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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLIS ID: 901206-029 Customer Sample I0: 3-109 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File 10: 10658 Sample Matrix: SOIL Instrument 10: 59703 Requisition Number: Authorized By: 0. C. Canada Date Sample Received: 6-DEC-1990 BNA -Base/Neutral/Acid Compounds CTCL) Date Extracted/Pr epa red: 12-DEC-IM9 Date Analyzed: 14-DEC-1990 Preparation Procedure Numb~er: Analysis Procedure Number: INA (CLP) NOP Percent Moisture: 8.0 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C MEENH Associated Blank: 901213-028 CA Fite Number: NA (I : Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ...... ............................ .......... ........... .............................. .......... 100-01-6 4-Nitroaniline 4701. 53-70-3 Dibenz~a,h)anthracene 980U 534-52-1 4,6-Dinitro-2-methytphenot 4700tU 191-24-2 Benzo(g~hi0perylene 98OU 86-30-6 M-Nitrosodiphenylamine 980U 101-55-3 4-Bromophenyl-phenvylether 9B0U 118-74-1 Nexachlorobenzene 9801. 87-86-5 Pentachtorophenol 4700tU 85-01-8 Phenanthrene 980U 120-12-7 Anthracene 981. 84-74-2 Di-n-butylphthalate 1700& %A 206-44-0 Fluoranthene 981. 129-00-0 Pyrene 980U 85-68-7 Butylbenzylplithalate 9BOU 91-94-1 3,3'-Dichtorobenzidinte 200OU 56-55-3 Senzo~a)anthracene 980U 117-81-7 bis(2-EthyLhexyt)phthaLate 380 d- -160 LA 218-01-9 Chrysene 98WU 117-84-0 Di-n-octylphthalate 981. 205-99-2 Uenzo(b)fluoranthene 98OU 207-08-9 Benzo(k)fluoranthene 980U 50-32-8 Benzo(a)pyrene 98OUI 193-39-5 Indeno(l*2,3-cd)pyrene 981.1 l / Data Reporting Qualifiers: 10%6 / U - Compounmd was analyzed for but not detected. The number Is the attainable detection limit for the sample. B - Analyte was founmd in the reagent blank as welt as the samle. J - indicates an estimated value. RD - Not detected. A - Aldol condensation product. 0 - Secondary dilution. E - Exceeds initial calibration range. D-46
WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department BNA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOUNDS AnaLIS 10: 901206-029 Customer Sample 1D: P-109 Laboratory: Organic Mass Spectroscopy Laborator Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL Fite ID: 10658 Level: (loa/med): LOW Date Received: 6-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 14-DEC-1990 % Moisture: not dec. 8.0 dec. _____Date Extracted: 12-OEC-1990 Extraction: (SepFIContISonc) SoxH PH: ____ GPC Cleanup: (YIN) N Numb~er TICs found: 14 Concentration Units (ug/L or uglKq): _uL~ I CAS NUMBER COM4POUND NAME j RT EST. CONC. a I1. I2. I3. 141-79-71 3-Penten-2-one, 4-methyl- 123-42.21 2-Pentanone. 4-hydroxy-4-methy 1 Unknown (Alkyt Hydrocarbon) j4.93 j I1100 .A J . 9 140300 d O 18.23 I580 IJ 4. jUnknown (Alkyt Hydrocarbon) j 18.78 I600 I 1 5. jUnknown (Atkyt Hydrocarbon) £ 19.43 I1800 1 6. jUnknown (Alkyl Hydrocarbon) 2 1.69-i 1180-4- JO 7. jUnknown (sat'd Hydrocarbon) j 2.?9 6C i5 0l a .j 9. J Unknown (sat'd Hydrocarbon) 1 Unknown _ n I11C - 25.87 j460 404 I 1 .1 10. Ill.___ 12. Unknown (Alkyt Hydrocarbon) _ junknown jUnknown (sat'd Hydrocarbon) I I61 2648- 27.69k 7 --- O I-a 5801 J -- see.- I.' da 13. 14. 115. ____ jUnknown (Atkyt Hydrocarbon) jUnknown (Hydrocarbon) I 32.59 430 J ~ 33.43 11200 J 116. _ 17. ____ 118. ____ 119. ____ _ _ 120.1I I 121. ____1II 22?.____ 123.1 124.1 125.1I I I 126. I 127. II 128. I 129. 130. I I I Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The numb~er is the attainable detection limit for the sample. B - Analyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. RD - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. P - Probable Identification. D-47
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P.O. Box 1970 Rfichland. WA 99352 W
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