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WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 1 of 2 AnaLIS ID: 901206-022 Customer Sample to: N-104 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 10649 Sample Matrix: SOIL Instrument ID: 597013 Reqisition Number: Authorized By: D. C. Canada Date Sample Received: 6-DEC-1990 RNA -Base/Neutral/Acid compounds CTCL) Date Extracted/Prepared: 12-DEC- 1990 Date Analyzed: 13-DEC-1990 Preparation Procedure Nu~mber: Analysis Procedure Number: DNA (CLP) NDP Percent Moisture: 5.2 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C KEENAN Associated Dlank: 901213-028 DA File Number: NA Cl:Result has been Corrected for Spike CAS ug/Kg CAS ug/Kg 108-95-2 Phenol IOOOU 106-47-8 4-Chtoroanitine 100OU 111-44-4 bisc2-Chtoroethyt)ether 1000U 87-68-3 Nexachlorobijtadiene 100OU 95-57-8 2-Chlorophenol 1000u 59-50-7 4-Ch Loro-3-methyLphenot 1000u 541-73-1 1,3-Dichlorobenzene 100OU 91-57-6 2-Methylnaphthalene 1000U 106-46-7 1*I-Dichtorobenzene WOW0 77-47-4 NexachLorocyctopentadiene 1000U 100-51-6 DenzyL Alcohol I DOW 88-06-2 2.,6-Trichlorophenol 100OU 95-50-1 1.2-Dichlorobenzene I1000U 95-95-4 2,4,5-TrichtorophenoL 4900U 95-48-7 2-MethytphenoL 100OU 91-58-7 2-Chloronaphthatene 1000U 108-60-1 bisC2-Chioroisopropyl)ether 1000U) 88-74-4 2-Nitroaniline 4900U 106-44-5 4-Methyiphenol 1000U 131-11-3 Dimethytphthalate 100OU 621-64-7 N-Nitroso-di-n-propyanine 100OU 208-96-8 Acenaphthytene 1000U 67-72-1 Hexachloroethane NOWO 99-09-2 3-Nitroanilina 4900U 98-95-3 Nitrobenzene 1000U 83-32-9 Acenaphthenve 1000U 78-59-1 isophorone 1000U 51-28-5 2.4-Dinitrophenol 4900U 88-75-5 2-Nitrophenol 1000U 100-02-7 4-Nitrophenol 4900U 105-67-9 2,4-Dimethytphentol 100OU 132-64-9 Dibenzofuran l0Ou 65-85-0 Denzoic Acid /600 WO do Lot 121-14-2 2,4-Dinitrotoluene 1000U 111-91-1 bis(2-ChLoroethoxy)methane 1000U 606-20-2 2,6-DinitrotoLuene 1000U 120-83-2 2,4-Dichlorophenol 100WU 84-66-2 DiethylphthaLate 1660 ego'-G do . 120-82-1 1,2,4-Trichtorobenzene 100OW 7005-72-3 4-Chtorophenyt-phenyLether 1000U 91-20-3 Naphthalene 100WU 86-73-7 FLuorene 1000U Data Reporting Qualifiers: U - Compound was analyzed for but niot detected. The numbi*er is the attainable detection limit for the samople. B - Analyte was founid in the reagent blank as well as the sample. J1 - Indicates an estimated value. ND - Not detected. / A-AldoL condensation product. D - Secondary dilution. E-Exceeds initial calibration range. D -28
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page 2 of 2 AnaLIS ID: 901206-022 Customer Sample 10: N-104 Laboratory: Organic Has$ Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK Fite ID: 10649 Sample Matrix: SOIL instrument ID: 597013 Requisition Number: Authorized By: 0. C. Canada Date Sample Received: 6-DEC-1990 BNA - *ase/NeutratlAcid Compounds (TCL) Date Extracted/Prepared: 12-DEC-1990 Date Analyzed: 13-OEC-1990 Preparation Procedure Number: Analysis Procedure Nmb~er: OKA (CLP) HOP Percent Moisture: 5.2 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: C KEENAN Associated Blank: 901213-028 aA File Number: NA [1 : Result has been Corrected for Spike CAS uglK9 CAS ug/Kg ...... ................... .......... ........... .............................. .......... 100-01-6 4-Nitroanitine 490OU S3-70-3 Dibenz~ah)anthracene 1000U S34-52-1 4.6-Dinitro-2-methylphenaL 4900U 191-24-2 *enzo(g,i)perytene I 000U 86-30-6 N-Nitrosodiphenytamine lOOOU 101-55-3 4-IroniophenyL-phenytether IOOOU 118-74-1 Hexachlorobenzene 100OU 87-86-5 PentachlorophenoL 4900W 85-01-5 Phenanthrene I100WU 120-12-7 Anthracene I1000t 84-74-2 Di-n-butyLphthaLate 260O'D.. L& 206-44-0 Ftuoranthene I100WU 129-00-0 Pyrene 100WU 85-68-7 Uutytbenzylphthalate 100WU 91-94-1 3,31-Dichlorobenzidine 200WU 56-55-3 Benzo(a)anthracene 117-81-7 bis(2-Ethythexyt)phthatate I100WU &MdO m; O10b LA 215-01-9 Chrysene 100Wt 117-84-0 Di-n-octylphthalate 100WU 205-99-2 Benzo(b)ftuoranthene 100OW 207-08-9 *enzo~kfluoranthene 1000W 50-32-8 Senzo(a)pyrene 100WU 193-39-5 Indeno(1,2,3-cd)pyrene 100WU Data Reporting Qualifiers: % l I U - Compound was analyzed for but not detected. The number is the attainable detection limit for the samrple. 8 Anatyte was found in the reagent blank as well as the sample. J - Indicates an estimated value. NO - Not detected. A -Atdol condensation product. D - Secondary dilution. E - Exceeds initial calibration range. D -29
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