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WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-ZS <strong>Site</strong> Analytical Chemistry Department BNA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED CMPOUJNDS AnaLIS ID: 901206-032 Customer Sample ID: N-112 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Sample Matrix: SOIL File ID: 10661 Level: (lowlmed): LOW Date Received: 6-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 14-DEC-1990 % Moisture: not dec. 4.3 dec. _____Date Extracted: 12-DEC-1990 Extraction: (SepFlContlSorc) SoxH PH: ____ GPC Cleanup: CYIN) N Concentration Units Number TICs found: 16 (ug/L or uglKg): u2K ICAS NLUER COMPOUND NAME I RT jEST. CONC. 0 1. 141-79-71 3-Penten-2-one, 4-methyl- I2. 123-42-21 2-Pentanome. 4-hydroxy-4-methy I3. 572-50-41 2-Pyrrolidinome. 1-methyl- I4. 25013-16-51 Phenot.(I.1-dimethylethyt)-4-m I5. 17851-53-51 1.2-genzenedicarboxytic acid~b I6. Unknown (sat'd Hydrocarbon) I7. JUnknown (Atkyl Hydrocarbon) 1 1 j 1.92 1 9.9? ! 9 8;1 4 14 piE.3 I Z1.69 I3 229 430 1 JiA 3190 I JM S60 se i d0 o 7990 I d~ o- L0 We 0J I 8. I'.__ 10. 11. jUnknown (Alkyt Hydrocarbon) _ JUnknown JUnknown (sat'd Hydrocarbon) JUnknown (Atkyl Hydrocarbon) j I J :L7" 3;9 I 24.00!1 2569 I 25.91 j970 o 440 1 1J - iNO ! - 1 q 12. I13. 123-79-51 Dloctyl Adipate 1 Unknown (Alkyt Hydrocarbon) j 26.40 j 46 to'I 2500 1 J J 114. 15. 1 Unknown 1 Unknown (Hydrocarbon) j J 27.711 e 1.I4.. 1400 1 ;40 d o 16. junknown j 33.57j 1000 1 17. 1 _ _ _ _ _ _ _ _ 1 _ _ _ 118. _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ 119.1__ _ _ _ _ _ _ _ _ _ 1__ _ _ 1 _ _ _ __ _ 120.1__ _ _ _ _ _ _ _ _ _ 1__ _ _ _1_ _ _ _ __ _ I 121.1__ _ _ _ _ _ _ _ _ 1.1_ _ _ _1_ _ 122. 1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _I_ _ _ _ 123. 1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _1_ _ _ _ 124. 1_ _ _ _ _ _ _ _ _ _ _ _ _ _ _I_ _ _ _ _ _ 125._II_ _ _ _ __ _ _ _ _ 126. __ _ _ _I_ _ _ _ I__ _ I 127.I __ _ _ _I_ _ _ _ __ _ I 128. __ _ _ _I_ _ _ _ I__ _ I 129. __ _ _ _I_ _ _ _ I__ _ I 130.II__ _ _ _I_ _ _ _ I__ _ I Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. 8 - Analyte was foun~d in the reagent blank as well as the sample. J3 - Indicates an estimated value. NO - Not detected. A - Atdol condensation product. O - Secondary dilution. E - Exceeds Initial calibration range. P - Probable Identification. D-60
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 1 AnaLIS I0: 901206-032 Customer Samrple ID: N-112 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 07616 Samrple Matrix: SOIL Instrument ID: 5970#2 Requisition Number: Authorized By: 0. C. Canada Date Samrple Received: 6-DEC-1990 VGA -Volatile Organic Compoun~ds CTCL) Date Extracted/Prepared: Date Analyzed: 11-DEC-1990 Preparation Procedure Number: PURGE & TRAP Analysis Procedure Numbier: VOA (CLP) NOP Percent Moisture: 6 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: CL HUDDLESTON Associated Blank: 901211-004 GA File Numer: NA U:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg ...... ................... .......... ........... .............................. .......... 74-87-3 Chtoromethane 11U 79-00-5 1,1.2-TrichLoroethane 5U 74-83-9 Bromomethane 11U 71-43-2 Benzene 5U 75-01-4. Vinyl Chloride 11U 10061-02-6 trans-1,3-Dichloropropene 5U 75-00-3 Chtoroethane 11U 75-25-2 Bromoform 5U 75-09-2 Methylene Chloride su 108-10-1 4-Methyl-2-pentenone 11U 67-64-1 Acetone 28 ILA 591-78-6 2-Hexanone 11u 75-15-0 Carbon Disulfide 5U 127-18-4 Tetrachloroethene 5U 75-35-4 1,1-Dichloroethene 5U 79-34-5 1.1.2,2-Tetrachloroethane 5U 75-36-3 1,1-Dichloroethane SU 108-88-3 Toluene 5U 540-59-0 1,2-Dichtoroethene (total) 5U 108-90-7 Chlorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-Dichloroethane SU '100-42-5 Styrene 5U4 78-93-3 2-Butanone 11U 1330-20-7 Xylene (total) 5U4 71-55-6 1.1,1-Trichloroethane 514 56-23-5 Carbon Tetrachloride 5U4 108-05-4 Vinyl Acetate 1114 75-27-4 Bromodichioromethane 514 78-87-5 1,2-Dichtoropropane SU 10061-01-5 cis-1,3-Dichtoropropene 514 79-01-6 Trichloroethene 514 124-48-1 Dibromchtoromethane 514 Data Reporting Oualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection limit for the sample. B - Anelyte was found In the reagent blank as well as the sample. J1 - Indicates an estimated value. ND - Not detected. A - Aldol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D-61
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