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WHC-SD-EN-TI-136, Rev. 0 Oak Ridge K-25 <strong>Site</strong> Analytical Chemistry Department SNA (TCL) SOIL ORGANICS ANALYSIS DATA SHEETS TENTATIVELY IDENTIFIED COMPOULND S AnaLIS ID: 901206-022 Customer Sample ID: N-104 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SNUCK Sample Matrix: SOIL Fite ID: 10649 Level: (low/mnd): LOW Date Received: 6-DEC-1990 Dilution Factor: 1.0 Date Analyzed: 13-DEC-1990 % Moisture: not dec. 5.2 dec. Date Extracted: 12-DEC-1990 Extraction: (SepF/Cont/Sonc) SOXH PH: GPC Cleanup: (Y/N) N Concentration Units Number TICs found: 16 (uglL or uglKg): _uL~ CAS NUMIER COMPOUND NAME R T jEST. CONC. a I1. 123-42-21 2-Pentanone, 4-hydroxy-4-methy I4 1(000 1 j 2.- 872-50-41 2-Pyrrotidinone, 1-methyl- I 9.82 ! 4ZO I 13. 1 Unknown 1 12.50! 7401. 4._25013-16-51 Phenot.(1.1-dimethytethyl)-4-m j .d.;I J 5- 1 Unknown (Atkyt Hydrocarbon) 1 19.44 I560 . 1 6. 17851-53-51 1.2-Benzenedicarboxytic acid.b 7. jUnknown (sat'd Hydrocarbon) 8. jUnknown I .______ Unknown (Alkyl Hydrocarbon) 10. IUnknown (Atkyt Hydrocarbon) I11- Unknown 12. IUnknown (sat'd Hydrocarbon) 2i1.38 -63 49- 2i6 4-9 1 I21.94 j630 I. 12 M .3- ~ .?*. ----- -! 0--O I24.11 J.440 I .9 I5 Al I1-dyOI 13.Unknown 14. IUnknown (sat'd Hyrocarbon) 15. IUnknown I16. IUnknown (sat'd Hydrocarbon) 117. 18. III___ I I27.74 25.99j 2&4 I I2400 31IZ I___ 450 1 ... 4 j l 1.1 j- 120. IIIj___ 121. II___ 122. .___I 123. II___ 124. III___ 125.- 1.___ 126.I .___I 127. III___ 128. II___ 129.I I 130.I II Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection Limit for the sample. 8S Analyte was found in the reagent blank as well as the sample. J-Indicates an estimated value. ND - Not detected. A -Aldo( condensation product. D Secondary dilution. E - Exceeds initial calibration range. P -Probable Identification. D-30
WHC-SD-EN-TI-136, Rev. 0 ANALYSIS DATA REPORT Page I of 1 AnaLIS ID: 901206-022 Customer Sample ID: M-104 Laboratory: Organic Mass Spectroscopy Laboratory Customer: J. KESSNER/R. SHUCK File ID: 07600 Sample Matrix: SOIL Instrument ID: 597002 Requisition Number: Authorized Dy: D. C. Canada Date Sample Received: 5-DEC-1990 VGA - volatile Organic Compounmds CTCL) Date Extracted/Prepared: Date Analyzed: 10-DEC- 1990 Preparation Procedure Nuber: PURGE & TRAP Analysis Procedure Number: VOA CCLP) MOP Percent Moisture: 5 Dilution Factor: 1.0 Percent Moisture (decanted): Analyst: SL STAFFORD Associated Blank: 901210-025 GA File Number: NA D : Result has been Corrected for Spike CAS ug/Kg CAS uglKg 74-87-3 ChLoromethane 1U1 79-00-5 1,1,2-TrichLoroethane SU 74-83-9 Bromomethane IllU 71-43-2 Benzene 5U 75-01-4 Vinyl Chloride 11U 10061-02-6 trans-1,3-Dichloropropene 5U 75-00-3 Chtoroethane litu 75-25-2 Bromoform 5U 75-09-2 Nethylene Chloride 5 dB~e LA 108-10-1 4-Methyl-2-pentanone 11U 67-64-1 Acetone 27 1. LA 591-78-6 2-Hexanone 11u 75-15-0 Carbon Disulfide 5U 127-18-4 Tetrachtoroethene 5U 75-35-4 1,1-Dichtoroethene 51) 79-34-5 1,1,2,2-Tetrachioroethane 5U 75-34-3 1,1-Dichloroethane 5U 108-88-3 Toluene 5U 540-59-0 1,2-Dichtoroethene (total) 5U 108-90-7 Chlorobenzene 5U 67-66-3 Chloroform 5U 100-41-4 Ethylbenzene 5U 107-06-2 1,2-DichLoroethane 5U 100-42-5 Styrene 5U 78-93-3 2-Butanone llU 1330-20-7 XyLene (total) 5U 71-55-6 1,1,1-TrichLoroethene 5U 56-23-5 Carbon Tetrachloride 5U 108-05-4 Vinyl Acetate 11t; 75-27-4 Drombdichloromethane 5U 78-87-5 1,2-DichLoropropane SU 10061-01-5 cis-1,3-Dichloropropene 5U 79-01-6 Trichloroethene 5U 124-48-1 Dibromochloromethane 5U Data Reporting Qualifiers: U - Compound was analyzed for but not detected. The number is the attainable detection Limit for the sample. * - Analyte was foun~d in the reagent blank as well as the sample. J1 - Indicates an estimated value. NO - Not detected. A - AldoL condensation product. O - Secondary dilution. E - Exceeds initial calibration range. D-31
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