCARBON jUNKNOWN HYDROCARBON UNKNOWN HYDROCARBON j I I 1 I Z7.Z 28.;q 29.6.3 29.80 I 30.86I 13 I 2888I 120is~ Q9 2300 I 1 100J 17. jUNKNOWN HYDROCARBON 31.0e I 74404-a 18. ______jUNKNOWN HYDROCARBON I 31.06 we 703 19. jUNKNOWN ALKOXY COMPOUND 37.24 2600 1 120.1__ _ _ _ _ _ _ _ _ _ 1__ _ _ 1__ _ _ 1__ _ 121. _ _ _ _1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _ _ 122.1__ _ _ _ _ _ _ _ _ _ 1 _ _ _ 11__ _ I 123. 1_ _ _ _ _ _ _ _ _ _ _1_ _ _ _1_ _ _ _ _ _ .24. 1_ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _1_ _ 125. 1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ _ _ 126.1__ _ _ _ _ _ _ _ _ _ 1__ _ _ 1__ _ _ 1__ _ 127.1__ _ _ _ _ _ _ _ _ _ 1__ _ _ 1__ _ _ 1__ _ 128.1__ _ _ _ _ _ _ _ _ _ 1__ _ _ 1__ _ _ 1__ _ 129.1 _ _ _ _ _ _ _ _ _ _ 1__ _ _ 1__ _ _ 1__ _ 130. I ___ _ Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sampl~e. 8 - Analyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. P - Probable Identification. D-99
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