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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 2 AnaLIS ID: M0206-031 Customer Sample ID: N-111 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 10660 Sample Matrix: SOIL Instrument ID: 597053 Reuqisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 RNA -Base/Neutral/Acid Compounds (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 14-DEC-1990 Preparation Procedure Number: Analysis Procedure Number: BHA CCLP) MOP Percent Moisture: 6.1 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEEHAN Associated Blank: 901213-028 GA File Number: NA UI : Result has been Corrected for Spike CAS ug/Kg CAS ugfKg ...... ............................ .......... ........... .............................. .......... 108-95-2 Phenol 99WU 106-47-8 4-Chtoroaniline 990U 111-14-4 bis(2-Chloroethyl)ether 990t.3 57-68-3 Hexachtorobutadiene 990U 95-57-8 2-Chlorophenol 991. 59-50-7 4-Chloro-3-methytphenot 990U 541-73-1 1,3-Dichtorobenzene 991. 91-57-6 2-MethytnaplhthaLene 990U 106-4.6-7 1*i-Dichlorobenzene 99OU 77-47-4 Nexachtorocyclopentadiene 990U 100-51-6 *enzyl Alcohol 99OU 58-06-2 2,4,6-TrichLorophenol 990U 95-50-1 1,2-Dichlorobenzene 99WU 95-95-4. 2,4.5-TrichLorophenoL 1.800U 95-1.8-7 2-Methytphenol 99WU 91-58-7 2-ChloronaphthaLene 990U 108-60-1 bis(2-Chlorolsopropyt)ether 99WU 88-74-1. 2-Nitroaniline 480OU 106-4.4-5 4-Methytphenol 990U 131-11-3 Dimethyiplithatate 990UJ 621-64-7 U-Nitroso-di-n-propylamine 99WU 208-96-8 Acenaphthytene 990U. 67-72-1 Hexachloroethane 9901 99-09-2 3-Nitroaniline 4800U 98-95-3 NItrobenzene 99WU 83-32-9 Acenaphthene 990U 78-59-1 Isophorone 99WU 51-25-5 2,I.-Dinitrophenol 4800U 88-75-5 2-Nitrophenol 990W 100-02-7 4-Nitrophenol 1.800U 105-67-9 2.4-Dimethytphenot 990U 132-64-9 Dibenzofuran 990U 65-85-0 Benzoic Acid -9,90 e+-*&fl- LA 121-14-2 2,4-Dinitrotoluene 99GU 111-91-1 bis(2-Chicroethoxy)methane 99WU 606-20-2 2,6-Dinitrotoluene 990U 120-83-2 2,4-Dichlorophenol 99WU 84-66-2 Diethylphthalate C 10 ~E-uie- LA 120-82-1 1,2,4-Trichlorobenzene 990U 7005-72-3 4-Chlorophenyl-phenylether 990U 91-20-3 Naphthalene 990U 86-73-7 Fluorene 990U Data Reporting Qualifiers: U -Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. B -Analyte was found in the reagent blank as well as the sample. J -Indicates an estimated value. RD -Not detected. A -Aldol condensation product. D Secondary dilution. E -Exceeds initial calibration range. D- 54
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLIS 1D: 901206-031 Customer Sample 10: N-111 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File 1D: 10660 Sample Matrix: SOIL Instrument ID: 597053 Requisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 UNA - Base/Neutral/Acid Compounds (TCL) Date Extracted/Prepared: 12-DEC- 1990 Date Analyzed: 14-DEC- 1990 Preparation Procedure Numb~er: Analysis Procedure Nuber: INA CCLP) HOP Percent Moisture: 6.1 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEEHAN Associated Blank: 901213-028 CA File Nwvber: NA El : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 100-01-6 /s-Nitroaniline 4080011 53-70-3 Dibenz(a,h)anthracene 99011 534-52-1 4,6-Dinitro-2-methytphenot 480011 191-24-2 Benzo(g,h~i)peryiene 9901 86-30-6 N-Uitrosodiphenylamine 99011 101-55-3 4-Bromopheny-phenytether 99011 118-74-1 Mexachlorobenzene 99011 87-86-5 Pentachtorophenot 480011 85-01-8 Phenanthrene 9901 120-12-7 Anthracene 99011 84-74-2 Di-n-butylphthalate - ie g- 99io LA 206-44-0 Fluoranthene 99011 129-00-0 Pyrene 99011 85-68-7 Butylbenzylphthalate 9901 91-94-1 3,31-Dichtorobenzidine 20001U 56-55-3 Senzo(a)anthracene 99011 117-81-7 bis(2-Ethythexyt)phthaLate 40-B do Cley0 LA 218-01-9 Chrystne 99011 117-84-0 Di-n-octylphthalate 99011 205-99-2 *enzo(b)fluoranthene 99011 207-08-9 Benzo(k)fluoranthene 99011 50-32-8 Ienzo(a)pyrene 99011 193-39-5 Indeno(1,2,3-cd)pyrene 99011 Data Reporting Qualifiers: U1 - Compound was analyzed for but not detected. The number Is the attainable detection Limit for the sample. B - Analyte was found in the reagent blank as well as the samiple. J - Indicates an estimated value. ND - Not detected. A - Aidol condensation product. 0 - Secondary dilution. E - Exceeds initial, calibration range. D-55
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P.O. Box 1970 Rfichland. WA 99352 W
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